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US4087366A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of preparing a piezoelectric ceramic composition

Assignee: TDK ELECTRONIC Co
•
Filing: 1973-11-30
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Granted: 1978-05-02
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Expires: 1993-11-30
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Abstract

Abstract A piezoelectric ceramic composition which comprises the combination of a pyrochlore composite oxide and a base ceramic mixture of PbTiO 3 and PbZrO 3 is prepared by individually forming pyrochlore composite oxide, PbTiO 3 and PbZrO 3 components; and sintering a mixture of the formed components at a temperature greater than 1,000° C.

Inventors

  • 👤 Yoichi Tanaka
  • 👤 Masamichi Tsuruta
  • 👤 Koji Takahashi
  • 👤 Tsutomu Hasegawa
  • 👤 Makoto Hori

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 06:19
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/01; C04B35/48; C04B35/49; C04B35/491; H; H10; H10N; H10N30/00; H10N30/80; H10N30/85; H10N30/853

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 176 words
A method for preparing a piezoelectric ceramic composition of the formula ##STR1## wherein said pyrochlore composite oxide is selected from the group consisting of Cd 2 Sb 2 O 7 , Cd 2 Nb 2 O 7 , Pb 2 Sb 2 O 7 , Pb 2 Nb 2 O 7 , Sr 2 Sb 2 O 7 , Sr 2 Nb 2 O 7 , Ba 2 Sb 2 O 7 and Ba 2 Nb 2 O 7 ; 0.2 ≦ y ≦ 0.8; 0.2 ≦ z ≦ 0.8; y+z = 1.0 and 0.001 ≦ x ≦ 0.2, and containing 0.01 to 3.0 wt% Mn as MnO 2 comprising: individually forming lead titanate, lead zirconate and pyrochlore composite oxide components; mixing said components with MnO 2 in an amount equivalent to 0.01 to 3.0 wt% Mn to provide a mixture in which said lead titanate, lead zirconate and pyrochlore composite oxide are present in amounts that satisfy said formula; and sintering said mixture at a temperature greater than 1000° C to form said piezoelectric composition.
Claim 2
Independent Claim 176 words
A method for preparing a piezoelectric ceramic composition of the formula ##STR1## wherein said pyrochlore composite oxide is selected from the group consisting of Cd 2 Sb 2 O 7 , Cd 2 Nb 2 O 7 , Pb 2 Sb 2 O 7 , Pb 2 Nb 2 O 7 , Sr 2 Sb 2 O 7 , Sr 2 Nb 2 O 7 , Ba 2 Sb 2 O 7 and Ba 2 Nb 2 O 7 ; 0.2 ≦ y ≦ 0.8; 0.2 ≦ z ≦ 0.8; y+z = 1.0 and 0.001 ≦ x ≦ 0.2, and containing 0.01 to 3.0 wt% Mn as MnO 2 comprising: individually forming lead titanate, lead zirconate and pyrochlore composite oxide components; mixing said components with MnO 2 in an amount equivalent to 0.01 to 3.0 wt% Mn to provide a mixture in which said lead titanate, lead zirconate and pyrochlore composite oxide are present in amounts that satisfy said formula; and sintering said mixture at a temperature greater than 1000° C to form said piezoelectric composition.
Claim 3
Dependent Claim 19 words
The process of claim 1, which further comprises: calcining said mixed components prior to the sintering of said mixture.

References Cited (Backward Citations)

GB1052870A Cited
US3194765A Cited
US3344073A Cited
US3518199A Cited
US3669887A Cited
US3649540A Cited
US3661781A Cited
US3671765A Cited
DE2001290A1 Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-05-01 1981-10-31 1982-05-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-05-01 1985-10-31 1986-05-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-05-01 1989-10-31 1990-05-02 $7700.00 Window Closed / Lapsed

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