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US4081338A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of breaking an oil-in-water emulsion

Assignee: Ford Motor Co
•
Filing: 1976-12-27
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Granted: 1978-03-28
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Expires: 1996-12-27
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Abstract

Abstract This disclosure is directed to a method of breaking an oil-in-water emulsion. Briefly, the method includes the steps of adjusting the pH of the oil-in-water emulsion to a pH in the range of 6 to 10. At least one part per million of a cation selected from Fe+2, Fe+3, Al+3, Cu+1 and Cu+2 is added to the oil-in-water emulsion. Thereafter, the oil-in-water emulsion is treated with a dissolvable iron electrode, the electrode being dissolvable by transmitting an electric current thereto. Sufficient electric current is transmitted through the electrode to develop a ferrous ion/oil weight ratio of at least 0.02. After treatment by the dissolvable electrode, the oil-in-water emulsion is held until the emulsion breaks.

Inventors

  • 👤 Amos Golovoy

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 20:30
CPC Classifications
B; B01; B01D; B01D17/00; B01D17/02; B01D17/04; B01D17/047; B01D17/06

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 107 words
A method of breaking an oil-in-water emulsion which comprises: adjusting the pH of the oil-in-water emulsion to a pH in the range of 6 to 10; adding to the oil-in-water emulsion at least 1 part per million of a cation or a combination thereof selected from the group of cations consisting essentially of Fe+2, Fe+3, Al+3, Cu+1 and Cu+2; treating the oil-in-water emulsion with a dissolvable iron electrode, said dissolvable iron electrode being dissolved by transmitting an electric current therethrough in an amount sufficient to develop an Fe+2/oil weight ratio of at least 0.02; holding the oil-in-water emulsion treated by said dissolvable electrode until the emulsion breaks.
Claim 2
Independent Claim 107 words
A method of breaking an oil-in-water emulsion which comprises: adjusting the pH of the oil-in-water emulsion to a pH in the range of 6 to 10; adding to the oil-in-water emulsion at least 1 part per million of a cation or a combination thereof selected from the group of cations consisting essentially of Fe+2, Fe+3, Al+3, Cu+1 and Cu+2; treating the oil-in-water emulsion with a dissolvable iron electrode, said dissolvable iron electrode being dissolved by transmitting an electric current therethrough in an amount sufficient to develop an Fe+2/oil weight ratio of at least 0.02; holding the oil-in-water emulsion treated by said dissolvable electrode until the emulsion breaks.
Claim 3
Dependent Claim 20 words
The method of claim 1 wherein: the pH is adjusted to a pH in the range from 6 to 8.
Claim 4
Dependent Claim 27 words
The method of claim 1 wherein: the cation added to the oil-in-water emulsion is in a range of 1 parts per million to 10 parts per million.
Claim 5
Dependent Claim 43 words
The method of claim 1 wherein: the cation added to the oil-in-water emulsion is in a range from 3 parts per million to 5 parts per million, and wherein: the pH is adjusted to a pH in the range from 6 to 8.
Claim 6
Dependent Claim 32 words
The method of claim 1 wherein: the oil-in-water emulsion is treated by said dissolvable metal electrode to develop an Fe+2/oil weight ratio of at least 0.02 but not in excess of 0.05.
Claim 7
Dependent Claim 63 words
The method of claim 5 wherein: the oil-in-water emulsion is treated by said dissolvable metal electrode to develop an Fe+2/oil weight ratio of about 0.035; wherein the cation added to the oil-in-water emulsion is in a range from 3 parts per million to 5 parts per million, and wherein: the pH is adjusted to a pH in the range from 6 to 8.

References Cited (Backward Citations)

US3892640A Cited
US3826725A Cited
US3959131A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-03-27 1981-09-26 1982-03-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-03-27 1985-09-26 1986-03-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-03-27 1989-09-26 1990-03-28 $7700.00 Window Closed / Lapsed

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