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US4080194A Expired / Lapsed US ⏱️ 0.0 years remaining

Titanium or zirconium reduction process by arc heater

Assignee: Westinghouse Electric Corp
•
Filing: 1976-11-26
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Granted: 1978-03-21
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Expires: 1996-11-26
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Abstract

Abstract A process for reducing a metal from a metal halide characterized by the steps of feeding into the arc heated stream of an arc heater a quantity of a reactant metal such as an alkali or alkaline-earth metal, feeding into the arc stream a quantity of a metal halide, which metal has a melting point higher than the boiling point of the co-product salt formed by reduction of the metal, the co-products being a liquid elemental metal and a gaseous salt, projecting the co-products into a reaction chamber tangentially to cause the liquid metal to separate centrifugally from the lighter, gaseous salt, and depositing the liquid metal in an associated receptacle.

Inventors

  • 👤 Maurice G. Fey

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 19:25
CPC Classifications
C; C22; C22B; C22B5/00; C22B5/02; C22B5/04; C22B34/00; C22B34/10; C22B34/12; C22B34/129; C22B34/14; Y; Y02; Y02P; Y02P10/00; Y02P10/10; Y02P10/122

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 240 words
A process for reducing a metal from a chloride salt comprising the steps of: a. providing an arc heater having at least a pair of axially spaced tubular electrodes forming an elongated arc chamber communicating with a reaction chamber, which arc chamber is coextensive with the spaced tubular electrodes, b. striking an electric arc in an axial gap between the electrodes, c. introducing a pressurized gas selected from the group consisting of argon, helium hydrogen, and carbon monoxide, radially inwardly through the gap and into the arc chamber to blow the electric arc from the gap and into the interior of the elongated arc chamber to form an elongated arc jet stream comprising the pressurized gas and projecting from the arc chamber into the reaction chamber, d. feeding into the arc jet stream a quantity of one element selected from the group consisting of an alkali metal and an alkaline-earth metal, e. feeding into the arc jet stream a quantity of a chloride of a metal having a melting point higher than the boiling point of the co-product salt formed with the metal, the co-products being a liquid elemental metal and a gaseous salt, f. projecting the reaction products into the reaction chamber tangentially to cause the liquid elemental metal to separate centrifugally from the lighter, gaseous salt, and g. depositing the liquid elemental metal on a downwardly extending surface to permit the metal to flow into an associated receptacle.
Claim 2
Dependent Claim 240 words
A process for reducing a metal from a chloride salt comprising the steps of: a. providing an arc heater having at least a pair of axially spaced tubular electrodes forming an elongated arc chamber communicating with a reaction chamber, which arc chamber is coextensive with the spaced tubular electrodes, b. striking an electric arc in an axial gap between the electrodes, c. introducing a pressurized gas selected from the group consisting of argon, helium hydrogen, and carbon monoxide, radially inwardly through the gap and into the arc chamber to blow the electric arc from the gap and into the interior of the elongated arc chamber to form an elongated arc jet stream comprising the pressurized gas and projecting from the arc chamber into the reaction chamber, d. feeding into the arc jet stream a quantity of one element selected from the group consisting of an alkali metal and an alkaline-earth metal, e. feeding into the arc jet stream a quantity of a chloride of a metal having a melting point higher than the boiling point of the co-product salt formed with the metal, the co-products being a liquid elemental metal and a gaseous salt, f. projecting the reaction products into the reaction chamber tangentially to cause the liquid elemental metal to separate centrifugally from the lighter, gaseous salt, and g. depositing the liquid elemental metal on a downwardly extending surface to permit the metal to flow into an associated receptacle.
Claim 3
Dependent Claim 20 words
The process of claim 1 in which three arc heaters are provided in peripherally spaced positions around the reaction chamber.
Claim 4
Dependent Claim 12 words
The process of claim 1 in which said one element is sodium.
Claim 5
Dependent Claim 12 words
The process of claim 1 in which said one element is magnesium.
Claim 6
Dependent Claim 20 words
The process of claim 1 in which titanium tetrachloride is fed in step (e) and liquid titanium is a co-product.
Claim 7
Dependent Claim 20 words
The process of claim 1 in which zirconium dichoride is fed in step (e) and liquid zirconium is a co-product.
Claim 8
Dependent Claim 14 words
The process of claim 1 in which the maximum operating temperature is 3500° K.
Claim 9
Dependent Claim 18 words
The process of claim 7 in which magnesium and titanium tetrachloride are fed in steps (d) and (e).
Claim 10
Dependent Claim 18 words
The process of claim 7 in which magnesium and zirconium tetrachloride are fed in steps (d) and (e).

References Cited (Backward Citations)

US2816828A Cited
US3825415A Cited
US3893845A Cited
US3843351A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-03-20 1981-09-19 1982-03-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-03-20 1985-09-19 1986-03-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-03-20 1989-09-19 1990-03-21 $7700.00 Window Closed / Lapsed

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