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US4078003A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for the preparation of 1,3-diamino-2,2-dimethyl propane

Assignee: Hoechst AG
•
Filing: 1976-09-14
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Granted: 1978-03-07
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Expires: 1996-09-14
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Abstract

Abstract A method for preparing neopentane diamine is disclosed comprising reacting neopentane glycol with ammonia in the presence of hydrogen and a nickel containing catalyst at elevated temperatures and pressures. Neopentane diamine is useful as an intermediate in the preparation of polyurethanes.

Inventors

  • 👤 Hans Feichtinger
  • 👤 Heinz Aschmann
  • 👤 Hans-Walter Birnkraut
  • 👤 Ludwig Brinkmann
  • 👤 Werner Pluta

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 21:32
CPC Classifications
C; C07; C07C; C07C211/00; C07C211/01; C07C211/02; C07C211/09; C07C211/11; C07C209/00; C07C209/04; C07C209/14; C07C209/16

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 72 words
A process for the production of 1,3 diamino-2,2 dimethyl propane comprising contacting neopentyl glycol, ammonia and hydrogen at a temperature of 150° - 300° C. and a pressure of at least 10 atmospheres in the presence of a nickel catalyst on a carrier, said catalyst containing 23 to 60% by weight of nickel and 16 to 40% by weight of chromium, and the hydroxyl group to ammonia ratio is 1:6 to 1:20.
Claim 2
Dependent Claim 72 words
A process for the production of 1,3 diamino-2,2 dimethyl propane comprising contacting neopentyl glycol, ammonia and hydrogen at a temperature of 150° - 300° C. and a pressure of at least 10 atmospheres in the presence of a nickel catalyst on a carrier, said catalyst containing 23 to 60% by weight of nickel and 16 to 40% by weight of chromium, and the hydroxyl group to ammonia ratio is 1:6 to 1:20.
Claim 3
Dependent Claim 14 words
The process according to claim 1 wherein said temperature is 240° to 260° C.
Claim 4
Dependent Claim 19 words
The process according to claim 1 wherein the chromium is in the form of Cr 2 O 3 .

References Cited (Backward Citations)

US2408171A Cited
US3270059A Cited
US3268588A Cited
US3347926A Cited
US3390184A Cited
US3520933A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-03-06 1981-09-05 1982-03-07 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-03-06 1985-09-05 1986-03-07 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-03-06 1989-09-05 1990-03-07 $7700.00 Window Closed / Lapsed

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