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US4075083A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for destructive distillation of hydrocarbonaceous materials

Assignee: Individual
•
Filing: 1976-06-11
•
Granted: 1978-02-21
•
Expires: 1996-06-11
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Abstract

Abstract A method of retorting oil shale which comprises the steps of passing the material in particulate form downwardly as a continuous vertical column of solid material successively through a preheating zone, a distillation zone, a combustion zone, and a residue cooling zone. An improved method of product oil recovery is disclosed whereby the vapor product is subjected to sequential treatment with cyclone separators and an absorption column, with a portion of the resulting noncondensible gases being recycled to the retort.

Inventors

  • 👤 Maurice W. Putman

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 23:20
CPC Classifications
C; C10; C10G; C10G1/00; C10G1/02

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 218 words
An improved method for recovering useful liquid products from distillation and combustion products produced by destructive distillation of oil shale and other particulate hydrocarbonaceous material within a gas combustion type of retort and recycling the product gases for use in the retort, the improvement comprising the steps of: a. removing the distillation and combustion products from the retort at a temperature in the range of 110° F to 200° F in the form of a stream containing oil mist, condensible oil vapors, combustible and noncombustible gases; b. recovering oil droplets from the oil mist containing stream by passing the stream removed in step a through at least one high velocity cyclone separator; c. removing condensible hydrocarbons from the stream from which the oil droplets were removed in step b by passage thereof through an absorption column countercurrent to the flow of an absorption oil therethrough; d. recovering the condensible hydrocarbons from said absorption oil by passage thereof through a desorber; e. adding a measured amount of air to a portion of the stream from which the condensible hydrocarbons were removed in step c; and f. directing the stream to which air was added in step e to one end of the retort for flow therethrough countercurrent to the flow of the oil shale and other particulate hydrocarbonaceous materials.
Claim 2
Dependent Claim 218 words
An improved method for recovering useful liquid products from distillation and combustion products produced by destructive distillation of oil shale and other particulate hydrocarbonaceous material within a gas combustion type of retort and recycling the product gases for use in the retort, the improvement comprising the steps of: a. removing the distillation and combustion products from the retort at a temperature in the range of 110° F to 200° F in the form of a stream containing oil mist, condensible oil vapors, combustible and noncombustible gases; b. recovering oil droplets from the oil mist containing stream by passing the stream removed in step a through at least one high velocity cyclone separator; c. removing condensible hydrocarbons from the stream from which the oil droplets were removed in step b by passage thereof through an absorption column countercurrent to the flow of an absorption oil therethrough; d. recovering the condensible hydrocarbons from said absorption oil by passage thereof through a desorber; e. adding a measured amount of air to a portion of the stream from which the condensible hydrocarbons were removed in step c; and f. directing the stream to which air was added in step e to one end of the retort for flow therethrough countercurrent to the flow of the oil shale and other particulate hydrocarbonaceous materials.
Claim 3
Dependent Claim 32 words
The method of claim 1 wherein said stream emerging from said absorption column of step c contains a maximum of one gallon of normally liquid hydrocarbons per 20,000 SCF of said stream.
Claim 4
Dependent Claim 32 words
The method of claim 1 wherein said stream emerging from said absorption column of step c contains a maximum of one gallon of normally liquid hydrocarbons per 40,000 SCF of said stream.
Claim 5
Dependent Claim 26 words
The method of claim 1 wherein said stream is removed from the retort in step a at a temperature ranging from 110° F to 130° F.
Claim 6
Dependent Claim 23 words
The method of claim 1 including the further step of recycling the absorption oil from said desorber for reuse in said absorption column.
Claim 7
Dependent Claim 23 words
The method of claim 1 including the further step of recovering the condensible hydrocarbons from said desorber by passage thereof through a condenser.

References Cited (Backward Citations)

US2813823A Cited
US3318798A Cited
US3526586A Cited
US3551322A Cited
US3736247A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-02-20 1981-08-22 1982-02-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-02-20 1985-08-22 1986-02-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-02-20 1989-08-22 1990-02-21 $7700.00 Window Closed / Lapsed

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