US4069103A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for recovering dextrose and dextrins from protein-containing starch products
Assignee: Chemap AG
•
Filing: 1976-04-20
•
Granted: 1978-01-17
•
Expires: 1996-04-20
Abstract
Abstract Dextrose and dextrins are obtained from protein-containing starch products by subjecting the starch product to an incomplete or complete acid or enzymatic hydrolysis or a combination of both types of hydrolysis and then circulating the hydrolysate containing a low viscosity sugar solution and water-soluble high molecular proteins through an ultrafilter to separate the proteins from the sugar solution whereupon the dextrose or, in case of incomplete hydrolysis, the dextrins are recovered from the filtrate obtained in the ultrafilter.
Inventors
- 👤 Hans Muller
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-26 16:09
CPC Classifications
C; C08; C08B; C08B30/00; C08B30/12; C08B30/18; C13; C13K; C13K1/00; C13K1/06
Claims Analysis
Total Claims: 13
Claim 1
Independent Claim
115 words
A process for obtaining dextrose and dextrins from a protein-containing starch product comprising subjecting the starch product to an incomplete or complete acid or enzymatic hydrolysis or a combination of both types of hydrolysis, then circulating the hydrolyzate containing a low viscosity sugar solution and water soluble high molecular proteins through an ultrafilter to separate the proteins from the sugar solution. and separately recovering the high molecular soluble protein from the filtrate of the ultrafiltration followed by subjecting it to spray-drying to obtain a high protein product useful as human food or animal feed, while recovering the dextrose or, in case of incomplete hydrolysis, the dextrins from the sugar solution obtained as the filter residue.
Claim 2
Dependent Claim
115 words
A process for obtaining dextrose and dextrins from a protein-containing starch product comprising subjecting the starch product to an incomplete or complete acid or enzymatic hydrolysis or a combination of both types of hydrolysis, then circulating the hydrolyzate containing a low viscosity sugar solution and water soluble high molecular proteins through an ultrafilter to separate the proteins from the sugar solution. and separately recovering the high molecular soluble protein from the filtrate of the ultrafiltration followed by subjecting it to spray-drying to obtain a high protein product useful as human food or animal feed, while recovering the dextrose or, in case of incomplete hydrolysis, the dextrins from the sugar solution obtained as the filter residue.
Claim 3
Dependent Claim
44 words
The process of claim 1 wherein the mass while circulating in the ultrafilter is subjected to a waterwash for so long as to cause the protein concentrate formed in the spray drying to have at least 70 to 80% solid contents of dry protein.
Claim 4
Dependent Claim
21 words
The process of claim 1 wherein the initial starch product is subjected to a wet grinding step prior to said hydrolysis.
Claim 5
Dependent Claim
35 words
The process of claim 1 wherein the ultrafiltration is effected at a pH of 3 to 9 for a time of 15-20 hours at a temperature of 20°-50° C and a pressure of 2-6 bar.
Claim 6
Dependent Claim
35 words
The process of claim 1 which includes the step of removing any husks and fat that may have been present from the initial starch product in the hydrolyzate by mechanical separation prior to said ultrafiltration.
Claim 7
Dependent Claim
48 words
The process of claim 1 wherein the sugar solution obtained as the filtrate from the ultrafiltration is subjected to a second hydrolysis in the form of an enzymatic hydrolysis followed by said recovery of the dextrose or dextrins which step may further be followed by conversion to isomerose.
Claim 8
Dependent Claim
14 words
The process of claim 1 wherein the starch product is a cereal or legume.
Claim 9
Dependent Claim
23 words
The process of claim 7 wherein the starch product is constituted by potatoes, arrowroot, manioc (cassava), maize, sorghum, wheat, rice, rye or barley.
Claim 10
Dependent Claim
42 words
The process of claim 1 which includes the step of separating out the insoluble residue including the water-insoluble proteins resulting from the hydrolysis by centrifuging or filtering the hydrolyzate prior to said ultrafiltration which insoluble proteins may be recovered for feed purposes.
Claim 11
Dependent Claim
85 words
The process of claim 9 wherein the insoluble residue separated out from the hydrolyzate is subjected to an alkaline treatment to further dissolve any residual water-insoluble proteins out of any husks resulting from the initial starch product, followed by separating the formed suspension into a protein-free residue and a protein containing solution, reuniting the protein containing solution with the said hydrolyzate and subjecting it after a neutralizing step to another hydrolysis in form of an enzymatic hydrolysis prior to passing the hydrolyzate through the ultrafilter.
Claim 12
Dependent Claim
40 words
The process of claim 9 wherein after the insoluble proteins are removed from said hydrolyzate by filtration and alkali treatment the remaining low viscosity solution is then subjected to a second hydrolysis prior to being passed through the ultrafiltration step.
Claim 13
Dependent Claim
17 words
The process of claim 1 wherein the two hydrolysis steps are in the form of enzymatic hydrolyses.
References Cited (Backward Citations)
US2307725A
Cited
US2410264A
Cited
US2571541A
Cited
US2583684A
Cited
US2698825A
Cited
US2797176A
Cited
US3228876A
Cited
US3305395A
Cited
US3276908A
Cited
US3342729A
Cited
US3383245A
Cited
US3720583A
Cited
US3668007A
Cited
US3756853A
Cited
US3788945A
Cited
US3958015A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1981-01-16 | 1981-07-18 | 1982-01-17 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1985-01-16 | 1985-07-18 | 1986-01-17 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1989-01-16 | 1989-07-18 | 1990-01-17 | $7700.00 | Window Closed / Lapsed |