Abstract A microscopic length scale typically about 50 μm long and graduated in veral intervals ranging from 1 μm to 20 μm. The scale is useful in calibrating the magnification of scanning electron microscopes (SEMs) and other electron imaging instruments. The scale comprises alternating layers of two metals deposited on a substrate. The two metals have substantially different electron emission coefficients to provide contrasting emission signals when scanned by an electron beam. One of the metals, preferably gold, is deposited in uniform layers about 40-80 nm thick. The other metal, preferably nickel, is deposited in several layers ranging from 1 μm or so thick near the substrate to 20 μm thick in the outermost layer. The resultant multilayer composite is cut into one or more samples and each sample is mounted on edge. The exposed edge is ground and metallographically polished and a microscopic indentation is made in the substrate near the first gold layer. The indentation defines a reference region, and the distances between the first gold layer and the subsequent gold layers in the reference region are measured. The measurement is made using a similar sample which was previously calibrated with the aid of a polarizing laser interferometer.
A scanning electron microscope micrometer scale comprising: a substantially nonmagnetic, corrosion resistant substrate; a microscopically thin multilayer composite deposited on the substrate, said composite formed of a plurality of straight parallel layers of one substantially nonmagnetic, corrosion resistant metal interleaved with a plurality of straight parallel layers of another substantially nonmagnetic corrosion resistant metal, said two metals being of substantially different electron emission coefficients; the layers of the one of said two metals having a uniform thickness of about 40-80 nm; the layers of the other of said two metals having thicknesses ranging from about 1 μm near said substrate to many μm away from said substrate; a cross sectional edge of said composite being ground and metallographically polished; and a microscopic indentation placed in said substrate adjacent said deposited layers to define a reference region.
Claim 2
Dependent Claim
136 words
A scanning electron microscope micrometer scale comprising: a substantially nonmagnetic, corrosion resistant substrate; a microscopically thin multilayer composite deposited on the substrate, said composite formed of a plurality of straight parallel layers of one substantially nonmagnetic, corrosion resistant metal interleaved with a plurality of straight parallel layers of another substantially nonmagnetic corrosion resistant metal, said two metals being of substantially different electron emission coefficients; the layers of the one of said two metals having a uniform thickness of about 40-80 nm; the layers of the other of said two metals having thicknesses ranging from about 1 μm near said substrate to many μm away from said substrate; a cross sectional edge of said composite being ground and metallographically polished; and a microscopic indentation placed in said substrate adjacent said deposited layers to define a reference region.
Claim 3
Dependent Claim
17 words
A scale as set forth in claim 1, wherein said one of said two metals is gold.
Claim 4
Dependent Claim
17 words
A scale as set forth in claim 1, wherein said other of said two metals is nickel.
Claim 5
Dependent Claim
15 words
A scale as set forth in claim 1, wherein said substrate is a nickel-copper alloy.
Claim 6
Dependent Claim
22 words
A scale as set forth in claim 1 wherein the number of layers of the one of said two metals is seven.