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US4066449A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for processing and densifying metal powder

Assignee: Individual
•
Filing: 1975-08-06
•
Granted: 1978-01-03
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Expires: 1995-08-06
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Abstract

Abstract A method of producing a densified compact from a loose metal powder, the method comprising introducing strain into each particle of the loose metal powder to impart a residual stress to increase the potential energy level of the particles above the potential energy which the particles may have acquired during production thereof, the strain being introduced at a temperature below the recrystallization temperature thereof, and thereafter hot consolidating the loose metal powder.

Inventors

  • 👤 Charles J. Havel

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 09:52
CPC Classifications
B; B22; B22F; B22F9/00; B22F9/02; B22F9/04

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 176 words
A method for producing a substantially fully dense compact from prealloyed powder metal comprising the steps of a. providing a fully alloyed powder of predetermined composition, b. cold working the particles of the prealloyed powder metal to introduce an amount of strain equivalent to at least about a forty percent reduction in size along a major axis of the particle to thereby lower the recrystallization temperature of the powder metal, said cold working being carried out at an energy level less than that which will cause extensive brittle fracture of the particles to maintain the integrity of the particles, c. maintaining the powder metal at a temperature below the lowered recrystallization temperature until the powder is to be consolidated and thereafter d. hot consolidating the powder metal by heating the powder metal to a temperature at least slightly above the lowered recrystallization temperature to recrystallize the powder metal, but below that at which excessive grain growth occurs to maintain a relatively small grain size in the compact and by applying pressure to the heated powder metal.
Claim 2
Independent Claim 176 words
A method for producing a substantially fully dense compact from prealloyed powder metal comprising the steps of a. providing a fully alloyed powder of predetermined composition, b. cold working the particles of the prealloyed powder metal to introduce an amount of strain equivalent to at least about a forty percent reduction in size along a major axis of the particle to thereby lower the recrystallization temperature of the powder metal, said cold working being carried out at an energy level less than that which will cause extensive brittle fracture of the particles to maintain the integrity of the particles, c. maintaining the powder metal at a temperature below the lowered recrystallization temperature until the powder is to be consolidated and thereafter d. hot consolidating the powder metal by heating the powder metal to a temperature at least slightly above the lowered recrystallization temperature to recrystallize the powder metal, but below that at which excessive grain growth occurs to maintain a relatively small grain size in the compact and by applying pressure to the heated powder metal.
Claim 3
Dependent Claim 26 words
A method as set forth in claim 1 wherein hot consolidating is carried out at a temperature at least as high as the lowered recrystallization temperature.
Claim 4
Dependent Claim 23 words
A method as set forth in claim 1 including subsequently heat treating said powder metal compact at temperatures sufficient to cause grain growth.
Claim 5
Dependent Claim 30 words
A method as set forth in claim 3 wherein said metal powder is composed of a metal selected from a group consisting of a nickel-base superalloy and a cobalt-base superalloy.
Claim 6
Dependent Claim 24 words
A method as set forth in claim 1 wherein said cold working includes deforming said particles by compressing the same between force transmitting members.
Claim 7
Dependent Claim 62 words
A method as set forth in claim 1 wherein hot consolidating is accomplished by encapsulating said metal powder in a vitreous container, heating said container and encapsulated powder to a temperature above said lowered recrystallization temperature, densifying said metal powder by applying external pressure to said container to collapse the same, and removing said collapsed container from the resultant densified metal compact.
Claim 8
Independent Claim 219 words
A method for producing a substantially fully dense compact from prealloyed powder metal by hot consolidation wherein the powder metal and resulting compact exhibit a marked increase in hot formability comprising the steps of a. providing a fully alloyed powder of predetermined composition, b. cold working the particles of the prealloyed powder metal to introduce an amount of strain equivalent to at least about a forty percent reduction in size along a major axis of the particle to thereby lower the recrystallization temperature of the powder metal, said cold working being carried out at an energy level less than that which will cause extensive brittle fracture of the particles to maintain the integrity of the particles, c. maintaining the powder metal at a temperature below the lowered recrystallization temperature until the powder is to be consolidated and thereafter d. hot consolidating the powder metal by heating the powder metal to a temperature at least slightly above the lowered recrystallization temperature to recrystallize the powder metal, but below that at which excessive grain growth occurs to maintain a relatively small grain size in the compact and by applying pressure to the heated powder metal thereby producing a condition of high hot formability in the powder particles during consolidation which is preserved in the resulting compact to facilitate subsequent hot forming.
Claim 9
Independent Claim 219 words
A method for producing a substantially fully dense compact from prealloyed powder metal by hot consolidation wherein the powder metal and resulting compact exhibit a marked increase in hot formability comprising the steps of a. providing a fully alloyed powder of predetermined composition, b. cold working the particles of the prealloyed powder metal to introduce an amount of strain equivalent to at least about a forty percent reduction in size along a major axis of the particle to thereby lower the recrystallization temperature of the powder metal, said cold working being carried out at an energy level less than that which will cause extensive brittle fracture of the particles to maintain the integrity of the particles, c. maintaining the powder metal at a temperature below the lowered recrystallization temperature until the powder is to be consolidated and thereafter d. hot consolidating the powder metal by heating the powder metal to a temperature at least slightly above the lowered recrystallization temperature to recrystallize the powder metal, but below that at which excessive grain growth occurs to maintain a relatively small grain size in the compact and by applying pressure to the heated powder metal thereby producing a condition of high hot formability in the powder particles during consolidation which is preserved in the resulting compact to facilitate subsequent hot forming.
Claim 10
Independent Claim 218 words
A method for producing a substantially fully dense compact from prealloyed powder metal by hot consolidation wherein the powder metal and resulting compact exhibit a marked increase in hot formability comprising the steps of a. providing a fully alloyed powder of predetermined composition, b. cold working the particles of the prealloyed powder metal to introduce an amount of strain equivalent to at least about a forty percent reduction in size along a major axis of the particles to thereby lower the recrystallization temperature of the powder metal, said cold working being carried out at an energy level less than that which will cause a reduction in the size of a significant number of individual particles, c. maintaining the powder metal at a temperature below the lowered recrystallization temperature until the powder is to be consolidated and thereafter d. hot consolidating the powder metal by heating the powder metal to a temperature at least slightly above the lowered recrystallization temperature to recrystallize the powder metal, but below that at which excessive grain growth occurs to maintain a relatively small grain size in the compact and by applying pressure to the heated powder metal thereby producing a condition of high hot formability in the powder particles during consolidation which is preserved in the resulting compact to facilitate subsequent hot forming.
Claim 11
Independent Claim 218 words
A method for producing a substantially fully dense compact from prealloyed powder metal by hot consolidation wherein the powder metal and resulting compact exhibit a marked increase in hot formability comprising the steps of a. providing a fully alloyed powder of predetermined composition, b. cold working the particles of the prealloyed powder metal to introduce an amount of strain equivalent to at least about a forty percent reduction in size along a major axis of the particles to thereby lower the recrystallization temperature of the powder metal, said cold working being carried out at an energy level less than that which will cause a reduction in the size of a significant number of individual particles, c. maintaining the powder metal at a temperature below the lowered recrystallization temperature until the powder is to be consolidated and thereafter d. hot consolidating the powder metal by heating the powder metal to a temperature at least slightly above the lowered recrystallization temperature to recrystallize the powder metal, but below that at which excessive grain growth occurs to maintain a relatively small grain size in the compact and by applying pressure to the heated powder metal thereby producing a condition of high hot formability in the powder particles during consolidation which is preserved in the resulting compact to facilitate subsequent hot forming.

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-01-02 1981-07-04 1982-01-03 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-01-02 1985-07-04 1986-01-03 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-01-02 1989-07-04 1990-01-03 $7700.00 Window Closed / Lapsed

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