Method and apparatus for countercurrent washing of particulate solids

Claim 2

A continuous, countercurrent washing unit for washing particulate solids with a washing solution, comprising a washing tower having means defining a plurality of washing sections disposed one above the other, each washing section of the tower including means defining a restricted opening at its base, a recirculation loop interconnected at one end with an upper portion of each washing section, the other end of the loop terminating adjacent the restricted opening in the base of each section, and a pump and throttle valve means arranged in each recirculation loop for drawing washing solution from the upper portion of each section and recirculating it upwardly into the bottom of the respective section through the restricted opening at a regulated rate to control passage of solids through the restricted opening, the washing unit further comprising, means in communication with the uppermost washing section for introducing particulate solids to be washed, and means for introducing washing solution into the lowermost washing section, the tower also comprising means defining an outlet section arranged beneath the lowermost washing section for receiving washed particulate solids therefrom, said outlet section including means defining a restricted passage for regulating the flow of washing solution in the tower.

Claim 3

The washing tower of claim 1 further comprising means for introducing additional washing solution into the washing tower above the restricted passage in the outlet section in order to minimize the flow of washing solution through the restricted passage of the outlet section with the particulate solids.

Claim 4

The washing tower of claim 2 further comprising an overflow means in communication with the uppermost washing section above the interconnection for the one end of the respective recirculation conduit and a flow regulating means for regulating the rate at which the additional washing solution is introduced into the outlet section of the tower above the restricted passage, the flow regulating means being adjustable to maintain the height of the washing solution column in the washing tower relative to the overflow means.

Claim 5

The washing tower of claim 1 wherein the recirculation loop for the lowermost washing section includes means for introducing fresh washing solution into the lowermost section along with the recirculated washing solution.

Claim 6

The washing tower of claim 1 further comprising overflow means in communication with an upper portion of the uppermost washing section.

Claim 7

The washing tower of claim 1 wherein the base of each washing section is formed by a conically shaped floor, the restricted opening being formed by a central portion of the conical floor, the other end of the respective recirculation loop comprising a nozzle outlet means extending upwardly through the central floor opening for each washing section.

Claim 8

The washing tower of claim 6 further comprising spacer means for positioning the nozzle relative to the restricted opening in the base of the washing section, a cylindrical element forming an extension of the restricted opening for receiving the nozzle and spacer means.

Claim 9

The washing tower of claim 1 wherein the other end of each respective recirculation loop is in communication with a nozzle outlet means extending upwardly through the restricted opening of the respective washing section.

Claim 10

A continuous countercurrent washing unit for washing particulate solids with a washing solution, wherein the particulate solids are microspherical particles containing fissile and/or fertile material, the washing solution being selected to remove foreign material from the microspherical particles, comprising means defining a washing tower including a plurality of washing sections disposed one above the other, each washing section of the tower including a tapered floor forming a centrally arranged restricted opening at the base of the respective washing section, a recirculation loop interconneted at one end with an upper portion of the respective washing section, the other end of the loop being in communication with a nozzle means extending upwardly through the restricted opening in the base of the respective section, and a pump and throttle valve means arranged in each respective recirculation loop for drawing washing solution from the upper portion of the section and recirculating it into the base of the section through the nozzle means, the recirculation loop for the lowermost washing section including means for introducing fresh washing solution into the lowermost washing section, the washing unit further comprising, means in communication with the uppermost washing section for introducing particulate solids to be washed, an outlet section arranged beneath the lowermost washing section for receiving washed solids therefore, said outlet section including a restricted passage means for regulating the flow of washing solution in the tower, overflow means in communication with an upper portion of an uppermost washing section, and means for introducing additional washing solution into the outlet section of the tower above the restricted passage in order to minimize the flow of washing solution from the tower through the restricted passage.

Claim 11

A continuous countercurrent washing unit for washing particulate solids with a washing solution, wherein the particulate solids are microspherical particles containing fissile and/or fertile material, the washing solution being selected to remove foreign material from the microspherical particles, comprising means defining a washing tower including a plurality of washing sections disposed one above the other, each washing section of the tower including a tapered floor forming a centrally arranged restricted opening at the base of the respective washing section, a recirculation loop interconneted at one end with an upper portion of the respective washing section, the other end of the loop being in communication with a nozzle means extending upwardly through the restricted opening in the base of the respective section, and a pump and throttle valve means arranged in each respective recirculation loop for drawing washing solution from the upper portion of the section and recirculating it into the base of the section through the nozzle means, the recirculation loop for the lowermost washing section including means for introducing fresh washing solution into the lowermost washing section, the washing unit further comprising, means in communication with the uppermost washing section for introducing particulate solids to be washed, an outlet section arranged beneath the lowermost washing section for receiving washed solids therefore, said outlet section including a restricted passage means for regulating the flow of washing solution in the tower, overflow means in communication with an upper portion of an uppermost washing section, and means for introducing additional washing solution into the outlet section of the tower above the restricted passage in order to minimize the flow of washing solution from the tower through the restricted passage.

Claim 12

In a method of washing particulate solids to remove foreign material, the steps comprising, forming a washing tower with a plurality of washing sections arranged one above the other and an outlet section at the base of the tower, each washing section including a restricted opening at its lower end, introducing fresh washing solution into the washing tower beneath the restricted opening for the lowermost washing section, withdrawing washing solution from an upper portion of each washing section and recirculating said withdrawn washing solution for introduction through the restricted opening in the bottom of the respective washing section, regulating the rate of washing solution recirculation for each washing section in order to selectively adjust the dwell time for particulate solids in each respective washing section, and restricting passage of particulate solids from the outlet section of the wash tower in order to regulate the flow of washing solution in the tower.

Claim 13

In a method of washing particulate solids to remove foreign material, the steps comprising, forming a washing tower with a plurality of washing sections arranged one above the other and an outlet section at the base of the tower, each washing section including a restricted opening at its lower end, introducing fresh washing solution into the washing tower beneath the restricted opening for the lowermost washing section, withdrawing washing solution from an upper portion of each washing section and recirculating said withdrawn washing solution for introduction through the restricted opening in the bottom of the respective washing section, regulating the rate of washing solution recirculation for each washing section in order to selectively adjust the dwell time for particulate solids in each respective washing section, and restricting passage of particulate solids from the outlet section of the wash tower in order to regulate the flow of washing solution in the tower.

Claim 14

The method of claim 10 further comprising the step of introducing additional washing solution into the outlet section of the washing tower for minimizing passage of the washing solution from the washing tower to the outlet section.

Claim 15

The method of claim 11 further comprising the step of withdrawing spent washing solution from the uppermost washing section of the tower and regulating the rate at which the additional washing soluion is introduced into the outlet section of the washing tower to maintain a washing solution column in the tower.

Claim 16

The method of claim 10 further comprising the step of receiving particulate solids from the outlet section of the washing tower in a suitable transport fluid.

Claim 17

The method of claim 10 wherein the particulate solids are microspherical particles containing fissile and/or fertile material and further comprising the step of selecting the washing solution to effectively remove foreign material for the microspherical particles.