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US4051659A Expired / Lapsed US ⏱️ 0.0 years remaining

Production of carbon fibre

Assignee: Morganite Modmor Ltd
•
Filing: 1976-02-17
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Granted: 1977-10-04
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Expires: 1996-02-17
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Abstract

Abstract Production of carbon fibre from a multifilament tow of organic precursor fibre, by heat treatment in an oxygen containing atmosphere and subsequent carbonization optionally followed by graphitization, the tow being given a twist between the oxygen treatment and carbonization, which twist is made permanent by the carbonization and maintains the fibres within the tow during the carbonization and subsequent handling.

Inventors

  • 👤 Harold Dennis Blakelock

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 20:19
CPC Classifications
D; D01; D01F; D01F9/00; D01F9/08; D01F9/12; D01F9/14; D01F9/20; D01F9/21; D01F9/22; D01F9/32

Claims Analysis

Total Claims: 12
Claim 1
Independent Claim 64 words
In the production of carbon fibre from a multifilament tow of organic precursor fibre, by heat treatment in an oxygen containing atmosphere and subsequent carbonisation optionally followed by graphitisation, the improvement comprising giving the tow a twist between the oxygen treatment and carbonisation, which twist is made permanent by the carbonisation and maintains the fibres within the tow during the carbonisation and subsequent handling.
Claim 2
Dependent Claim 64 words
In the production of carbon fibre from a multifilament tow of organic precursor fibre, by heat treatment in an oxygen containing atmosphere and subsequent carbonisation optionally followed by graphitisation, the improvement comprising giving the tow a twist between the oxygen treatment and carbonisation, which twist is made permanent by the carbonisation and maintains the fibres within the tow during the carbonisation and subsequent handling.
Claim 3
Dependent Claim 116 words
In the production of carbon fibre according to claim 1, from a multifilament tow of 2,000 to 20,000, 0.5 to 5 denier filaments of organic precursor fibre, by heat treatment in an oxygen-containing atmosphere at 200 to 300° C for 1 to 3 hours under tension a least sufficient to prevent shrinkage of the fibre by more than 5%, subsequent carbonisation at 1000° to 2000° C, and optionally graphitisation at 2000° to 3000° C, the improvement wherein the tow is given a twist of 10 to 130 turns/meter between the oxygen treatment and the carbonisation, which twist is made permanent by the carbonisation and maintains the fibres within the tow during the carbonisation and subsequent handling.
Claim 4
Dependent Claim 16 words
Production of carbon fibres according to claim 2, wherein the twist is 50 to 120 turns/meter.
Claim 5
Dependent Claim 18 words
Production of carbon fibre according to claim 2, wherein the precursor is a polymer or copolymer of acrylonitrile.
Claim 6
Dependent Claim 17 words
Production of carbon fiber as claimed in claim 2 wherein the twist is 70 to 120 turns/meter.
Claim 7
Dependent Claim 22 words
A tow of carbon fibre, made by the method of claim 1, having a permanent twist maintaining the fibres within the tow.
Claim 8
Dependent Claim 27 words
A tow, according to claim 6, of 2,000 to 20,000 carbon fibres having a permanent twist of 10 to 130 turns/meter maintaining the fibre within the tow.
Claim 9
Dependent Claim 14 words
A tow according to claim 7, wherein the twist is 50 to 120, turns/meter.
Claim 10
Dependent Claim 15 words
A tow is claimed in claim 7 wherein the twist is 70 to 120 turns/meter.
Claim 11
Dependent Claim 15 words
Carbon fibre in woven or braided form, made from a tow according to claim 6.
Claim 12
Dependent Claim 28 words
Carbon fiber in the form of a continuous filament tow having a permanent twist maintaining the fibers within the tow, and made by the method of claim 1.

References Cited (Backward Citations)

US3412062A Cited
US3841079A Cited
US3702054A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-10-03 1981-04-04 1981-10-04 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-10-03 1985-04-04 1985-10-04 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-10-03 1989-04-04 1989-10-04 $7700.00 Window Closed / Lapsed

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