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US4051264A Expired / Lapsed US ⏱️ 0.0 years remaining

Cold water extractable tea leaf and process

Assignee: Lever Brothers Co
•
Filing: 1976-11-16
•
Granted: 1977-09-27
•
Expires: 1996-11-16
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Abstract

Abstract Cold water extractable tea leaf is prepared by treatment of fresh green tea with the enzyme tannase under anaerobic conditions. The cold water extractable tea leaf is also used to prepare an instant tea product.

Inventors

  • 👤 Gary Warner Sanderson
  • 👤 Andrew Charles Hoefler
  • 👤 Harold Nathaniel Graham
  • 👤 Philip Coggon

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 20:00
CPC Classifications
A; A23; A23F; A23F3/00; A23F3/16; A23F3/166; A23F3/06; A23F3/08; A23F3/10

Claims Analysis

Total Claims: 28
Claim 1
Independent Claim 86 words
A process for preparing black tea leaf from green tea leaf which comprises the steps of comminuting freshly harvested green tea leaf, treating the comminuted fresh green tea leaf with tannase at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, fermenting the treated green tea leaf, and firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5% and produce a cold water extractable fired black tea leaf.
Claim 2
Dependent Claim 86 words
A process for preparing black tea leaf from green tea leaf which comprises the steps of comminuting freshly harvested green tea leaf, treating the comminuted fresh green tea leaf with tannase at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, fermenting the treated green tea leaf, and firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5% and produce a cold water extractable fired black tea leaf.
Claim 3
Dependent Claim 67 words
In a process for preparing manufactured green tea leaf, the improvement comprising the steps of bringing comminuted green tea leaf into contact with tannase under essentially anaerobic conditions at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, and thereafter firing the tea leaf to reduce the moisture content of the tea leaf to below about 5%.
Claim 4
Dependent Claim 67 words
In a process for preparing manufactured green tea leaf, the improvement comprising the steps of bringing comminuted green tea leaf into contact with tannase under essentially anaerobic conditions at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, and thereafter firing the tea leaf to reduce the moisture content of the tea leaf to below about 5%.
Claim 5
Dependent Claim 87 words
A process for preparing manufactured green tea leaf which comprises the steps of heating freshly harvested green tea leaf at a temperature and for a time sufficient to inactivate tea leaf enzymes before fermentation has taken place, comminuting the tea leaf, treating the comminuted tea leaf with tannase at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, and firing the treated tea leaf to reduce the moisture content of the tea leaf to below about 5%.
Claim 6
Dependent Claim 87 words
A process for preparing manufactured green tea leaf which comprises the steps of heating freshly harvested green tea leaf at a temperature and for a time sufficient to inactivate tea leaf enzymes before fermentation has taken place, comminuting the tea leaf, treating the comminuted tea leaf with tannase at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, and firing the treated tea leaf to reduce the moisture content of the tea leaf to below about 5%.
Claim 7
Dependent Claim 130 words
A process for preparing black tea leaf from freshly harvested green tea leaf comprising the steps of preparing fresh green tea leaf for fermentation by comminution techniques, adding tannase to the comminuted tea leaf at a level of from about 2 to about 20 units per gram of tea leaf, while maintaining the temperature of the tea leaf within the range of about 25° C to about 45° C and maintaining essentially anaerobic conditions, maintaining the tea leaf in contact with tannase to provide a substantial increase in cold water extractable solids, fermenting the tannase contacted tea leaf under aerobic conditions, and firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5% and produce a cold water extractable fired black tea leaf.
Claim 8
Dependent Claim 130 words
A process for preparing black tea leaf from freshly harvested green tea leaf comprising the steps of preparing fresh green tea leaf for fermentation by comminution techniques, adding tannase to the comminuted tea leaf at a level of from about 2 to about 20 units per gram of tea leaf, while maintaining the temperature of the tea leaf within the range of about 25° C to about 45° C and maintaining essentially anaerobic conditions, maintaining the tea leaf in contact with tannase to provide a substantial increase in cold water extractable solids, fermenting the tannase contacted tea leaf under aerobic conditions, and firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5% and produce a cold water extractable fired black tea leaf.
Claim 9
Dependent Claim 15 words
The process of claim 4, wherein said anaerobic conditions are maintained up to 30 minutes.
Claim 10
Dependent Claim 24 words
The process of claim 4, wherein the tannase is added at a level of 8 enzyme units per gram of dry green tea leaf.
Claim 11
Dependent Claim 35 words
The process of claim 4, wherein potassium hydroxide is added to the comminuted green tea leaf prior to the step of tannase treatment to provide a pH within the range of about 4.5 to 7.5.
Claim 12
Dependent Claim 26 words
The process of claim 4, wherein sufficient alkali is added after the tannase treatment to adjust the pH to that of the original comminuted tea leaf.
Claim 13
Dependent Claim 112 words
A process for preparing black tea leaf from freshly harvested green tea leaf which comprises the steps of commimuting freshly harvested green tea leaf, adding the comminuted tea leaf to water to form a tea slurry, treating the tea slurry with tannase under essentially anaerobic conditions at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, fermenting the treated tea slurry, and drying the fermented tea slurry with a firing step at the terminus of the drying process, to reduce the moisture content of the tea leaf to below about 5% and to provide a cold water extractable fired black tea leaf.
Claim 14
Dependent Claim 112 words
A process for preparing black tea leaf from freshly harvested green tea leaf which comprises the steps of commimuting freshly harvested green tea leaf, adding the comminuted tea leaf to water to form a tea slurry, treating the tea slurry with tannase under essentially anaerobic conditions at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, fermenting the treated tea slurry, and drying the fermented tea slurry with a firing step at the terminus of the drying process, to reduce the moisture content of the tea leaf to below about 5% and to provide a cold water extractable fired black tea leaf.
Claim 15
Dependent Claim 152 words
A process for preparing black tea leaf from freshly harvested green tea leaf which comprises the steps of comminuting freshly harvested green tea leaf, adding the comminuted tea leaf to water to form a tea leaf slurry, maintaining the tea leaf slurry at a temperature from 25° C to 50° C for a time sufficient to provide a substantial amount of extracted tea solids, separating the tea leaf slurry into extract and tea leaf residue, treating the extract with tannase immobilized on a solid support, adding the extracted tea leaf residue back to the tannase-treated extract to form a second tea leaf slurry, fermenting the second tea leaf slurry, and drying the fermented second tea leaf slurry with a firing step at the terminus of the drying process, to reduce the moisture content of the tea leaf to below about 5% and to provide a cold water extractable fired back tea leaf.
Claim 16
Dependent Claim 152 words
A process for preparing black tea leaf from freshly harvested green tea leaf which comprises the steps of comminuting freshly harvested green tea leaf, adding the comminuted tea leaf to water to form a tea leaf slurry, maintaining the tea leaf slurry at a temperature from 25° C to 50° C for a time sufficient to provide a substantial amount of extracted tea solids, separating the tea leaf slurry into extract and tea leaf residue, treating the extract with tannase immobilized on a solid support, adding the extracted tea leaf residue back to the tannase-treated extract to form a second tea leaf slurry, fermenting the second tea leaf slurry, and drying the fermented second tea leaf slurry with a firing step at the terminus of the drying process, to reduce the moisture content of the tea leaf to below about 5% and to provide a cold water extractable fired back tea leaf.
Claim 17
Dependent Claim 92 words
A process for preparing an instant tea which comprises the steps of comminuting freshly harvested green tea leaf, treating the comminuted green tea leaf with tannase at a temperature and for a time sufficient to impart a substantial cold water extractability to the tea leaf, fermenting the treated green tea leaf, firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5%, preparing a hot water extract of the tea leaf, polishing the tea extract, and drying the extract to provide a powdered instant tea.
Claim 18
Dependent Claim 92 words
A process for preparing an instant tea which comprises the steps of comminuting freshly harvested green tea leaf, treating the comminuted green tea leaf with tannase at a temperature and for a time sufficient to impart a substantial cold water extractability to the tea leaf, fermenting the treated green tea leaf, firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5%, preparing a hot water extract of the tea leaf, polishing the tea extract, and drying the extract to provide a powdered instant tea.
Claim 19
Dependent Claim 134 words
A process for preparing an instant tea which comprises the steps of comminuting freshly harvested green tea leaf, adding tannase to the comminuted green tea leaf at a level of from about 2 to about 20 units per gram of the greem tea leaf, maintaining the tea leaf in contact with the tannase at a temperature within the range of about 25° C to about 45° C under essentially anaerobic conditions for a sufficient time to provide a substantial increase in extractable solids, fermenting the tannase contacted tea leaf under aerobic conditions, firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5%, preparing a hot water extract of the fired tea leaf, polishing the tea extract and drying the extract to provide a powdered instant tea.
Claim 20
Dependent Claim 134 words
A process for preparing an instant tea which comprises the steps of comminuting freshly harvested green tea leaf, adding tannase to the comminuted green tea leaf at a level of from about 2 to about 20 units per gram of the greem tea leaf, maintaining the tea leaf in contact with the tannase at a temperature within the range of about 25° C to about 45° C under essentially anaerobic conditions for a sufficient time to provide a substantial increase in extractable solids, fermenting the tannase contacted tea leaf under aerobic conditions, firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5%, preparing a hot water extract of the fired tea leaf, polishing the tea extract and drying the extract to provide a powdered instant tea.
Claim 21
Dependent Claim 81 words
In a process for preparing black tea leaf from comminuted fresh green tea leaf, the improvement comprising the steps of contacting the comminuted green tea leaf with tannase at a temperature and for a time sufficient to provide a substantial increase in cold water extractable solids, fermenting the tannase contacted tea leaf and firing the fermented tea leaf to reduce the moisture content of the tea leaf of below about 5% and produce a cold water extractable fired back tea leaf.
Claim 22
Dependent Claim 81 words
In a process for preparing black tea leaf from comminuted fresh green tea leaf, the improvement comprising the steps of contacting the comminuted green tea leaf with tannase at a temperature and for a time sufficient to provide a substantial increase in cold water extractable solids, fermenting the tannase contacted tea leaf and firing the fermented tea leaf to reduce the moisture content of the tea leaf of below about 5% and produce a cold water extractable fired back tea leaf.
Claim 23
Dependent Claim 80 words
A cold water extractable fired black tea leaf prepared by comminuting freshly harvested green tea leaf, treating the comminuted fresh green tea leaf with tannase at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, fermenting the treated green tea leaf and firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5% and produce a cold water extractable fired black tea leaf.
Claim 24
Dependent Claim 80 words
A cold water extractable fired black tea leaf prepared by comminuting freshly harvested green tea leaf, treating the comminuted fresh green tea leaf with tannase at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, fermenting the treated green tea leaf and firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5% and produce a cold water extractable fired black tea leaf.
Claim 25
Dependent Claim 96 words
A cold water extractable fired green tea leaf prepared by heating freshly harvested green tea leaf at a temperature and for a time sufficient to inactivate tea leaf enzymes before fermentation has taken place, comminuting the green tea leaf, treating the comminuted tea leaf with tannase at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, and firing the treated tea leaf to reduce the moisture content of the tea leaf to below about 5% and to produce a cold water extractable fired green tea leaf.
Claim 26
Dependent Claim 96 words
A cold water extractable fired green tea leaf prepared by heating freshly harvested green tea leaf at a temperature and for a time sufficient to inactivate tea leaf enzymes before fermentation has taken place, comminuting the green tea leaf, treating the comminuted tea leaf with tannase at a temperature and for a time sufficient to impart a substantial cold water extractability to the manufactured tea leaf, and firing the treated tea leaf to reduce the moisture content of the tea leaf to below about 5% and to produce a cold water extractable fired green tea leaf.
Claim 27
Dependent Claim 93 words
A process for preparing oolong tea leaf from green tea leaf which comprises the steps of comminuting freshly harvested green tea leaf, treating the comminuted fresh green tea leaf with tannase at a temperature and for a time sufficient to impart substantial cold water extractability to the manufactured tea leaf, fermenting the treated green tea leaf for a time sufficient to impart oolong character, and firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5% and produce a cold water extractable fired oolong tea leaf.
Claim 28
Dependent Claim 93 words
A process for preparing oolong tea leaf from green tea leaf which comprises the steps of comminuting freshly harvested green tea leaf, treating the comminuted fresh green tea leaf with tannase at a temperature and for a time sufficient to impart substantial cold water extractability to the manufactured tea leaf, fermenting the treated green tea leaf for a time sufficient to impart oolong character, and firing the fermented tea leaf to reduce the moisture content of the tea leaf to below about 5% and produce a cold water extractable fired oolong tea leaf.

References Cited (Backward Citations)

US2785979A Cited
US2975057A Cited
US3438785A Cited
GB1380135A Cited
US3812266A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-09-26 1981-03-28 1981-09-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-09-26 1985-03-28 1985-09-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-09-26 1989-03-28 1989-09-27 $7700.00 Window Closed / Lapsed

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