US4045589A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Fat emulsion product and process for producing the same
Assignee: Nestec SA
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Filing: 1976-06-21
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Granted: 1977-08-30
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Expires: 1996-06-21
Abstract
Abstract A stable, dry, non-dairy fat emulsion product suitable for use as a coffee whitener is prepared without the use of protein by incorporating a chemically modified dextrinized starch having a lipophilic character in the formulation. The chemically modified starch is included in an aqueous emulsion containing fat or oil and a conventional emulsifier to stabilize the emulsion through the drying step so that upon reconstitution in coffee a stable emulsion is formed. The pH of the liquid emulsion must be controlled in order for the chemically modified starch to be effective in stabilizing the emulsion through the drying step. A buffering agent is mixed with the dried emulsion to improve the taste of coffee whitened with the dried emulsion.
Inventors
- 👤 Gary E. Petrowski
- 👤 John M. Wolcott
- 👤 Erlinda P. Ortiz
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 09:18
CPC Classifications
A; A23; A23C; A23C11/00; A23C11/02; A23C11/10
Claims Analysis
Total Claims: 20
Claim 1
Independent Claim
104 words
A dry, protein-free coffee whitener which comprises a dried emulsion concentrate containing from 0%-55% by weight of a water soluble carbohydrate, from 0.2%-1.25% of an emulsifier, and from 20%-50% by weight of an edible fat having an average particle size of about 1-3 microns in diameter, said fat being stabilized with a chemically modified dextrinized starch derivative having a lipophilic character in an amount sufficient to provide the product with a starch derivative to fat ratio of between about 0.4-1.25 to 1, and a buffering salt in an amount sufficient to provide the product with a pH in the range of 6-7 when reconstituted.
Claim 2
Dependent Claim
104 words
A dry, protein-free coffee whitener which comprises a dried emulsion concentrate containing from 0%-55% by weight of a water soluble carbohydrate, from 0.2%-1.25% of an emulsifier, and from 20%-50% by weight of an edible fat having an average particle size of about 1-3 microns in diameter, said fat being stabilized with a chemically modified dextrinized starch derivative having a lipophilic character in an amount sufficient to provide the product with a starch derivative to fat ratio of between about 0.4-1.25 to 1, and a buffering salt in an amount sufficient to provide the product with a pH in the range of 6-7 when reconstituted.
Claim 3
Dependent Claim
25 words
The coffee whitener defined in claim 1 in which the chemically modified starch is a dextrinized starch acid-ester of a substituted cyclic dicarboxylic acid anhydride.
Claim 4
Dependent Claim
43 words
The coffee whitener defined in claim 1 in which the whitener contains from 1% to 3% by weight of a buffering agent selected from the group consisting of phosphate and citrate salts and mixtures thereof which have a pH of from about 6-8.
Claim 5
Dependent Claim
113 words
The coffee whitener defined in claim 1 in which the whitener comprises a dried emulsion concentrate containing from 20%-35% by weight of an edible fat having a melting point of about 110° F.-115° F., no more than about 1.25% by weight of an emulsifier, and from 10%-35% by weight of a carbohydrate, said fat being stabilized with a dextrinized waxy maize acid-ester of a substituted succinic acid derived from octenyl succinic acid anhydride in an amount sufficient to provide a ratio of starch derivative to fat of 0.6-0.8 to 1, and a buffering salt comprising from 2.0-2.5% by weight of a mixture of mono- and dipotassium phosphate salts having a pH of 6-8.
Claim 6
Dependent Claim
20 words
The coffee whitener defined in claim 1 in which the chemically modified starch derivative has a pH of about 2.5-3.0.
Claim 7
Dependent Claim
23 words
The coffee whitener defined in claim 1 in which the buffering salt is selected from the group consisting of phosphate and citrate salts.
Claim 8
Dependent Claim
30 words
The coffee whitener defined in claim 1 in which the chemically modified starch is a dextrinized waxy maize acid-ester of a substituted succinic acid derived from octenyl succinic acid anhydride.
Claim 9
Dependent Claim
22 words
The coffee whitener defined in claim 1 in which the dried emulsion concentrate has a pH of no more than about 4.0.
Claim 10
Dependent Claim
19 words
The coffee whitener defined in claim 8 in which the dried emulsion concentrate has a pH of from 3.5-4.0.
Claim 11
Independent Claim
118 words
A method of preparing a stable, dry, protein-free coffee whitener which comprises forming a liquid emulsion concentrate containing an edible fat having an average particle size of about 1-3 microns in diameter, an emulsifier, water and a chemically modified dextrinized starch having a lipophilic character, the emulsion concentrate containing sufficient fat to provide said concentrate, when dried, with a fat content of from 20%-50% by weight, and having a pH of no more than about 4.0 and a starch derivative to fat ratio of between about 0.4-1.25 to 1 drying the liquid emulsion concentrate, and admixing the dried emulsion concentrate with at least one buffering salt to provide the whitener with a pH of about 6-7, when reconstituted.
Claim 12
Independent Claim
118 words
A method of preparing a stable, dry, protein-free coffee whitener which comprises forming a liquid emulsion concentrate containing an edible fat having an average particle size of about 1-3 microns in diameter, an emulsifier, water and a chemically modified dextrinized starch having a lipophilic character, the emulsion concentrate containing sufficient fat to provide said concentrate, when dried, with a fat content of from 20%-50% by weight, and having a pH of no more than about 4.0 and a starch derivative to fat ratio of between about 0.4-1.25 to 1 drying the liquid emulsion concentrate, and admixing the dried emulsion concentrate with at least one buffering salt to provide the whitener with a pH of about 6-7, when reconstituted.
Claim 13
Dependent Claim
81 words
The method defined in claim 10 in which a fat phase containing fat and emulsifier and having a temperature of about 130° F.-140° F., and an aqueous phase containing the chemically modified starch derivative and having a temperature of about 150°-200° F. are combined and homogenized to provide a stable emulsion concentrate having a pH of no more than 4.0 in which the fat particles have an average diameter of about 1-3 microns, and the liquid emulsion concentrate is spray dried.
Claim 14
Dependent Claim
34 words
The method defined in claim 10 in which the dried emulsion concentrate is dry blended with from 2.0%-2.5% by weight of a mixture of mono- and dipotassium phosphate salts having a pH of 6-8.
Claim 15
Dependent Claim
24 words
The method defined in claim 10 in which the chemically modified starch is a dextrinized starch acid-ester of a substituted cyclic dicarboxylic acid anhydride.
Claim 16
Dependent Claim
52 words
The method defined in claim 13 in which the chemically modified starch is a dextrinized waxy maize acid-ester of a substituted succinic acid derived from octenyl succinic anhydride and is present in an amount sufficient to provide the liquid emulsion concentrate with a starch derivative to fat ratio of 0.6-0.8 to 1.
Claim 17
Dependent Claim
36 words
The method defined in claim 10 in which the liquid emulsion concentrate contains a water soluble carbohydrate in an amount sufficient to provide the concentrate, when dried, with a carbohydrate content of from 10%-35% by weight.
Claim 18
Dependent Claim
34 words
The method defined in claim 10 in which the dried emulsion concentrate is dry blended with from 1%-3% by weight of a buffering salt selected from the group consisting of phosphate and citrate salts.
Claim 19
Dependent Claim
26 words
The method defined in claim 10 in which the dried emulsion concentrate has a pH of between about 3.5-4.0 prior to admixing with the buffering salt.
Claim 20
Dependent Claim
15 words
The method defined in claim 10 in which the liquid emulsion concentrate is spray dried.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-08-29 | 1981-02-28 | 1981-08-30 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-08-29 | 1985-02-28 | 1985-08-30 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-08-29 | 1989-02-28 | 1989-08-30 | $7700.00 | Window Closed / Lapsed |