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US4040972A Expired / Lapsed US ⏱️ 0.0 years remaining

Ion-exchanging aluminum silicate with hydrophilic surfaces

Assignee: Henkel AG and Co KGaA
•
Filing: 1976-03-05
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Granted: 1977-08-09
•
Expires: 1996-03-05
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Abstract

Abstract There are provided alkali aluminum silicates having a hydrophilic surface. They are prepared by mixing a crystalline, ion-exchanging alkali aluminum silicate with a hydrophilic material, preferably ortho-phosphoric acid or an alkali ortho phosphate.

Inventors

  • 👤 Wolfgang Roebke
  • 👤 Dieter Kneitel
  • 👤 Erfried Parr

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 04:54
CPC Classifications
C; C11; C11D; C11D3/00; C11D3/02; C11D3/12; C11D3/124; C11D3/1246; C11D3/128; B; B01; B01J; B01J20/00; B01J20/02; B01J20/10; B01J20/16; B01J20/18; B01J20/186; C01; C01B; C01B33/00; C01B33/20; C01B33/26; C01B33/28; C01B33/2807; C01B33/2815

Claims Analysis

Total Claims: 22
Claim 1
Independent Claim 99 words
A process for the production of an ion-exchanging alkali metal aluminum silicate having a hydrophilic surface comprising mixing a crystalline ion exchanging alkali metal aluminum silicate with a hydrophilic material which is ortho phosphoric acid, an alkali metal ortho phosphate, pentasodium tripolyphosphate, tartaric, acid, an alkali metal tartrate or pentaerythritol in the presence of water, said hydrophilic material being employed in an amount sufficient to impart hydrophilicity to the alkali metal aluminum silicate but not over 30% of the weight of the silicate, drying and subsequently grinding the treated silicate to a particle size of not over 100 microns.
Claim 2
Dependent Claim 99 words
A process for the production of an ion-exchanging alkali metal aluminum silicate having a hydrophilic surface comprising mixing a crystalline ion exchanging alkali metal aluminum silicate with a hydrophilic material which is ortho phosphoric acid, an alkali metal ortho phosphate, pentasodium tripolyphosphate, tartaric, acid, an alkali metal tartrate or pentaerythritol in the presence of water, said hydrophilic material being employed in an amount sufficient to impart hydrophilicity to the alkali metal aluminum silicate but not over 30% of the weight of the silicate, drying and subsequently grinding the treated silicate to a particle size of not over 100 microns.
Claim 3
Dependent Claim 44 words
A process according to claim 1 wherein the hydrophilic material is an ortho phosphoric acid or an alkali metal ortho phosphate in an amount sufficient to impart hydrophilicity to the alkali metal aluminum silicate but not over 30% of the weight of the silicate.
Claim 4
Dependent Claim 22 words
A process according to claim 2 wherein the phosphoric acid or alkali metal ortho phosphate is employed as a solution in water.
Claim 5
Dependent Claim 21 words
A process according to claim 1 wherein the hydrophilic material is ortho phosphoric acid, alkali metal ortho phosphate, or pentasodium tripolyphosphate.
Claim 6
Dependent Claim 36 words
A process according to claim 1 wherein the hydrophilic material is pentasodium tripolyphosphate in an amount sufficient to impart hydrophilicity to the alkali metal aluminum silicate but not over 30% of the weight of the silicate.
Claim 7
Dependent Claim 17 words
A process according to claim 5 wherein the pentasodium tripolyphosphate is employed as a solution in water.
Claim 8
Dependent Claim 41 words
A process according to claim 1 wherein the hydrophilic material is tartaric acid or a alkali metal tartrate in an amount sufficient to impart hydrophilicity to the alkali metal aluminum silicate but not over 30% of the weight of the silicate.
Claim 9
Dependent Claim 21 words
A process according to claim 7 wherein the tartaric acid or alkali metal tartrate is employed as a solution in water.
Claim 10
Dependent Claim 13 words
The hydrophilic alkali metal aluminum silicate prepared by the process of claim 7.
Claim 11
Dependent Claim 35 words
A process according to claim 1 wherein the hydrophilic material is pentaerythritol in an amount sufficient to impart hydrophilicity to the alkali metal aluminum silicate but not over 30% of the weight of the silicate.
Claim 12
Dependent Claim 16 words
A process according to claim 10 wherein the pentaerythritol is employed as a solution in water.
Claim 13
Dependent Claim 13 words
The hydrophilic alkali metal aluminum silicate prepared by the process of claim 10.
Claim 14
Dependent Claim 16 words
The process of claim 26 wherein the alkali metal aluminum silicate employed is sodium aluminum silicate.
Claim 15
Dependent Claim 20 words
The process of claim 13 wherein the silicate employed is Zeolite Type A, Zeolite Type X or Zeolite Type Y.
Claim 16
Dependent Claim 100 words
A process for the production of an ion-exchanging alkali metal aluminum silicate having a hydrophilic surface consisting of mixing a crystalline ion exchanging alkali metal aluminum silicate with a hydrophilic material which is ortho phosphoric acid, an alkali metal ortho phosphate, pentasodium tripolyphosphate, tartaric acid, an alkali metal tartrate or pentaerythritol in the presence of water, said hydrophilic material being employed in an amount sufficient to impart hydrophilicity to the alkali metal aluminum silicate but not over 30% of the weight of the silicate, drying and subsequently grinding the treated silicate to a particle size of not over 100 microns.
Claim 17
Dependent Claim 100 words
A process for the production of an ion-exchanging alkali metal aluminum silicate having a hydrophilic surface consisting of mixing a crystalline ion exchanging alkali metal aluminum silicate with a hydrophilic material which is ortho phosphoric acid, an alkali metal ortho phosphate, pentasodium tripolyphosphate, tartaric acid, an alkali metal tartrate or pentaerythritol in the presence of water, said hydrophilic material being employed in an amount sufficient to impart hydrophilicity to the alkali metal aluminum silicate but not over 30% of the weight of the silicate, drying and subsequently grinding the treated silicate to a particle size of not over 100 microns.
Claim 18
Dependent Claim 44 words
A process according to claim 15 wherein the hydrophilic material is an ortho phosphoric acid or an alkali metal ortho phosphate in an amount sufficient to impart hydrophilicity to the alkali metal aluminum silicate but not over 30% of the weight of the silicate.
Claim 19
Dependent Claim 36 words
A process according to claim 15 wherein the hydrophilic material is pentasodium tripolyphosphate in an amount sufficient to impart hydrophilicity to the alkali metal aluminum silicate but not over 30% of the weight of the silicate.
Claim 20
Dependent Claim 13 words
The hydrophilic alkali metal aluminum silicate prepared by the process of claim 15.
Claim 21
Dependent Claim 13 words
The hydrophilic alkali metal aluminum silicate prepared by the process of claim 16.
Claim 22
Dependent Claim 13 words
The hydrophilic alkali metal aluminum silicate prepared by the process of claim 17.

References Cited (Backward Citations)

US3692684A Cited
BE813581A Cited
DE2422655A1 Cited
US3962132A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-08-08 1981-02-07 1981-08-09 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-08-08 1985-02-07 1985-08-09 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-08-08 1989-02-07 1989-08-09 $7700.00 Window Closed / Lapsed

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