Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
262 words
In a device for the insertion of samples into a generally vertical chromatography column comprising: a sample holder comprising a plate mounted to rotate about an axis transverse to said column, said plate defining a plurality of cavities arranged in a ring about said axis, said chromatography column being located on one side of the sample holder, a syringe mounted on the other side of said sample holder in a position such that said cavities become successively aligned with said syringe as said plate rotates, said syringe comprising an elongated hollow body, a needle at one end of said body, and a piston mounted in said body, and both said piston and said body being mounted for translational movement parallel to said axis, and the improvement according to which at least some of said cavities are adapted to receive a sample cell while others are holes passing through said plate, the axis of rotation of the plate and the path of translational movement of said syringe lie in the same vertical plane, and the center line of a cavity aligned with said syringe, taken in a vertical plane containing said axis, is at an acute angle of at least 10° to the horizontal, and said device comprises control means for correlating the rotation of said plate to the translational movements of said syringe and piston in order to carry out a cycle of operations including the withdrawal of a sample from a cell in one of said cavities and the injection of said sample through one of said holes into said column.
Claim 2
Dependent Claim
262 words
In a device for the insertion of samples into a generally vertical chromatography column comprising: a sample holder comprising a plate mounted to rotate about an axis transverse to said column, said plate defining a plurality of cavities arranged in a ring about said axis, said chromatography column being located on one side of the sample holder, a syringe mounted on the other side of said sample holder in a position such that said cavities become successively aligned with said syringe as said plate rotates, said syringe comprising an elongated hollow body, a needle at one end of said body, and a piston mounted in said body, and both said piston and said body being mounted for translational movement parallel to said axis, and the improvement according to which at least some of said cavities are adapted to receive a sample cell while others are holes passing through said plate, the axis of rotation of the plate and the path of translational movement of said syringe lie in the same vertical plane, and the center line of a cavity aligned with said syringe, taken in a vertical plane containing said axis, is at an acute angle of at least 10° to the horizontal, and said device comprises control means for correlating the rotation of said plate to the translational movements of said syringe and piston in order to carry out a cycle of operations including the withdrawal of a sample from a cell in one of said cavities and the injection of said sample through one of said holes into said column.
Claim 3
Dependent Claim
44 words
Device as claimed in claim 1 in which the axis of rotation of said plate and the path of translation of said syringe lie at about 10° to the horizontal and the center lines of said cavities are parallel to said axis and path.
Claim 4
Dependent Claim
51 words
A device as claimed in claim 1 in which said syringe body is mounted on a carriage and said control means comprises a cam integral with said carriage and a slotted drum coaxial with and integral with said plate, and containing the same number of slots as the plate has holes.
Claim 5
Dependent Claim
39 words
A device as claimed in claim 1 in which said cavities are grouped in series of three, one of which contains a sample cell, one of which is a through hole, and one of which contains a rinsing cell.
Claim 6
Dependent Claim
70 words
Device as claimed in claim 1 in which the axis of rotation of said plate and path of translation of said syringe are horizontal and the center lines of said cavities lie in a conical locus, and wherein the axis of said conical locus is the axis about which said plate rotates and the vertex of said locus is located in the other side of said plate from said syringe.
Claim 7
Dependent Claim
26 words
A device as claimed in claim 5 comprising cells fitting into said cell-receiving cavities, said cells having tapered ends with a vertex angle of about 20°.
Claim 8
Dependent Claim
13 words
A device as claimed in claim 5 in which said needle is flexible.