← Back to Patent Explorer
US4038874A Expired / Lapsed US ⏱️ 0.0 years remaining

Device for the insertion of samples into a chromatography column

Assignee: Societe Nationale Elf Aquitaine Production SA
•
Filing: 1976-04-21
•
Granted: 1977-08-02
•
Expires: 1996-04-21
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract This invention concerns a device for inserting samples into a chromatography column. The device comprises a syringe mounted on a carriage, a sample-holder consisting of a circular plate and a control system linking the syringe and sample-holder. The plate and syringe axes are parallel, the axis of the sample-holder cell is at an angle of at least 10° to the horizontal, each cavity for a sample-holder cell is followed in turn by an aperture and a cavity for a cell containing a rinsing liquid, and a control system is provided so that during injection of the sample into the chromatography column, the syringe needle passes through the aperture. The proposed device is specially adapted for chromatographic analysis of samples in the trace form.

Inventors

  • 👤 Pierre Baldin
  • 👤 Albert Brocco
  • 👤 Jean-Paul Winstel

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 05:43
CPC Classifications
G; G01; G01N; G01N30/00; G01N30/02; G01N30/04; G01N30/16; G01N30/18; G01N35/00; G01N35/02; G01N35/04; G01N2035/0439; G01N2035/0441; G01N35/10; G01N35/1095

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 262 words
In a device for the insertion of samples into a generally vertical chromatography column comprising: a sample holder comprising a plate mounted to rotate about an axis transverse to said column, said plate defining a plurality of cavities arranged in a ring about said axis, said chromatography column being located on one side of the sample holder, a syringe mounted on the other side of said sample holder in a position such that said cavities become successively aligned with said syringe as said plate rotates, said syringe comprising an elongated hollow body, a needle at one end of said body, and a piston mounted in said body, and both said piston and said body being mounted for translational movement parallel to said axis, and the improvement according to which at least some of said cavities are adapted to receive a sample cell while others are holes passing through said plate, the axis of rotation of the plate and the path of translational movement of said syringe lie in the same vertical plane, and the center line of a cavity aligned with said syringe, taken in a vertical plane containing said axis, is at an acute angle of at least 10° to the horizontal, and said device comprises control means for correlating the rotation of said plate to the translational movements of said syringe and piston in order to carry out a cycle of operations including the withdrawal of a sample from a cell in one of said cavities and the injection of said sample through one of said holes into said column.
Claim 2
Dependent Claim 262 words
In a device for the insertion of samples into a generally vertical chromatography column comprising: a sample holder comprising a plate mounted to rotate about an axis transverse to said column, said plate defining a plurality of cavities arranged in a ring about said axis, said chromatography column being located on one side of the sample holder, a syringe mounted on the other side of said sample holder in a position such that said cavities become successively aligned with said syringe as said plate rotates, said syringe comprising an elongated hollow body, a needle at one end of said body, and a piston mounted in said body, and both said piston and said body being mounted for translational movement parallel to said axis, and the improvement according to which at least some of said cavities are adapted to receive a sample cell while others are holes passing through said plate, the axis of rotation of the plate and the path of translational movement of said syringe lie in the same vertical plane, and the center line of a cavity aligned with said syringe, taken in a vertical plane containing said axis, is at an acute angle of at least 10° to the horizontal, and said device comprises control means for correlating the rotation of said plate to the translational movements of said syringe and piston in order to carry out a cycle of operations including the withdrawal of a sample from a cell in one of said cavities and the injection of said sample through one of said holes into said column.
Claim 3
Dependent Claim 44 words
Device as claimed in claim 1 in which the axis of rotation of said plate and the path of translation of said syringe lie at about 10° to the horizontal and the center lines of said cavities are parallel to said axis and path.
Claim 4
Dependent Claim 51 words
A device as claimed in claim 1 in which said syringe body is mounted on a carriage and said control means comprises a cam integral with said carriage and a slotted drum coaxial with and integral with said plate, and containing the same number of slots as the plate has holes.
Claim 5
Dependent Claim 39 words
A device as claimed in claim 1 in which said cavities are grouped in series of three, one of which contains a sample cell, one of which is a through hole, and one of which contains a rinsing cell.
Claim 6
Dependent Claim 70 words
Device as claimed in claim 1 in which the axis of rotation of said plate and path of translation of said syringe are horizontal and the center lines of said cavities lie in a conical locus, and wherein the axis of said conical locus is the axis about which said plate rotates and the vertex of said locus is located in the other side of said plate from said syringe.
Claim 7
Dependent Claim 26 words
A device as claimed in claim 5 comprising cells fitting into said cell-receiving cavities, said cells having tapered ends with a vertex angle of about 20°.
Claim 8
Dependent Claim 13 words
A device as claimed in claim 5 in which said needle is flexible.

References Cited (Backward Citations)

US3096653A Cited
US3190731A Cited
US3508442A Cited
US3550453A Cited
US3713777A Cited
US3754443A Cited
US3918913A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-08-01 1981-01-31 1981-08-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-08-01 1985-01-31 1985-08-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-08-01 1989-01-31 1989-08-02 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag