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US4038180A Expired / Lapsed US ⏱️ 0.0 years remaining

Process of dewatering sewage sludge

Assignee: Agway Inc
•
Filing: 1976-01-09
•
Granted: 1977-07-26
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Expires: 1996-01-09
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Abstract

Abstract Sludge from a municipal or industrial sewage treatment facility is mixed with a mineral acid or anhydride thereof to release the entrapped water in the sludge. The remaining mixture of sludge solids and diluted acid or anhydride is then mixed with a basic material, such as ammonia, the heat generated by reaction of the base and acid evaporates the water to form either a completely dry mixture of sludge solids and a salt, or a mixture having a predetermined moisture content which may be air dried. In some applications it is preferable to recycle a portion of the end product by adding it to the reaction vessel.

Inventors

  • 👤 Norwood K. Talbert

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 06:59
CPC Classifications
C; C02; C02F; C02F1/00; C02F1/02; C02F1/04; C02F1/048; C02F11/00; C02F11/18; C02F11/12; C02F11/13

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 153 words
A process of dewatering non-compressible sewage sludge initially containing a known percentage by weight of water but no gaseous air phase to form an end product containing a predetermined percentage by weight of sludge solids, said process consisting essentially of: a. physically mixing a quantity of sewage sludge having a water content sufficient to render it non-compressible with a quantity of mineral acid or anhydride thereof sufficient to extract substantially all of the water initially contained in the sludge to form a mixture of sludge solids and water diluted acid; and b. placing in a reaction vessel said mixture and a base of a type and quantity sufficient to react with the acid or anhydride contained in said mixture to generate a reactive heat sufficient to remove by evaporation all of the water remaining in said mixture required to allow formation, without filtration, of a granular product comprising sludge solids and a salt.
Claim 2
Dependent Claim 153 words
A process of dewatering non-compressible sewage sludge initially containing a known percentage by weight of water but no gaseous air phase to form an end product containing a predetermined percentage by weight of sludge solids, said process consisting essentially of: a. physically mixing a quantity of sewage sludge having a water content sufficient to render it non-compressible with a quantity of mineral acid or anhydride thereof sufficient to extract substantially all of the water initially contained in the sludge to form a mixture of sludge solids and water diluted acid; and b. placing in a reaction vessel said mixture and a base of a type and quantity sufficient to react with the acid or anhydride contained in said mixture to generate a reactive heat sufficient to remove by evaporation all of the water remaining in said mixture required to allow formation, without filtration, of a granular product comprising sludge solids and a salt.
Claim 3
Dependent Claim 31 words
The invention according to claim 1 wherein said acid or anhydride is selected from the group consisting of phosphoric acid, phosphorous acid, sulfuric acid, sulfurous acid, sulfur dioxide, and sulfur trioxide.
Claim 4
Dependent Claim 11 words
The invention according to claim 2 wherein said base is ammonia.
Claim 5
Dependent Claim 23 words
The invention according to claim 1 wherein said predetermined quantity of water evaporated constitutes substantially all of the water contained in said mixture.
Claim 6
Dependent Claim 49 words
The invention according to claim 1 wherein said predetermined quantity of water evaporated constitutes substantially less than all of the water contained in said mixture, and including the further step of air drying the product after reaction of said base with the acid or anhydride contained in said mixture.
Claim 7
Dependent Claim 23 words
The invention according to claim 1 wherein the temperature of the reacting mass generated by said reactive heat is at least 250° F.
Claim 8
Dependent Claim 30 words
The invention according to claim 1 and further including recycling a predetermined portion of said product by adding said portion to said reaction vessel simultaneously with said mixture and base.
Claim 9
Dependent Claim 45 words
The invention according to claim 7 wherein the relative proportions of said recycled portion of said product, said mixture and said base are balanced to maintain a temperature and moisture content of the mass within said reaction vessel yielding a desired consistency of said mass.
Claim 10
Dependent Claim 41 words
The invention according to claim 5 and including the further step of condensing in a heat exchanger at least a portion of any volatile substances which are boiled off by the heat generated by mixing the sludge and acid or anhydride.
Claim 11
Dependent Claim 28 words
The invention according to claim 9 and further including providing at least a portion of the heated air from said heat exchanger to perform said air drying step.

References Cited (Backward Citations)

US3050383A Cited
US3527592A Cited
US3676100A Cited
US3772191A Cited
US3758287A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-07-25 1981-01-24 1981-07-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-07-25 1985-01-24 1985-07-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-07-25 1989-01-24 1989-07-26 $7700.00 Window Closed / Lapsed

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