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US4033780A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of enhancing the refractoriness of high purity fused silica

Assignee: Corning Glass Works
•
Filing: 1976-04-26
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Granted: 1977-07-05
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Expires: 1996-04-26
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Abstract

Abstract A method is disclosed wherein high purity fused silica is produced from a liquid flowable form of a silica slurry or sol and the refractoriness of the fused silica is enhanced by homogeneously doping the silica with elemental silicon.

Inventors

  • 👤 Charles E. Baumgartner
  • 👤 Peter P. Bihuniak

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 02:18
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/01; C04B35/14; C03; C03B; C03B19/00; C03B19/06; C03B19/066; C03B20/00; C03C; C03C3/00; C03C3/04; C03C3/06; C03B2201/00; C03B2201/06; C03B2201/30; C03B2201/58

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 69 words
In a method of producing a high purity fused silica product, wherein a liquid containing silica is dried to form solid silica bodies which are then thermally vitrified, the improvement, whereby the refractoriness of the fused silica is enhanced, which comprises doping a liquid flowable form of silica slurry or sol with 200 to 2500 parts per million by weight, as based on the fused silica, of elemental silicon.
Claim 2
Dependent Claim 69 words
In a method of producing a high purity fused silica product, wherein a liquid containing silica is dried to form solid silica bodies which are then thermally vitrified, the improvement, whereby the refractoriness of the fused silica is enhanced, which comprises doping a liquid flowable form of silica slurry or sol with 200 to 2500 parts per million by weight, as based on the fused silica, of elemental silicon.
Claim 3
Independent Claim 74 words
A method of producing a high purity fused silica product which comprises the steps of doping a liquid flowable form of silica slurry or sol with 200 to 2500 ppm by weight, as based on the fused silica, of elemental silicon, drying the silicon doped source of silica to rigid silica fragments containing dispersed silicon, calcining the silica fragments at about 1000°-1500° C., and then firing said silica fragments to a fused silica product.
Claim 4
Independent Claim 74 words
A method of producing a high purity fused silica product which comprises the steps of doping a liquid flowable form of silica slurry or sol with 200 to 2500 ppm by weight, as based on the fused silica, of elemental silicon, drying the silicon doped source of silica to rigid silica fragments containing dispersed silicon, calcining the silica fragments at about 1000°-1500° C., and then firing said silica fragments to a fused silica product.
Claim 5
Dependent Claim 38 words
A method in accordance with claim 2 wherein the calcined product is milled to form a slip which is cast in a mold and the product thus formed is fired to a fused silica body of corresponding shape.
Claim 6
Dependent Claim 19 words
A method in accordance with claim 2 wherein the amount of silicon dopant present is less than 1500 ppm.
Claim 7
Independent Claim 61 words
A method of enhancing the refractoriness of a fused silica product which comprises doping a liquid flowable form of silica slurry or sol with 200 to 2500 ppm by weight, as based on the fused silica, of elemental silicon, drying the silicon doped source of silica to form solid silica bodies, and firing said silica bodies to a fused silica product.
Claim 8
Independent Claim 61 words
A method of enhancing the refractoriness of a fused silica product which comprises doping a liquid flowable form of silica slurry or sol with 200 to 2500 ppm by weight, as based on the fused silica, of elemental silicon, drying the silicon doped source of silica to form solid silica bodies, and firing said silica bodies to a fused silica product.
Claim 9
Dependent Claim 20 words
A method in accordance with claim 4 wherein the silicon dopant is present in an amount less than 1500 ppm.

References Cited (Backward Citations)

US3370921A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-07-04 1981-01-03 1981-07-05 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-07-04 1985-01-03 1985-07-05 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-07-04 1989-01-03 1989-07-05 $7700.00 Window Closed / Lapsed

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