US4029736A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Processing pearlite to obtain metal silicates
Assignee: Individual
•
Filing: 1973-06-07
•
Granted: 1977-06-14
•
Expires: 1993-06-07
Abstract
Abstract Processing of pearlite by treating the same with an alkaline solution having a concentration of 40-140 g/l taken in an amount which brings the ratio of the liquid and solid phases to (0.7-1.5) : 1 and then separating by filtration the water glass, obtained in the process of heat treatment, from the residue formed.
Inventors
- 👤 Garegin Sarkisovich Melkonian
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-06 17:31
CPC Classifications
C; C01; C01B; C01B33/00; C01B33/20; C01B33/22; C01B33/24; C01B33/32
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
112 words
A method of processing pearlite comprising treating pearlite with an alkali metal hydroxide solution having a concentration of 40-140 g/l taken in an amount which brings the ratio of the liquid and solid phases to (0.7-1.5) : 1, to form a pulp, hydrothermally treating the obtained pulp in an autoclave to form water glass and separating the water glass from the residue by filtration, treating the residue with an alkali metal hydroxide solution having a concentration of 150-200 g/l taken in an amount which brings the ratio of the liquid and solid phases to 0.5:1, at a temperature not below 50° C, followed by filtering to separate a residue of sodium metasilicate.
Claim 2
Independent Claim
112 words
A method of processing pearlite comprising treating pearlite with an alkali metal hydroxide solution having a concentration of 40-140 g/l taken in an amount which brings the ratio of the liquid and solid phases to (0.7-1.5) : 1, to form a pulp, hydrothermally treating the obtained pulp in an autoclave to form water glass and separating the water glass from the residue by filtration, treating the residue with an alkali metal hydroxide solution having a concentration of 150-200 g/l taken in an amount which brings the ratio of the liquid and solid phases to 0.5:1, at a temperature not below 50° C, followed by filtering to separate a residue of sodium metasilicate.
Claim 3
Dependent Claim
21 words
The method of claim 1, wherein the residue, separated upon filtering sodium metasilicate, containing alkali metal aluminosilicates is subjected to drying.
Claim 4
Dependent Claim
53 words
The method of claim 1, wherein the filtrate, obtained on separating the sodium metasilicate by filtration is reacted with hydroxides of alkaline earth metals taken in equivalent ratios to form a pulp, and the pulp is heated to the boiling temperature, whereupon the precipitated silicates of alkaline earth metals are separated by filtration.
Claim 5
Dependent Claim
48 words
The method of claim 1, wherein the filtrate, obtained on separating the sodium metasilicate by filtration, is reacted with lead nitrate taken in an equivalent ratio to form a pulp, and the pulp is heated to the boiling temperature, whereupon the precipitated lead silicates are separated by filtration.
Claim 6
Independent Claim
138 words
A method of processing pearlite comprising treating pearlite with an alkali metal hydroxide solution have a concentration of 40-140 g/l taken in an amount which brings the ratio of the liquid and solid phases to (0.7-1.5) : 1, to form a pulp, hydrothermally treating the obtained pulp in an autoclave to form water glass and separating the water glass from the residue by filtration, treating the residue with a sodium hydroxide solution having a concentration of 150-250 g/l taken in an amount which brings the ratio of the liquid and solid phases to (4-8) : 1 at a temperature not below 50° C, to form a pulp, filtering the pulp and cooling the filtrate obtained by said filtration to a temperature below 15° C until crystals of sodium metasilicate nonahydrate are formed and separating said crystals by filtration.
Claim 7
Independent Claim
138 words
A method of processing pearlite comprising treating pearlite with an alkali metal hydroxide solution have a concentration of 40-140 g/l taken in an amount which brings the ratio of the liquid and solid phases to (0.7-1.5) : 1, to form a pulp, hydrothermally treating the obtained pulp in an autoclave to form water glass and separating the water glass from the residue by filtration, treating the residue with a sodium hydroxide solution having a concentration of 150-250 g/l taken in an amount which brings the ratio of the liquid and solid phases to (4-8) : 1 at a temperature not below 50° C, to form a pulp, filtering the pulp and cooling the filtrate obtained by said filtration to a temperature below 15° C until crystals of sodium metasilicate nonahydrate are formed and separating said crystals by filtration.
Claim 8
Dependent Claim
22 words
The method of claim 5 wherein the residue, separated upon filtering sodium metasilicate nonahydrate, containing alkali metal aluminosilicates is subjected to drying.
Claim 9
Dependent Claim
53 words
The method of claim 5, wherein the filtrate, obtained on separating the sodium metasilicate nonahydrate by filtration, is reacted with hydroxides of alkaline earth taken in equivalent ratios to form a pulp, and the pulp is heated to the boiling temperature whereupon the precipitate silicates of alkaline earth metals are separated by filtration.
Claim 10
Dependent Claim
49 words
The method of claim 5, wherein the filtrate, obtained on separating the sodium metasilicate nonahydrate by filtration, is reacted with lead nitrate taken in an equivalent ratio to form a pulp, and the pulp is heated to the boiling temperature, whereupon the precipitated lead silicates are separated by filtration.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-06-13 | 1980-12-13 | 1981-06-14 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-06-13 | 1984-12-13 | 1985-06-14 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-06-13 | 1988-12-13 | 1989-06-14 | $7700.00 | Window Closed / Lapsed |