US4022665A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Two phase anaerobic digestion
Assignee: Gas Technology Institute
•
Filing: 1974-12-09
•
Granted: 1977-05-10
•
Expires: 1994-12-09
Abstract
Abstract An improved two phase anaerobic digestion process in which an initial phase continually receives an organic feed for short detention times of less than two days under conditions which efficiently liquefy and breakdown the feed to lower molecular weight acids and other intermediates for conversion to methane. A succeeding phase is operated to treat the lower molecular weight acids and intermediates for detention times of about two to about seven days under conditions which efficiently lead to production of methane. The feed is loaded in the first phase at rates from about 1 to about 10 pounds of total organics per cubic foot per day; and the products from the initial phase are loaded in the succeeding phase at rates of about 0.1 to about 0.5 pounds total organics per cubic foot per day.
Inventors
- 👤 Sambhunath Ghosh
- 👤 Donald L. Klass
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-26 18:56
CPC Classifications
C; C02; C02F; C02F3/00; C02F3/28; C02F3/286; C02F3/34; C12; C12P; C12P5/00; C12P5/02; C12P5/023; Y; Y02; Y02E; Y02E50/00; Y02E50/30; Y10; Y10S; Y10S435/00; Y10S435/801; Y10S435/819; Y10S435/8215; Y10S435/822
Claims Analysis
Total Claims: 13
Claim 1
Independent Claim
179 words
A method for producing methane gas by a two phase anaerobic digestion of solid organic waste and biomass containing insoluble materials which includes the improved steps of: continuously delivering said feed to an acid phase digester at a loading rate of about 1 to about 10 lb. total organics per cubic foot-day, fermenting the feed in the acid phase digester under anaerobic conditions for a detention time of about 1/2 day to about 11/2 days, at a ph between about 5-6 and a temperature between about 20°-40° C., conveying the resultant acid effluent to a separate methane phase digester at a loading rate up from about 0.1 to less than about 2 lb. of total organics per cubic foot-day, fermenting the acid effluent in the methane phase digester for a detention time of about 2 to about 7 days, at a ph between about 6.8 - 7.4, and a temperature between about 20°-65° C., removing the methane for collection, and removing the feed effluent from the methane phase digester to process the solid and liquid components of the effluent.
Claim 2
Independent Claim
179 words
A method for producing methane gas by a two phase anaerobic digestion of solid organic waste and biomass containing insoluble materials which includes the improved steps of: continuously delivering said feed to an acid phase digester at a loading rate of about 1 to about 10 lb. total organics per cubic foot-day, fermenting the feed in the acid phase digester under anaerobic conditions for a detention time of about 1/2 day to about 11/2 days, at a ph between about 5-6 and a temperature between about 20°-40° C., conveying the resultant acid effluent to a separate methane phase digester at a loading rate up from about 0.1 to less than about 2 lb. of total organics per cubic foot-day, fermenting the acid effluent in the methane phase digester for a detention time of about 2 to about 7 days, at a ph between about 6.8 - 7.4, and a temperature between about 20°-65° C., removing the methane for collection, and removing the feed effluent from the methane phase digester to process the solid and liquid components of the effluent.
Claim 3
Dependent Claim
38 words
A method which includes the improved steps of claim 1 wherein the acid effluent is loaded in the methane phase digester at a rate of about 0.1 lb to about 0.5 lb. of total organics per cubic foot-day.
Claim 4
Dependent Claim
42 words
A method which includes the improved steps of claim 1 wherein the acid effluent is loaded in the methane phase digester at a thermophilic range of about 50° to about 65° C at a rate of about 2 lb. per cubic foot-day.
Claim 5
Dependent Claim
14 words
A method which includes the improved steps of claim 1 and which further includes
Claim 6
Dependent Claim
29 words
hydrolyzing the feed mixture in a prehydrolysis zone, adding a neutralizing agent to the hydrolysed feed mixture, and then delivering the hydrolysed feed mixture to the acid phase digester.
Claim 7
Dependent Claim
29 words
hydrolyzing the feed mixture in a prehydrolysis zone, adding a neutralizing agent to the hydrolysed feed mixture, and then delivering the hydrolysed feed mixture to the acid phase digester.
Claim 8
Dependent Claim
23 words
A method which includes the steps of claim 4 above wherein effluent from the methane phase digester is recycled to the prehydrolysis zone.
Claim 9
Dependent Claim
51 words
A method which includes the improved steps of claim 1 above wherein effluent from the methane phase digester is delivered to a post gasification hydrolysis zone, adding a neutralizing agent to the post hydrolysed effluent, and recycling the post hydrolysed effluent mixture to one of the acid and gas phase digesters.
Claim 10
Dependent Claim
50 words
A method which includes the improved steps of claim 1 above wherein the methane digester produces methane and carbon dioxide, and further including the step of conveying such produced gases to a gas clean-up zone to separate substantially methane, and then delivering said substantially separated methane to a collecting pipeline.
Claim 11
Dependent Claim
59 words
A method which includes the improved steps of claim 1 above and which further includes the steps of delivering effluent from the methane digester phase to a second methane digester phase, fermenting the effluent in said second methane digester phase, collecting gasification products from said second methane digester phase, and collecting the effluent from said second methane digester phase.
Claim 12
Dependent Claim
43 words
A method which includes the improved steps of claim 1 and which further includes collecting methane and carbon dioxide from the methane phase digester, and recycling said carbon dioxide to the methane phase digester for methanation and physical agitation of the mixture therein.
Claim 13
Dependent Claim
40 words
A method which includes the improved steps of claim 1 above and which further includes recycling effluent from the methane phase digester to the acid phase digester to denitrify the effluent and to reduce the volatile acids in such effluent.
References Cited (Backward Citations)
US1990523A
Cited
US3640846A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-05-09 | 1980-11-08 | 1981-05-10 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-05-09 | 1984-11-08 | 1985-05-10 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-05-09 | 1988-11-08 | 1989-05-10 | $7700.00 | Window Closed / Lapsed |