US4017952A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method for disassembling and repairing a sodium-handling apparatus
Assignee: Hitachi Ltd
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Filing: 1974-11-04
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Granted: 1977-04-19
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Expires: 1994-11-04
Abstract
Abstract A sodium-handling apparatus is disassembled and repaired by (1) contacting an inert gas with the sodium-contacting surfaces within the apparatus after discharge of sodium from the apparatus, thereby solidifying the deposited sodium, (2) flushing the inert gas with a reacting gas capable of reacting with sodium, capable of being dissolved in sodium and capable of forming a weak alkali therein, thereby forming a solid film of a neutral salt on surfaces of the deposited sodium by reaction of sodium with the reacting gas, (3) discharging the reacting gas from the apparatus, (4) disassembling and repairing the apparatus in the atmosphere, and then (5) continuing operation of the apparatus while the solid film is being retained on the surfaces of the apparatus.
Inventors
- 👤 Kiyomitsu Nemoto
- 👤 Kesahiro Naito
- 👤 Megumu Urata
- 👤 Norihiko Sagawa
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-27 09:10
CPC Classifications
B; B01; B01J; B01J19/00; B01J19/0006; B01J19/002; F; F22; F22B; F22B1/00; F22B1/02; F22B1/06; F22B1/063; G; G21; G21C; G21C1/00; G21C1/02; Y; Y02; Y02E; Y02E30/00; Y02E30/30; Y10; Y10T; Y10T29/00; Y10T29/49; Y10T29/4935; Y10T29/49352; Y10T29/49718; Y10T29/49721; Y10T29/49758; Y10T29/4981; Y10T29/49812; Y10T29/49815; Y10T29/49817
Claims Analysis
Total Claims: 20
Claim 1
Independent Claim
100 words
A method for disassembling and repairing sodium-handling apparatus for use at a high temperature, said sodium-handling apparatus having a sodium-handling space therein for handling sodium, which comprises: 1. discharging metallic sodium from the sodium-handling space of said apparatus, 2. filling an inert gas in the sodium-handling space of the apparatus, 3. cooling metallic sodium retained on the surfaces of the sodium-handling space of the apparatus to lower than the sodium solidification temperature, 4. flushing the inert gas from said sodium-handling space with a reacting gas capable of reacting with metallic sodium to form a weak alkali soluble in metallic sodium,
Claim 2
Independent Claim
100 words
A method for disassembling and repairing sodium-handling apparatus for use at a high temperature, said sodium-handling apparatus having a sodium-handling space therein for handling sodium, which comprises: 1. discharging metallic sodium from the sodium-handling space of said apparatus, 2. filling an inert gas in the sodium-handling space of the apparatus, 3. cooling metallic sodium retained on the surfaces of the sodium-handling space of the apparatus to lower than the sodium solidification temperature, 4. flushing the inert gas from said sodium-handling space with a reacting gas capable of reacting with metallic sodium to form a weak alkali soluble in metallic sodium,
Claim 3
Dependent Claim
68 words
forming a solid film of a neutral salt on the surfaces of the metallic sodium by reaction of the reacting gas with metallic sodium, 6. discharging the reacting gas from the apparatus, 7. disassembling and repairing the apparatus in the atmosphere, and thereafter 8. putting the apparatus in a high temperature operation while retaining the solid films of the neutral salt on the surfaces of the metallic sodium.
Claim 4
Dependent Claim
68 words
forming a solid film of a neutral salt on the surfaces of the metallic sodium by reaction of the reacting gas with metallic sodium, 6. discharging the reacting gas from the apparatus, 7. disassembling and repairing the apparatus in the atmosphere, and thereafter 8. putting the apparatus in a high temperature operation while retaining the solid films of the neutral salt on the surfaces of the metallic sodium.
Claim 5
Dependent Claim
17 words
A method according to claim 1, wherein only an argon gas is used as the inert gas.
Claim 6
Dependent Claim
38 words
A method according to claim 1, wherein the reacting gas capable of forming a weak alkali soluble in the metallic sodium in step (4) is carbon dioxide gas, and the neutral salt in step (5) is sodium carbonate.
Claim 7
Dependent Claim
17 words
A method according to claim 3, wherein only an argon gas is used as the inert gas.
Claim 8
Dependent Claim
123 words
A process for disassembling a sodium-handling apparatus including an internal space for handling liquid, metallic sodium, said internal space being defined by sodium-contacting surfaces, said process comprising: 1. discharging liquid, metallic sodium from said internal space, 2. filling said internal space with an inert gas, 3. cooling any liquid, metallic sodium retained on said sodium-contacting surfaces after step (1) below the solidification temperature thereof, 4. flushing said inert gas from said internal space with a reacting gas capable of reacting with metallic sodium to form a weak alkali salt soluble in liquid, metallic sodium to thereby form a solid film of said weak alkali salt on the surfaces of the solid metallic sodium deposited on said sodium-contacting surfaces, and 5. disassembling said apparatus.
Claim 9
Dependent Claim
123 words
A process for disassembling a sodium-handling apparatus including an internal space for handling liquid, metallic sodium, said internal space being defined by sodium-contacting surfaces, said process comprising: 1. discharging liquid, metallic sodium from said internal space, 2. filling said internal space with an inert gas, 3. cooling any liquid, metallic sodium retained on said sodium-contacting surfaces after step (1) below the solidification temperature thereof, 4. flushing said inert gas from said internal space with a reacting gas capable of reacting with metallic sodium to form a weak alkali salt soluble in liquid, metallic sodium to thereby form a solid film of said weak alkali salt on the surfaces of the solid metallic sodium deposited on said sodium-contacting surfaces, and 5. disassembling said apparatus.
Claim 10
Dependent Claim
42 words
The process of claim 5, further comprising: 6. reassembling said apparatus while retaining the solid film of weak alkali salt on the surfaces of the metallic sodium deposited on said sodium-contacting surfaces, and 7. filling said internal space with liquid, metallic sodium.
Claim 11
Dependent Claim
38 words
The process of claim 6, wherein the temperature of the liquid metallic sodium filled into said internal space in step (7) is at a temperature high enough to cause the film of weak alkali salt to dissolve therein.
Claim 12
Dependent Claim
20 words
The process of claim 7, wherein said reacting gas is carbon dioxide and said weak alkali salt is sodium carbonate.
Claim 13
Dependent Claim
11 words
The process of claim 8, wherein said inert gas is argon.
Claim 14
Dependent Claim
20 words
The process of claim 6, wherein said reacting gas is carbon dioxide and said weak alkali salt is sodium carbonate.
Claim 15
Dependent Claim
11 words
The process of claim 10, wherein said inert gas is argon.
Claim 16
Dependent Claim
20 words
The process of claim 5, wherein said reacting gas is carbon dioxide and said weak alkali salt is sodium carbonate.
Claim 17
Dependent Claim
11 words
The process of claim 12, wherein said inert gas is argon.
Claim 18
Dependent Claim
172 words
In a process for disassembling and reassembling a sodium-handling apparatus having an internal space therein for handling liquid, metallic sodium, said internal space being defined by sodium-contacting surfaces, in which liquid, metallic sodium is removed from said apparatus, an inert gas is filled into said internal space, the apparatus is cooled to a temperature below the solidification temperature of sodium so that liquid, metallic sodium retained on said sodium-contacting surfaces solidifies, the apparatus is disassembled, the apparatus is then reassembled, and then liquid, metallic sodium is recharged into said internal space, the improvement comprising flushing the inert gas from said internal space with a reacting gas capable of reacting with metallic sodium to form a weak alkali salt soluble in liquid, metallic sodium after solidification of liquid, metallic sodium retained on said sodium-contacting surfaces and prior to disassembly of said apparatus so that a solid film of said weak alkali salt is formed on the surfaces of the solid metallic sodium deposited on said sodium-contacting surfaces prior to disassembly of said apparatus.
Claim 19
Dependent Claim
172 words
In a process for disassembling and reassembling a sodium-handling apparatus having an internal space therein for handling liquid, metallic sodium, said internal space being defined by sodium-contacting surfaces, in which liquid, metallic sodium is removed from said apparatus, an inert gas is filled into said internal space, the apparatus is cooled to a temperature below the solidification temperature of sodium so that liquid, metallic sodium retained on said sodium-contacting surfaces solidifies, the apparatus is disassembled, the apparatus is then reassembled, and then liquid, metallic sodium is recharged into said internal space, the improvement comprising flushing the inert gas from said internal space with a reacting gas capable of reacting with metallic sodium to form a weak alkali salt soluble in liquid, metallic sodium after solidification of liquid, metallic sodium retained on said sodium-contacting surfaces and prior to disassembly of said apparatus so that a solid film of said weak alkali salt is formed on the surfaces of the solid metallic sodium deposited on said sodium-contacting surfaces prior to disassembly of said apparatus.
Claim 20
Dependent Claim
20 words
The process of claim 14, wherein said reacting gas is carbon dioxide and said weak alkali salt is sodium carbonate.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-04-18 | 1980-10-18 | 1981-04-19 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-04-18 | 1984-10-18 | 1985-04-19 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-04-18 | 1988-10-18 | 1989-04-19 | $7700.00 | Window Closed / Lapsed |