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US4017570A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of producing three dimensional skeletal structures

Assignee: Chemotronics International Inc
•
Filing: 1973-04-02
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Granted: 1977-04-12
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Expires: 1993-04-02
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Abstract

Abstract The preparation of three dimensional skeletal structures using the step of deforming rounded beads to form a mold or matrix is described. A filler material is introduced and then rigidified to form the skeletal structure. The deformable beads are composed of materials which deform upon compression or expansion due to pressure from adjacent beads and included, for instance, metals, waxes, salts, polymers, and ceramic compositions in their plasticly deformable states. The filler material which rigidifies to form the skeletal structure can be composed of solidifiable materials such as metals, polymers, or ceramic compositions. The solid material volume of the skeletal structure so formed upon removal of the beads is between about 2% to 20% of a corresponding volume of a non-skeletal solid material. The corresponding porosities representing the interconnected void volumes are between about 80% and 98% of a corresponding volume of a non-skeletal solid material. The skeletal structures so formed can be flexible, semiflexible or rigid and are useful as heat exchangers, catalyst supports, distillation tower packings, filters and the like.

Inventors

  • 👤 Warren A. Rice
  • 👤 Clarence S. Vinton
  • 👤 Hugh Richard Norris

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 21:14
CPC Classifications
B; B29; B29C; B29C44/00; B29C44/02; B29C44/12; B01; B01D; B01D39/00; B01D39/14; B01D39/20; B01D39/2027; B01D39/2031; B01D39/2037; B01D39/2051; B01D39/2068; B01D39/2093; B22; B22F; B22F3/00; B22F3/10; B22F3/11; B22F3/1103; B22F3/1112; B01D2239/00; B01D2239/04; B01D2239/0471

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 225 words
In the method of producing a three dimensional skeletal structure by introducing and rigidifying a powdered filler material which is to form the skeletal structure in a matrix formed by a removable mold of packed beads which can be removed by melting, decomposition or volatilization or by a solvent or reactant which is a non-solvent or non-reactant with the filler material, the improvement which comprises: a. partially deforming packed deformable beads having comparable dimensions and an average diameter of at least about one one-hundredth of an inch which are in contact with each other to form a mold with interconnected void spaces between the partially deformed beads; b. introducing particles of a powdered filler material which is loosely bondable upon compression into the interconnected void spaces between the packed, partially deformed beads while maintaining the beads in contact with each other; c. compressing the powdered filler material and the partially deformed beads to form a heterogeneous solid mass of fully deformed beads with the particles of the filler material bonded together to form the continuous and interconnected skeletal structure without being bonded to the beads sufficiently to prevent removal and wherein the fully deformed beads occupy between about 80 and 98 percent of the total volume; and d. removing the deformed beads from the heterogeneous mass without removing the filler material forming the skeletal structure.
Claim 2
Dependent Claim 225 words
In the method of producing a three dimensional skeletal structure by introducing and rigidifying a powdered filler material which is to form the skeletal structure in a matrix formed by a removable mold of packed beads which can be removed by melting, decomposition or volatilization or by a solvent or reactant which is a non-solvent or non-reactant with the filler material, the improvement which comprises: a. partially deforming packed deformable beads having comparable dimensions and an average diameter of at least about one one-hundredth of an inch which are in contact with each other to form a mold with interconnected void spaces between the partially deformed beads; b. introducing particles of a powdered filler material which is loosely bondable upon compression into the interconnected void spaces between the packed, partially deformed beads while maintaining the beads in contact with each other; c. compressing the powdered filler material and the partially deformed beads to form a heterogeneous solid mass of fully deformed beads with the particles of the filler material bonded together to form the continuous and interconnected skeletal structure without being bonded to the beads sufficiently to prevent removal and wherein the fully deformed beads occupy between about 80 and 98 percent of the total volume; and d. removing the deformed beads from the heterogeneous mass without removing the filler material forming the skeletal structure.
Claim 3
Dependent Claim 17 words
The method of claim 1 wherein the beads are essentially spherical and have a substantially uniform diameter.
Claim 4
Dependent Claim 14 words
The method of claim 1 wherein the deformable beads are composed of a polymer.
Claim 5
Dependent Claim 14 words
The method of claim 1 wherein the deformable beads are composed of a metal.
Claim 6
Dependent Claim 13 words
The method of claim 1 wherein the powdered filler material is a metal.
Claim 7
Dependent Claim 27 words
The method of claim 1 wherein the beads are removed by heat at a temperature less than the destruction temperature of the bonded powdered filler material particles.
Claim 8
Dependent Claim 25 words
The method of claim 1 wherein the partial deformation of the beads is less than about fifty percent of the final deformation of the beads.
Claim 9
Dependent Claim 15 words
The method of claim 1 wherein the beads are metal and the power is metal.
Claim 10
Dependent Claim 34 words
The method of claim 1 wherein the powder is metal, the beads are metal and the partial deformation of the beads is less than about fifty percent of the final deformation of the beads.
Claim 11
Dependent Claim 11 words
The method of claim 9 wherein the metal powder contains iron.

References Cited (Backward Citations)

US2695231A Cited
US3078552A Cited
US3258349A Cited
US3396923A Cited
US3535110A Cited
US3734723A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-04-11 1980-10-11 1981-04-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-04-11 1984-10-11 1985-04-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-04-11 1988-10-11 1989-04-12 $7700.00 Window Closed / Lapsed

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