US4014965A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for scrapless forming of plastic articles
Assignee: Dow Chemical Co
•
Filing: 1972-11-24
•
Granted: 1977-03-29
•
Expires: 1992-11-24
Abstract
Abstract Plastic articles without foam spots are produced by an improved powder forming process wherein a powder of normally solid, thermoplastic polymer is compacted by means of vibratory energy into briquettes which are subsequently forged and formed into articles of fused polymer.
Inventors
- 👤 Steven H. Stube
- 👤 Douglas S. Chisholm
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 14:50
CPC Classifications
B; B29; B29C; B29C43/00; B29C43/02; B29C43/16; B29C43/006; B29C2791/00; B29C2791/001; B29C2791/004; B29C2791/008; B29K; B29K2055/00; B29K2086/00; B29K2105/00; B29K2105/25; B29K2105/251; B29K2105/253; B29K2105/255
Claims Analysis
Total Claims: 15
Claim 1
Independent Claim
120 words
In a process for forming articles from a powder of a thermoplastic resinous polymer wherein the powder in an amount sufficient to produce the article is compressed at a temperature below the melt temperature of the powder into a briquette containing polymer particles and having green strength and the briquette having been maintained at a temperature in the range from about the alpha transition temperature to less than the melt temperature of the polymer for a time sufficient to effect sintering of the polymer particles of the briquette is forged into an article of fused polymer; the improvement which comprises compacting the powder with vibratory energy to form the briquette having a percent compaction of at least about 85 percent.
Claim 2
Dependent Claim
120 words
In a process for forming articles from a powder of a thermoplastic resinous polymer wherein the powder in an amount sufficient to produce the article is compressed at a temperature below the melt temperature of the powder into a briquette containing polymer particles and having green strength and the briquette having been maintained at a temperature in the range from about the alpha transition temperature to less than the melt temperature of the polymer for a time sufficient to effect sintering of the polymer particles of the briquette is forged into an article of fused polymer; the improvement which comprises compacting the powder with vibratory energy to form the briquette having a percent compaction of at least about 85 percent.
Claim 3
Dependent Claim
15 words
The improvement of claim 1 wherein the vibratory energy is supplied by a reciprocating means.
Claim 4
Dependent Claim
14 words
The improvement of claim 2 wherein the reciprocating means is a reciprocating pneumatic hammer.
Claim 5
Dependent Claim
14 words
The improvement of claim 1 wherein the vibratory energy is supplied by oscillating means.
Claim 6
Dependent Claim
19 words
The improvement of claim 1 wherein the vibratory energy is supplied by a combination sonic means and compacting means.
Claim 7
Dependent Claim
20 words
The improvement of claim 5 wherein the sonic means is a hydroacoustic oscillator and the compacting means is a press.
Claim 8
Dependent Claim
55 words
The improvement of claim 1 wherein a polyethylene powder is compacted with vibratory energy for a time in the range from about 0.008 to about 45 seconds, using a pressure in the range from about 40 to about 60,000 psi and a frequency in the range from about 1 to about 25,000 cycles per second.
Claim 9
Dependent Claim
24 words
The improvement of claim 7 wherein the polyethylene powder has an average particle size in the range from about 20 to about 100 microns.
Claim 10
Dependent Claim
169 words
In a process for forming articles from a powder of a thermoplastic resinous polymer wherein the powder in an amount sufficient to produce the article is compressed at a temperature below the melt temperature of the powder into a briquette containing polymer particles and having green strength and the briquette having been maintained at a temperature in the range from about the alpha transition temperature to less than the melt temperature of the polymer for a time sufficient to effect sintering of the polymer particles of the briquette is forged into an article of fused polymer; the improvement which comprises compacting the powder with vibratory energy for a time in the range from about 0.008 to about 45 seconds, using a compaction pressure in the range from about 40 to about 60,000 psi, a frequency in the range from about 1 to about 25,000 cycles per second and a temperature within the range from ambient up to temperatures below the melting point of the polymer to form the briquette.
Claim 11
Dependent Claim
169 words
In a process for forming articles from a powder of a thermoplastic resinous polymer wherein the powder in an amount sufficient to produce the article is compressed at a temperature below the melt temperature of the powder into a briquette containing polymer particles and having green strength and the briquette having been maintained at a temperature in the range from about the alpha transition temperature to less than the melt temperature of the polymer for a time sufficient to effect sintering of the polymer particles of the briquette is forged into an article of fused polymer; the improvement which comprises compacting the powder with vibratory energy for a time in the range from about 0.008 to about 45 seconds, using a compaction pressure in the range from about 40 to about 60,000 psi, a frequency in the range from about 1 to about 25,000 cycles per second and a temperature within the range from ambient up to temperatures below the melting point of the polymer to form the briquette.
Claim 12
Dependent Claim
60 words
The improvement of claim 7 wherein the time is in the range from about 0.008 to 15 seconds, the pressure is in the range from about 5,000 to about 25,000 psi, the frequency is in the range from about 25 to about 15,000 cycles per second and the temperature is in the range from about 20° to about 120° C.
Claim 13
Dependent Claim
30 words
The improvement of claim 1 wherein the polymer is a crystalline polymer and the alpha transition temperature is suitable to render the polymer sufficiently ductile to cold flow and fuse.
Claim 14
Dependent Claim
139 words
In a process for forming articles from a powder of a thermoplastic resinous polymer wherein the powder in an amount sufficient to produce the article is compressed at a temperature below the melt temperature of the powder into a briquette containing polymer particles and having green strength and the briquette having been maintained at a temperature in the range from about the alpha transition temperature to less than the melt temperature of the polymer for a time sufficient to effect sintering of the polymer particles of the briquette is forged with a forging apparatus into an article of fused polymer wherein lubrication is provided between the contacting surfaces of the briquette and the forging apparatus; the improvement which comprises compacting the powder with vibratory energy to form the briquette having a percent compaction of at least about 85 percent.
Claim 15
Dependent Claim
139 words
In a process for forming articles from a powder of a thermoplastic resinous polymer wherein the powder in an amount sufficient to produce the article is compressed at a temperature below the melt temperature of the powder into a briquette containing polymer particles and having green strength and the briquette having been maintained at a temperature in the range from about the alpha transition temperature to less than the melt temperature of the polymer for a time sufficient to effect sintering of the polymer particles of the briquette is forged with a forging apparatus into an article of fused polymer wherein lubrication is provided between the contacting surfaces of the briquette and the forging apparatus; the improvement which comprises compacting the powder with vibratory energy to form the briquette having a percent compaction of at least about 85 percent.
References Cited (Backward Citations)
US2198612A
Cited
US2246165A
Cited
US2384215A
Cited
US2645836A
Cited
US2747231A
Cited
US3152082A
Cited
US3555605A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-03-28 | 1980-09-27 | 1981-03-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-03-28 | 1984-09-27 | 1985-03-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-03-28 | 1988-09-27 | 1989-03-29 | $7700.00 | Window Closed / Lapsed |