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US4013505A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of deinking printed wastepapers

Assignee: Vyzkumny Ustav Papieru A Celulosy
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Filing: 1975-05-30
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Granted: 1977-03-22
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Expires: 1995-05-30
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Abstract

Abstract A method for deinking printed wastepapers in a system of separators through which printed wastepapers, previously impregnated with surface-active agents and alkalis, and repulped in the presence of an organic hydrocarbon compound and high-adsorptive flakes obtained by precipitating solutions of metal soaps of fatty or bituminous acids with solutions of salts of alkaline earths, are forced. The adsorptive flakes containing printing ink are separated from the repulped paper stock by latent vortex action.

Inventors

  • 👤 Cestmir Balcar
  • 👤 Antonin Kostka
  • 👤 Jaroslav Havranek
  • 👤 Marcel Lalak

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 06:00
CPC Classifications
D; D21; D21C; D21C5/00; D21C5/02; D21C5/025; D21C5/027; Y; Y02; Y02W; Y02W30/00; Y02W30/50; Y02W30/64

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 234 words
Process of deinking printed wastepapers which comprises impregnating said papers with a solution of alkali reacting compounds selected from the group consisting of sodium hydroxide, potassium hydroxide, sodium silicate and sodium carbonate in an amount of from 0.5 to 4.0% by weight of wastepaper charge, and of from 0.2 to 2.0% by weight of wastepaper charge of surface active agents characterized by having wetting and detergent power selected from the group consisting of alkyl benzene sulphonates, alkyl ether polyoxyethylene sulphonates, alkyl phenyl ether polyoxyethylene sulphonates, polyoxyethylene alkyl phenol ethers, polyoxyethylene alkyl ethers, polyglycol esters of fatty acids, alkylolamides of fatty acids, and quaternary condensation products of fatty amine with ethylene oxide for releasing the printing ink from the paper, thereafter repulping said paper to effect separation of the ink from the paper, during the repulping adding large flakes of granular shape of high-adsorptive material to the solution containing paper, said flakes being prepared separately by precipitating a solution of metal soaps of organic acids with a solution of salt of alkaline earths, together with addition of a suitable organic compound of hydrocarbon character to increase the stability of said flakes and to improve adsorption of the printing ink onto said flakes, and thereafter removing said granular flakes with adsorbed printing ink from the repulped paper stock by latent vortex action in an outer vortex in the solution in which the repulped paper is suspended.
Claim 2
Dependent Claim 234 words
Process of deinking printed wastepapers which comprises impregnating said papers with a solution of alkali reacting compounds selected from the group consisting of sodium hydroxide, potassium hydroxide, sodium silicate and sodium carbonate in an amount of from 0.5 to 4.0% by weight of wastepaper charge, and of from 0.2 to 2.0% by weight of wastepaper charge of surface active agents characterized by having wetting and detergent power selected from the group consisting of alkyl benzene sulphonates, alkyl ether polyoxyethylene sulphonates, alkyl phenyl ether polyoxyethylene sulphonates, polyoxyethylene alkyl phenol ethers, polyoxyethylene alkyl ethers, polyglycol esters of fatty acids, alkylolamides of fatty acids, and quaternary condensation products of fatty amine with ethylene oxide for releasing the printing ink from the paper, thereafter repulping said paper to effect separation of the ink from the paper, during the repulping adding large flakes of granular shape of high-adsorptive material to the solution containing paper, said flakes being prepared separately by precipitating a solution of metal soaps of organic acids with a solution of salt of alkaline earths, together with addition of a suitable organic compound of hydrocarbon character to increase the stability of said flakes and to improve adsorption of the printing ink onto said flakes, and thereafter removing said granular flakes with adsorbed printing ink from the repulped paper stock by latent vortex action in an outer vortex in the solution in which the repulped paper is suspended.
Claim 3
Dependent Claim 34 words
Method as defined in claim 1, wherein the organic compound of hydrocarbon character is selected from the group consisting of terpene hydrocarbons, terpene alcohols, aliphatic hydrocarbons, aromatic hydrocarbons, and alcohols and a mixture thereof.
Claim 4
Dependent Claim 21 words
Method as defined in claim 1, wherein the organic acids are selected from the group consisting of fatty and bituminous acids.
Claim 5
Dependent Claim 35 words
Method as defined in claim 1, wherein the preparation of said flakes is carried out in the presence of loading materials in an amount of from 0.5 to 5.0% by weight of the wastepaper charge.
Claim 6
Dependent Claim 28 words
Method as defined in claim 4, wherein the loading materials are selected from the group consisting of bentonite, china clay, blavo fixe, gypsum, barytes, activated silica and magnetite.

References Cited (Backward Citations)

US2077059A Cited
US2005742A Cited
US1990376A Cited
US2112562A Cited
US3056713A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-03-21 1980-09-20 1981-03-22 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-03-21 1984-09-20 1985-03-22 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-03-21 1988-09-20 1989-03-22 $7700.00 Window Closed / Lapsed

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