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US4009231A Expired / Lapsed US ⏱️ 0.0 years remaining

Powder barrier bonding technique

Assignee: United States Department of the Navy
•
Filing: 1975-03-20
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Granted: 1977-02-22
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Expires: 1995-03-20
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Abstract

Abstract A barrier layer made up of a suitable powder interspersed within either a trix of cured propellant binder or a matrix of silicone rubber is interposed between a silicone rubber insulator and a solid propellant grain in a rocket motor to prevent curatives from migrating from the propellant into the silicone rubber layer when the propellant is cast.

Inventors

  • 👤 Bernard Wasserman
  • 👤 William H. Thielbahr

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 11:24
CPC Classifications
C; C06; C06B; C06B21/00; C06B21/0083; C06B45/00; C06B45/12

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 73 words
In a method for loading a rocket motor which comprises casting and curing a solid propellant within a combustion chamber which is lined with a layer of cured silicone rubber insulator material, the improvement residing in casting and curing a barrier layer on said layer of insulator material before casting and curing the propellant grain to prevent materials in the propellant grain from migrating into the insulator layer as the propellant grain cures.
Claim 2
Dependent Claim 73 words
In a method for loading a rocket motor which comprises casting and curing a solid propellant within a combustion chamber which is lined with a layer of cured silicone rubber insulator material, the improvement residing in casting and curing a barrier layer on said layer of insulator material before casting and curing the propellant grain to prevent materials in the propellant grain from migrating into the insulator layer as the propellant grain cures.
Claim 3
Dependent Claim 51 words
In a method according to claim 1 the additional improvement residing in utilizing, as said barrier layer, a composite made up of a powder selected from the group consisting of copper, silica and aluminum interspersed in a matrix of binder selected from the group consisting of carboxy and hydroxy terminated polybutadiene.
Claim 4
Dependent Claim 19 words
A method according to claim 2 wherein the powder is silica powder and the matrix is carboxy terminated polybutadiene.
Claim 5
Dependent Claim 35 words
A method according to claim 3 wherein from 65 to 75 weight percent of the barrier layer is silica and wherein from 35 to 25 weight percent of the barrier layer is carboxy terminated polybutadiene.
Claim 6
Independent Claim 51 words
A method for providing a barrier layer to substantially prevent migration of a curing agent from a solid propellant grain into an insulation layer comprising the steps of: 1. applying an uncured blend of silicone rubber and a powder onto the cured insulation; and 2. allowing said barrier layer to cure.
Claim 7
Independent Claim 51 words
A method for providing a barrier layer to substantially prevent migration of a curing agent from a solid propellant grain into an insulation layer comprising the steps of: 1. applying an uncured blend of silicone rubber and a powder onto the cured insulation; and 2. allowing said barrier layer to cure.
Claim 8
Dependent Claim 34 words
A method according to claim 5 wherein said insulation layer is made up of silicone rubber and wherein said powder is selected from the group consisting of copper powder, silica powder and aluminum powder.

References Cited (Backward Citations)

US3301924A Cited
US3578520A Cited
US3813308A Cited
US3855176A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-02-22 1980-08-23 1981-02-22 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-02-22 1984-08-23 1985-02-22 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-02-22 1988-08-23 1989-02-22 $7700.00 Window Closed / Lapsed

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