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US3990955A Expired / Lapsed US ⏱️ 0.0 years remaining

Electrodeposition of hard nickel

Assignee: Huntington Alloys Corp
•
Filing: 1974-11-29
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Granted: 1976-11-09
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Expires: 1994-11-29
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Abstract

Abstract Sulfur-free hard nickel in thicknesses in excess of about 50 microns is electrodeposited from nickel plating baths containing 1 to about 8 grams per liter (gpl) of aromatic amide.

Inventors

  • 👤 Aloys J. Dill

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-02 22:44
CPC Classifications
C; C25; C25D; C25D3/00; C25D3/02; C25D3/12; C25D3/14

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 81 words
A process of nickel electrodeposition comprising electrolyzing an aqueous nickel plating bath containing in addition to nickel salt, about 0.5 to about 8 grams per liter of an organic, saturated, hydrolysis resistant sulfur-free aromatic, carboxylic acid amide at a cathode current density of about 1.5 to about 50 amperes per square decimeter and at a temperature in the range of about 30° to about 70° C for a time sufficient to form a hard deposit at least about 100 microns thick.
Claim 2
Dependent Claim 81 words
A process of nickel electrodeposition comprising electrolyzing an aqueous nickel plating bath containing in addition to nickel salt, about 0.5 to about 8 grams per liter of an organic, saturated, hydrolysis resistant sulfur-free aromatic, carboxylic acid amide at a cathode current density of about 1.5 to about 50 amperes per square decimeter and at a temperature in the range of about 30° to about 70° C for a time sufficient to form a hard deposit at least about 100 microns thick.
Claim 3
Dependent Claim 19 words
A process as in claim 1 wherein the bath contains one or more of benzamide, phthalamide or hippuric acid.
Claim 4
Dependent Claim 29 words
A process as in claim 1 wherein the bath contains nickel principally as the sulfate or sulphamate and is maintained at a temperature of up to about 60° C.
Claim 5
Dependent Claim 83 words
A process of nickel electrodeposition comprising electrolyzing an aqueous nickel plating bath containing in addition to nickel salt selected from the group consisting of nickel sulfate and nickel sulphamate about 1.5 to about 3 grams per liter of hippuric acid at a cathode current density of about 0.5 to about 5.0 amperes per square decimeter and at a temperature in the range of about 30° to about 60° C for a time sufficient to form a hard deposit at least 50 microns thick.
Claim 6
Dependent Claim 83 words
A process of nickel electrodeposition comprising electrolyzing an aqueous nickel plating bath containing in addition to nickel salt selected from the group consisting of nickel sulfate and nickel sulphamate about 1.5 to about 3 grams per liter of hippuric acid at a cathode current density of about 0.5 to about 5.0 amperes per square decimeter and at a temperature in the range of about 30° to about 60° C for a time sufficient to form a hard deposit at least 50 microns thick.

References Cited (Backward Citations)

US2694041A Cited
US2781305A Cited
GB899795A Cited
US3139393A Cited
US3576725A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-11-09 1980-05-10 1980-11-09 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-11-09 1984-05-10 1984-11-09 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-11-09 1988-05-10 1988-11-09 $7700.00 Window Closed / Lapsed

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