US3985841A
Expired / Lapsed
US
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Method and means for producing solid evacuated microspheres of hydrogen
Assignee: Energy Research and Development Administration ERDA
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Filing: 1975-11-06
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Granted: 1976-10-12
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Expires: 1995-11-06
Abstract
Abstract A method is provided for producing solid, evacuated microspheres comprised of hydrogen. The spheres are produced by forming a jet of liquid hydrogen and exciting mechanical waves on the jet of appropriate frequency so that the jet breaks up into drops with a bubble formed in each drop by cavitation. The drops are exposed to a pressure less than the vapor pressure of the liquid hydrogen so that the bubble which is formed within each drop expands. The drops which contain bubbles are exposed to an environment having a pressure just below the triple point of liquid hydrogen and they thereby freeze giving solid, evacuated spheres of hydrogen.
Inventors
- 👤 Robert J. Turnbull
- 👤 Christopher A. Foster
- 👤 Charles D. Hendricks
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-26 09:17
CPC Classifications
C; C01; C01B; C01B3/00; Y; Y10; Y10S; Y10S376/00; Y10S376/916
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
86 words
A method for producing solid, evacuated microspheres comprised of hydrogen, including the steps of: a. forming a jet of liquid hydrogen; b. exciting mechanical waves on the jet to induce said jet to break up into drops and to induce bubbles to form within said drops; c. subjecting said drops with bubbles therein to a pressure less than the vapor pressure of said liquid hydrogen so that said bubbles expand at a desired rate; and d. freezing said drops thereby forming solid, evacuated microspheres of hydrogen.
Claim 2
Independent Claim
86 words
A method for producing solid, evacuated microspheres comprised of hydrogen, including the steps of: a. forming a jet of liquid hydrogen; b. exciting mechanical waves on the jet to induce said jet to break up into drops and to induce bubbles to form within said drops; c. subjecting said drops with bubbles therein to a pressure less than the vapor pressure of said liquid hydrogen so that said bubbles expand at a desired rate; and d. freezing said drops thereby forming solid, evacuated microspheres of hydrogen.
Claim 3
Dependent Claim
20 words
The method of claim 1 further including the step of slightly superheating said liquid hydrogen prior to forming said jet.
Claim 4
Dependent Claim
49 words
The method of claim 2 wherein said freezing includes subjecting said drops with bubbles to a pressure less than the triple point pressure of hydrogen so that said drops freeze prior to bursting and so that gaseous hydrogen within said bubbles condenses thereby producing solid evacuated microspheres of hydrogen.
Claim 5
Dependent Claim
24 words
The method of claim 3 wherein said exciting said jet causes cavitation nuclei to form in said drops, said cavitation nuclei being said bubbles.
References Cited (Backward Citations)
No citation records indexed.
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-10-12 | 1980-04-12 | 1980-10-12 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-10-12 | 1984-04-12 | 1984-10-12 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-10-12 | 1988-04-12 | 1988-10-12 | $7700.00 | Window Closed / Lapsed |