US3982973A — Cube textured nickel

Claim 1

Independent Claim 226 words

A process comprising providing a billet of metal having the fine-grain condition characterized by an average grain size up to 0.08 millimeter and having a composition consisting essentially of 0.0002% to about 0.003% sulfur, up to about 6% cobalt, up to 0.10% carbon, at least one ingredient from the group consisting of 0.1% to 0.5% iron, 0.1% to 0.5% manganese, 0.01% to 0.1% in total of the rare earth metals lanthanum and neodymium, 0.001% to 0.1% calcium and combinations thereof, with balance essentially nickel, provided that when the billet metal contains at least 0.0008% sulfur the billet metal also contain at least one of the rare earth metals and calcium ingredients, cold working the billet metal unidirectionally to reduce the thickness at least 95% and form the metal to strip having a thickness of up to about 0.25 millimeter, heating the cold worked strip in a nonoxidizing atmosphere in the temperature range of about 800° C to about 1260° C, provided that the heating be in the range of 900° C to 1100° C when the rare earth ingredient is present and the iron, manganese and calcium ingredients are absent, for a time sufficient to anneal and recrystallize the metal to the primary recrystallized cube texture condition and then cooling the recrystallized metal sufficiently to maintain the primary recrystallized cube texture condition and prevent secondary recrystallization.

Claim 2

Dependent Claim 226 words

A process comprising providing a billet of metal having the fine-grain condition characterized by an average grain size up to 0.08 millimeter and having a composition consisting essentially of 0.0002% to about 0.003% sulfur, up to about 6% cobalt, up to 0.10% carbon, at least one ingredient from the group consisting of 0.1% to 0.5% iron, 0.1% to 0.5% manganese, 0.01% to 0.1% in total of the rare earth metals lanthanum and neodymium, 0.001% to 0.1% calcium and combinations thereof, with balance essentially nickel, provided that when the billet metal contains at least 0.0008% sulfur the billet metal also contain at least one of the rare earth metals and calcium ingredients, cold working the billet metal unidirectionally to reduce the thickness at least 95% and form the metal to strip having a thickness of up to about 0.25 millimeter, heating the cold worked strip in a nonoxidizing atmosphere in the temperature range of about 800° C to about 1260° C, provided that the heating be in the range of 900° C to 1100° C when the rare earth ingredient is present and the iron, manganese and calcium ingredients are absent, for a time sufficient to anneal and recrystallize the metal to the primary recrystallized cube texture condition and then cooling the recrystallized metal sufficiently to maintain the primary recrystallized cube texture condition and prevent secondary recrystallization.

Claim 3

Dependent Claim 21 words

A process as set forth in claim 1 wherein the average grain size of the billet is up to 0.03 millimeters.

Claim 4

Dependent Claim 21 words

A process as set forth in claim 1 wherein the carbon content of the billet metal is up to 0.05% carbon.

Claim 5

Dependent Claim 22 words

A process as set forth in claim 1 wherein the temperature of heating the cold worked strip is at least 980° C.

Claim 6

Dependent Claim 23 words

A process as set forth in claim 4 wherein the period of heating the cold worked strip is 3 minutes to 20 minutes.

Claim 7

Dependent Claim 34 words

A process as set forth in claim 1 wherein the billet is a compacted and sintered powder metal billet that contains 0.1% to 0.5% of metal from the group iron, manganese and mixtures thereof.

Claim 8

Dependent Claim 24 words

A process as set forth in claim 1 wherein the billet is a melted, cast and rolled metal billet containing 0.02% to 0.06% calcium.

Claim 9

Dependent Claim 53 words

A process as set forth in claim 1 wherein the billet is a melted, cast and rolled metal billet containing 0.01% to 0.1% in total of metal from the group lanthanum and neodymium and wherein the temperature of heating the cold worked strip is in the range of 900° C to 1100° C.

Claim 10

Dependent Claim 209 words

A cold-rolled and cube-textured nickel metal strip product having a thickness up to about 0.25 millimeters, a composition consisting essentially of 0.0002% to about 0.003% sulfur, up to about 6% cobalt, up to 0.1% carbon, at least one ingredient from the group consisting of 0.1% to 0.5% iron, 0.1% to 0.5% manganese, 0.01% to 0.1% in total of the rare earth metals lanthanum and neodymium, 0.001% to 0.1% calcium, and mixtures thereof, provided that when the product metal contains at least 0.0008% sulfur the product metal also contain at least one of the rare earth metals and calcium ingredients, with balance essentially nickel and characterized by a second velocity in the metal parallel to the direction of cold rolling of up to 4000 meters per second, said strip product having been heated in a non-oxidizing atmosphere in the temperature range of about 800° C to about 1260° C, provided that the heating having been in the range of 900° C to 1100° C when the rare earth ingredient is present and the iron, manganese and calcium ingredients are absent, for a time sufficient to anneal and recrystallize the metal, said strip product having been subsequently cooled sufficiently to maintain the primary recrystallized cube texture condition and prevent secondary recrystallization.

Claim 11

Dependent Claim 209 words

A cold-rolled and cube-textured nickel metal strip product having a thickness up to about 0.25 millimeters, a composition consisting essentially of 0.0002% to about 0.003% sulfur, up to about 6% cobalt, up to 0.1% carbon, at least one ingredient from the group consisting of 0.1% to 0.5% iron, 0.1% to 0.5% manganese, 0.01% to 0.1% in total of the rare earth metals lanthanum and neodymium, 0.001% to 0.1% calcium, and mixtures thereof, provided that when the product metal contains at least 0.0008% sulfur the product metal also contain at least one of the rare earth metals and calcium ingredients, with balance essentially nickel and characterized by a second velocity in the metal parallel to the direction of cold rolling of up to 4000 meters per second, said strip product having been heated in a non-oxidizing atmosphere in the temperature range of about 800° C to about 1260° C, provided that the heating having been in the range of 900° C to 1100° C when the rare earth ingredient is present and the iron, manganese and calcium ingredients are absent, for a time sufficient to anneal and recrystallize the metal, said strip product having been subsequently cooled sufficiently to maintain the primary recrystallized cube texture condition and prevent secondary recrystallization.

Claim 12

Dependent Claim 31 words

A product as set forth in claim 9 containing up to 0.1% cobalt and further characterized by a K 1p value of minus 37,500 ergs per cubic centimeter or more negative.

Annuity Stage	Window Opens	Payment Deadline	Surcharge Period Until	Estimated Fee	Status
3.5 Years (Year 4)	1979-09-28	1980-03-29	1980-09-28	$2000.00	Window Closed / Lapsed
7.5 Years (Year 8)	1983-09-28	1984-03-29	1984-09-28	$3760.00	Window Closed / Lapsed
11.5 Years (Year 12)	1987-09-28	1988-03-29	1988-09-28	$7700.00	Window Closed / Lapsed

Cube textured nickel

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