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US3979335A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the preparation of synthetic zeolites

Assignee: Individual
•
Filing: 1974-12-27
•
Granted: 1976-09-07
•
Expires: 1994-12-27
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Abstract

Abstract A process for the preparation of synthetic zeolites comprising mixing zeolite powder of a particle size not exceeding 5 mcm with a natural binder of a particle size of 250-500 A. The resulting mixture is wetted with water and pelletized, the pellets thus obtained being calcined at 600°-700°C.

Inventors

  • 👤 Georgy Anatolievich Golovko
  • 👤 Boris Alexandrovich Lipkind
  • 👤 Albina Timofeevna Slepneva
  • 👤 Alexandr Semenovich Leontiev
  • 👤 Vladimir Mikhailovich Mazin
  • 👤 Elena Nikolaevna Berezovskaya
  • 👤 Valentin Alexandrovich Burylov
  • 👤 Alexandr Mikhailovich Zubkov
  • 👤 Olga Alexeevna Konakova
  • 👤 Alexandr Ivanovich Judaev
  • 👤 Valentin Nikolaevich Pavlychev
  • 👤 Jury Yakovlevich Ignatov
  • 👤 Evgeny Alexandrovich Kharitonov

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 11:41
CPC Classifications
B; B01; B01J; B01J20/00; B01J20/02; B01J20/10; B01J20/16; B01J20/18

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 57 words
A process for the preparation of synthetic zeolite pellets of high mechanical strength and dynamic activity comprising mixing zeolite powder of a particle size not exceeding 5 mcm with a natural clay binder of a particle size of 250-500 A; wetting the resulting mixture with water and pelletizing the same; and calcining the resulting pellets at 600°-700°C.
Claim 2
Dependent Claim 57 words
A process for the preparation of synthetic zeolite pellets of high mechanical strength and dynamic activity comprising mixing zeolite powder of a particle size not exceeding 5 mcm with a natural clay binder of a particle size of 250-500 A; wetting the resulting mixture with water and pelletizing the same; and calcining the resulting pellets at 600°-700°C.
Claim 3
Dependent Claim 14 words
A process according to claim 1, wherein the natural clay binder comprises plastic kaolinites.
Claim 4
Dependent Claim 15 words
A process according to claim 1, wherein the natural clay binder comprises plastic hydromica varieties.
Claim 5
Dependent Claim 24 words
A process according to claim 1, wherein the pellets are dried at 150°-200°C to a residual moisture content of 20-25% prior to the calcination.
Claim 6
Dependent Claim 51 words
A process according to claim 1, wherein the pellets after the calcination are leached with 1-10% aqueous solution of a sodium compound selected from the group consisting of caustic soda, sodium carbonate, and sodium silicate at 75°-95°C, with subsequent washing of the pellets with water to pH=6-8 and calcination at 350°-450°C.
Claim 7
Dependent Claim 40 words
A process according to claim 5, wherein the pellets are treated after the leaching and before the washing with water with 1-1.5N aqueous solution of a salt selected from the group consisting of calcium chloride, potassium chloride and silver nitrate.
Claim 8
Dependent Claim 29 words
A process according to claim 5, wherein the pellets are dried at 150°-200°C to a residual moisture content of 20-25% after the washing with water and before the calcination.
Claim 9
Dependent Claim 48 words
A process according to claim 1, wherein the pellets are treated after the calcination with 1-1.5N aqueous solution of a salt selected from the group consisting of calcium chloride potassium chloride and silver nitrate, with subsequent washing of the pellets with water to pH=6-8 and calcination at 350°-450°C.
Claim 10
Dependent Claim 18 words
A process according to claim 1 wherein the particle size of said zeolite powder is between 1-5 mcm.
Claim 11
Dependent Claim 20 words
A process according to claim 1 wherein the calcining of the pellets at 600°-700°C is carried out for 12-24 hours.

References Cited (Backward Citations)

US3065054A Cited
US3158579A Cited
US3234147A Cited
US3324047A Cited
US3326797A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-09-07 1980-03-08 1980-09-07 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-09-07 1984-03-08 1984-09-07 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-09-07 1988-03-08 1988-09-07 $7700.00 Window Closed / Lapsed

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