US3976649A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Production of easily dispersible, high tinctorial strength perylene-3,4,9,10-tetracarboxylic acid diimides
Assignee: BASF SE
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Filing: 1974-04-01
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Granted: 1976-08-24
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Expires: 1994-04-01
Abstract
Abstract High tinctorial strength, easily dispersible perylene-3,4,9,10-tetracarboximides and N,N'-dialkylperylene-3,4,9,10-tetracarboximides are produced by introducing a finely ground crude pigment whose primary particle size is not more than 0.05 micron into a primary aliphatic or aromatic amine, into a heterocyclic base, into an aliphatic carboxamide, into a mixture thereof, or into from 75 to 84% by weight sulfuric acid and converting it into pigmentary form at a temperature of from ambient temperature to 160°C. The products are easily dispersible pigments of high tinctorial strength.
Inventors
- 👤 Wolfgang Fabian
- 👤 Klaus Schrempp
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 19:05
CPC Classifications
C; C09; C09B; C09B68/00; C09B68/20; C09B68/24; C09B5/00; C09B5/62; C09B67/00; C09B67/0001; C09B67/0096; C09B68/40; C09B68/44; C09B68/443
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
134 words
In a process for the production in pigmentary form of perylene-3,4,9,10-tetracarboxylic acid diimide or the corresponding N-alkyl diimides of one to four carbon atoms in each alkyl, the improvement for producing a pigment which has high tinctorial strength and is easily dispersible which comprises the steps of: grinding the crude pigment until the mean primary particle size is not more than 0.05 micron; introducing the ground material into a treatment medium which consists essentially of an aliphatic primary amine selected from the group consisting of ethylamine, n-propylamine, n-butylamine, n-hexylamine, ethanolamine, 1-aminopropanol, 3-aminopropanol, β-methoxyethylamine, β-ethoxyethylamine, β-butoxyethylamine, γ-methoxypropylamine, γ-ethoxypropylamine, γ-butoxypropylamine or a mixture of the same; mixing the ground pigment in said medium at a temperature of from ambient temperature to 160°C until the pigment has recrystallized; and then separating the pigment from the treatment medium.
Claim 2
Dependent Claim
134 words
In a process for the production in pigmentary form of perylene-3,4,9,10-tetracarboxylic acid diimide or the corresponding N-alkyl diimides of one to four carbon atoms in each alkyl, the improvement for producing a pigment which has high tinctorial strength and is easily dispersible which comprises the steps of: grinding the crude pigment until the mean primary particle size is not more than 0.05 micron; introducing the ground material into a treatment medium which consists essentially of an aliphatic primary amine selected from the group consisting of ethylamine, n-propylamine, n-butylamine, n-hexylamine, ethanolamine, 1-aminopropanol, 3-aminopropanol, β-methoxyethylamine, β-ethoxyethylamine, β-butoxyethylamine, γ-methoxypropylamine, γ-ethoxypropylamine, γ-butoxypropylamine or a mixture of the same; mixing the ground pigment in said medium at a temperature of from ambient temperature to 160°C until the pigment has recrystallized; and then separating the pigment from the treatment medium.
Claim 3
Dependent Claim
18 words
A process as claimed in claim 1 wherein the treatment is carried out at from 50° to 150°C.
Claim 4
Dependent Claim
25 words
A process as claimed in claim 1 wherein the weight of treatment medium used is from 0.5 to 5 times the weight of crude pigment.
Claim 5
Dependent Claim
16 words
A process as claimed in claim 1 wherein the recrystallized pigment is isolated by freeze drying.
Claim 6
Dependent Claim
17 words
A process as claimed in claim 1 wherein perylene-3,4,9,10-tetracarboxylic acid diimide is used as the crude pigment.
Claim 7
Dependent Claim
17 words
A process as claimed in claim 1 wherein N,N'-dimethylperylene-3,4,9,10-tetracarboxylic acid diimide is used as the crude pigment.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-08-24 | 1980-02-23 | 1980-08-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-08-24 | 1984-02-23 | 1984-08-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-08-24 | 1988-02-23 | 1988-08-24 | $7700.00 | Window Closed / Lapsed |