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US3974245A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing free flowing powder and product

Assignee: GTE Sylvania Inc
•
Filing: 1975-04-25
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Granted: 1976-08-10
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Expires: 1995-04-25
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Abstract

Abstract Free flowing powders such as for flame spray applications are produced by agglomerating finely divided material, classifying the agglomerates to obtain a desired size range, entraining the agglomerates in a carrier gas, feeding the agglomerates through a high temperature plasma reactor to cause at least partial melting of the particles, and collecting the particles in a cooling chamber containing a protective gaseous atmosphere, wherein the particles are solidified.

Inventors

  • 👤 Richard F. Cheney
  • 👤 Charles L. Moscatello
  • 👤 Frederick J. Mower

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 10:49
CPC Classifications
C; C23; C23C; C23C4/00; C23C4/04; B; B22; B22F; B22F1/00; B22F1/06; B22F1/065; B22F1/14; B22F1/148; C23C4/06; C23C4/08

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 200 words
Process for producing a free flowing flame spray powder consisting essentially of substantially spherical particles of an inorganic material having a melting point above 500°C; the particles having an apparent density of at least 40 percent of the theoretical density of the material, a particle size distribution within the range of about 60 micrometers, substantially smooth non-porous surfaces and a Hall flow within the range of from about 9 to 21 seconds; the process comprising: a. entraining powder particles in a carrier gas, said particles consisting essentially of agglomerates of a finely divided particulate of the inorganic material, the agglomerates having a size range of 60 micrometers and 80 percent of the agglomerates having a size range of 30 micrometers, b. feeding the entrained particles through a high temperature reactor having a temperature above the melting point of the highest melting component of the powder material, at a feed rate sufficient to result in the melting of at least the outer surfaces of a substantial portion of the particles, and c. cooling the at least partially melted particle to solidify at least the outer surfaces of the particles prior to their contact with a solid surface or with each other.
Claim 2
Dependent Claim 200 words
Process for producing a free flowing flame spray powder consisting essentially of substantially spherical particles of an inorganic material having a melting point above 500°C; the particles having an apparent density of at least 40 percent of the theoretical density of the material, a particle size distribution within the range of about 60 micrometers, substantially smooth non-porous surfaces and a Hall flow within the range of from about 9 to 21 seconds; the process comprising: a. entraining powder particles in a carrier gas, said particles consisting essentially of agglomerates of a finely divided particulate of the inorganic material, the agglomerates having a size range of 60 micrometers and 80 percent of the agglomerates having a size range of 30 micrometers, b. feeding the entrained particles through a high temperature reactor having a temperature above the melting point of the highest melting component of the powder material, at a feed rate sufficient to result in the melting of at least the outer surfaces of a substantial portion of the particles, and c. cooling the at least partially melted particle to solidify at least the outer surfaces of the particles prior to their contact with a solid surface or with each other.
Claim 3
Dependent Claim 42 words
Process of claim 1 in which the high temperature reactor is a plasma reactor having a temperature within the range of 10,000°F to 30,000°F and in which the powder feed rate through the reactor is from 1/2 to 30 pounds per hour.
Claim 4
Dependent Claim 18 words
Process of claim 2 in which the powder feed rate is from 1/2 to 15 pounds per hour.
Claim 5
Dependent Claim 15 words
Process of claim 1 in which the inorganic material has a melting point above 1800°C.
Claim 6
Dependent Claim 20 words
Process of claim 4 in which the material is selected from the group consisting of molybdenum, tungsten and their alloys.

References Cited (Backward Citations)

US3211548A Cited
US3475158A Cited
US3852061A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-08-10 1980-02-09 1980-08-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-08-10 1984-02-09 1984-08-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-08-10 1988-02-09 1988-08-10 $7700.00 Window Closed / Lapsed

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