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US3974069A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the dehydration of fatty sludge and the recovery of chemicals

Assignee: Individual
•
Filing: 1975-10-20
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Granted: 1976-08-10
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Expires: 1995-10-20
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Abstract

Abstract A process is disclosed for concentrating a fatty sludge precipitated from a fatty and proteinaceous aqueous emulsion by successive addition of hydrolyzable metals salts and alkaline earth salts thereto and subsequently separated from the aqueous portion of the emulsion, comprising acidifying the separated fatty sludge with mineral acid and allowing a supernatant concentrated sludge to form above an aqueous phase. The supernatant concentrated sludge which is formed may be heated preferably to boiling either separately or without separation from the aqueous phase to further concentrate the sludge and produce a fatty acid containing supernatant phase. The chemicals originally used for precipitating the fatty sludge may be recovered from the aqueous phase.

Inventors

  • 👤 Per Oscar Nettli

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 14:06
CPC Classifications
C; C11; C11B; C11B13/00; Y; Y02; Y02W; Y02W30/00; Y02W30/50; Y02W30/74; Y10; Y10S; Y10S530/00; Y10S530/859

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 164 words
A process for concentrating a precipitated stabilized fatty sludge which has been recovered from a fatty, proteinaceous, aqueous emulsion waste effluent, said stabilized sludge being obtained by adding to the effluent an acid hydrolyzing metal salt in an amount sufficient to bind organic material present into a complex and reducing the pH to below 5, whereafter the formed complex is precipitated, in the presence of alkaline earth ions by raising the pH to 6-9, whereafter the thus formed stabilized sludge is separated, which process consists essentially of the steps of acidifying said stabilized sludge to a pH less than 2, to thereby form a first aqueous phase and a supernatant, concentrated fatty phase which is separated from said first aqueous phase, heating said separated, concentrated fatty phase to form thereby a free fatty acid-containing liquid phase and a second aqueous phase which contains the precipitation chemicals of said stabilized fatty sludge, and separating said free fatty acid-containing liquid phase from said second aqueous phase.
Claim 2
Dependent Claim 164 words
A process for concentrating a precipitated stabilized fatty sludge which has been recovered from a fatty, proteinaceous, aqueous emulsion waste effluent, said stabilized sludge being obtained by adding to the effluent an acid hydrolyzing metal salt in an amount sufficient to bind organic material present into a complex and reducing the pH to below 5, whereafter the formed complex is precipitated, in the presence of alkaline earth ions by raising the pH to 6-9, whereafter the thus formed stabilized sludge is separated, which process consists essentially of the steps of acidifying said stabilized sludge to a pH less than 2, to thereby form a first aqueous phase and a supernatant, concentrated fatty phase which is separated from said first aqueous phase, heating said separated, concentrated fatty phase to form thereby a free fatty acid-containing liquid phase and a second aqueous phase which contains the precipitation chemicals of said stabilized fatty sludge, and separating said free fatty acid-containing liquid phase from said second aqueous phase.
Claim 3
Dependent Claim 21 words
The process of claim 1, wherein acidifying is affected by the addition of acid effluent from the decomposition of soap stock.
Claim 4
Dependent Claim 28 words
The process of claim 2, wherein said second aqueous phase containing the precipitating chemicals, after separation of said free fatty acid-containing phase therefrom is reused as a precipitant.
Claim 5
Dependent Claim 27 words
The process of claim 1, wherein said second aqueous phase containing the precipitating chemicals, after separation of said free fatty acid-containing phase therefrom, is reused as precipitant.
Claim 6
Dependent Claim 15 words
The process of claim 1 wherein said effluent is the effluent from a margarine factory.
Claim 7
Dependent Claim 16 words
The process of claim 1 wherein said effluent is the effluent from a meat/bone meal factory.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-08-10 1980-02-09 1980-08-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-08-10 1984-02-09 1984-08-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-08-10 1988-02-09 1988-08-10 $7700.00 Window Closed / Lapsed

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