US3971631A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Pelletizing alkali metal polysilicates
Assignee: JM Huber Corp
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Filing: 1974-08-26
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Granted: 1976-07-27
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Expires: 1994-08-26
Abstract
Abstract A method for producing alkali metal polysilicates is disclosed. Polysilicates, produced by hydrothermally reacting an aqueous dispersion of finely-divided silica and an alkali metal hydroxide are spray dried and the solid product is fractured and pulverized. The fractured mass is then pelletized employing the solubility of the polysilicates to form a free-flowing product having a continuous, even surface. Pelletization may be effected with or without the use of water and/or binders.
Inventors
- 👤 Guillermo Almagro
- 👤 Orlando L. Bertorelli
- 👤 Robert K. Mays
- 👤 Lloyd E. Williams
- 👤 Howard F. Zimmerman, Jr.
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 00:39
CPC Classifications
C; C11; C11D; C11D3/00; C11D3/02; C11D3/04; C11D3/08; B; B01; B01J; B01J2/00; B01J2/02; C01; C01B; C01B33/00; C01B33/20; C01B33/32; C01B33/325; C01D; C01D7/00; C01D7/42
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
94 words
A method for pelletizing finely divided alkali metal polysilicate particles comprising the steps of: 1. spray drying a silicate product by passing an aqueous mixture of silicate particles into the upper portion of a drying chamber and dispersing said mixture in the form of fine droplets in said chamber; the temperature of the inlet air to the spray drier being of the order of from about 400° to 1000° F.; whereby said droplets form minute hollow polysilicate microspheres; 2. collecting said spherical polysilicate droplets from the spray dryer and passing to a milling apparatus;
Claim 2
Independent Claim
94 words
A method for pelletizing finely divided alkali metal polysilicate particles comprising the steps of: 1. spray drying a silicate product by passing an aqueous mixture of silicate particles into the upper portion of a drying chamber and dispersing said mixture in the form of fine droplets in said chamber; the temperature of the inlet air to the spray drier being of the order of from about 400° to 1000° F.; whereby said droplets form minute hollow polysilicate microspheres; 2. collecting said spherical polysilicate droplets from the spray dryer and passing to a milling apparatus;
Claim 3
Dependent Claim
48 words
fracturing and pulverizing said hollow spheres in said milling apparatus to the extent that the density of the resulting fractured particles is increased to at least 25 lbs/cubic foot, and particles having sharp and uneven surfaces are formed; 4. passing said milled product to a rotating pelletizer vessel;
Claim 4
Dependent Claim
48 words
fracturing and pulverizing said hollow spheres in said milling apparatus to the extent that the density of the resulting fractured particles is increased to at least 25 lbs/cubic foot, and particles having sharp and uneven surfaces are formed; 4. passing said milled product to a rotating pelletizer vessel;
Claim 5
Dependent Claim
109 words
rotating said product in said rotating vessel at a temperature of 30°-150°C. while adding sufficient water thereto to increase the moisture content of the rotating product to 30%, said rotation and moisture content being sufficient to dissolve the outer surfaces of said milled particles and effect incipient fusion of two or more of said particles to form a plurality of free-flowing particles of the pelletized material having continuously even surfaces, a bulk density of at least 55 pounds per cubic foot and a particle size of minus 8 plus 100 mesh; and 6. adding additional dry milled product to the resulting particles to reduce the moisture content to 25%.
Claim 6
Dependent Claim
109 words
rotating said product in said rotating vessel at a temperature of 30°-150°C. while adding sufficient water thereto to increase the moisture content of the rotating product to 30%, said rotation and moisture content being sufficient to dissolve the outer surfaces of said milled particles and effect incipient fusion of two or more of said particles to form a plurality of free-flowing particles of the pelletized material having continuously even surfaces, a bulk density of at least 55 pounds per cubic foot and a particle size of minus 8 plus 100 mesh; and 6. adding additional dry milled product to the resulting particles to reduce the moisture content to 25%.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-07-27 | 1980-01-26 | 1980-07-27 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-07-27 | 1984-01-26 | 1984-07-27 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-07-27 | 1988-01-26 | 1988-07-27 | $7700.00 | Window Closed / Lapsed |