← Back to Patent Explorer
US3970485A Expired / Lapsed US ⏱️ 0.0 years remaining

Binder and lubricant removal from cobalt-rare earth alloys

Assignee: Hitachi Metals International Ltd
•
Filing: 1975-01-20
•
Granted: 1976-07-20
•
Expires: 1995-01-20
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract An organic binder or lubricant in a pressed or compacted green body formed of cobalt-rare earth intermetallic particles is substantially removed from the green body before the carbon can react with the rare earth during sintering. This is accomplished by exposing the green body to a temperature of about 100 DEG to 300 DEG C in a hydrogen-containing atmosphere. The hydrogen reacts with the organic binder or lubricant which allows the resulting organic molecules to volatilize from the green body. The green body is then sintered after which it is cooled to room temperature.

Inventors

  • 👤 Manfred Doser

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 17:25
CPC Classifications
H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/032; H01F1/04; H01F1/047; H01F1/053; H01F1/055; H01F1/0555; H01F1/0557

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 144 words
A process for producing a cobalt-rare earth intermetallic product having substantially stable permanent magnet properties which comprises providing an alloy of cobalt and rare earth metal in particulate form, said cobalt and rare earth metal being used in proportions substantially corresponding to those desired in a final sintered product, mixing an organic binder material with said particulate alloy, pressing said particulate alloy into a green body, subjecting said green body to a bake cycle in (a hydrogen-containing) an atmosphere containing 1 to 100% by volume hydrogen at an intermediate temperature (at which) of between 100° and 500°C for about a half-hour whereby the hydrogen reacts with the molecules forming the organic binder and the resulting molecules volatilize from the green body, and (maintaining said intermediate temperature until the bulk of the organic binder molecules have been volatilized from said body.) thereafter sintering said body.
Claim 2
Dependent Claim 144 words
A process for producing a cobalt-rare earth intermetallic product having substantially stable permanent magnet properties which comprises providing an alloy of cobalt and rare earth metal in particulate form, said cobalt and rare earth metal being used in proportions substantially corresponding to those desired in a final sintered product, mixing an organic binder material with said particulate alloy, pressing said particulate alloy into a green body, subjecting said green body to a bake cycle in (a hydrogen-containing) an atmosphere containing 1 to 100% by volume hydrogen at an intermediate temperature (at which) of between 100° and 500°C for about a half-hour whereby the hydrogen reacts with the molecules forming the organic binder and the resulting molecules volatilize from the green body, and (maintaining said intermediate temperature until the bulk of the organic binder molecules have been volatilized from said body.) thereafter sintering said body.
Claim 3
Dependent Claim 17 words
The process of claim 1 wherein the intermediate temperature is within a range of 100° to 300°C.
Claim 4
Dependent Claim 12 words
The process of claim 2 in which the temperature is about 250°C.
Claim 5
Dependent Claim 12 words
The process of claim 1 in which the rare earth is samarium.
Claim 6
Dependent Claim 17 words
The process of claim 1 in which the rare earth is a mixture of samarium and cerium-mischmetal.
Claim 7
Dependent Claim 17 words
The process of claim 1 in which the rare earth is a mixture of samarium and praseodymium.
Claim 8
Dependent Claim 17 words
The process of claim 1 in which the rare earth is a mixture of samarium and gadolinium.
Claim 9
Dependent Claim 17 words
The process of claim 1 in which the rare earth is a mixture of samarium and neodymium.

References Cited (Backward Citations)

US3607462A Cited
US3728110A Cited
US3681151A Cited
US3684593A Cited
US3755007A Cited
US3785881A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-07-20 1980-01-19 1980-07-20 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-07-20 1984-01-19 1984-07-20 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-07-20 1988-01-19 1988-07-20 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag