US3970485A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Binder and lubricant removal from cobalt-rare earth alloys
Assignee: Hitachi Metals International Ltd
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Filing: 1975-01-20
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Granted: 1976-07-20
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Expires: 1995-01-20
Abstract
Abstract An organic binder or lubricant in a pressed or compacted green body formed of cobalt-rare earth intermetallic particles is substantially removed from the green body before the carbon can react with the rare earth during sintering. This is accomplished by exposing the green body to a temperature of about 100 DEG to 300 DEG C in a hydrogen-containing atmosphere. The hydrogen reacts with the organic binder or lubricant which allows the resulting organic molecules to volatilize from the green body. The green body is then sintered after which it is cooled to room temperature.
Inventors
- 👤 Manfred Doser
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-26 17:25
CPC Classifications
H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/032; H01F1/04; H01F1/047; H01F1/053; H01F1/055; H01F1/0555; H01F1/0557
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
144 words
A process for producing a cobalt-rare earth intermetallic product having substantially stable permanent magnet properties which comprises providing an alloy of cobalt and rare earth metal in particulate form, said cobalt and rare earth metal being used in proportions substantially corresponding to those desired in a final sintered product, mixing an organic binder material with said particulate alloy, pressing said particulate alloy into a green body, subjecting said green body to a bake cycle in (a hydrogen-containing) an atmosphere containing 1 to 100% by volume hydrogen at an intermediate temperature (at which) of between 100° and 500°C for about a half-hour whereby the hydrogen reacts with the molecules forming the organic binder and the resulting molecules volatilize from the green body, and (maintaining said intermediate temperature until the bulk of the organic binder molecules have been volatilized from said body.) thereafter sintering said body.
Claim 2
Dependent Claim
144 words
A process for producing a cobalt-rare earth intermetallic product having substantially stable permanent magnet properties which comprises providing an alloy of cobalt and rare earth metal in particulate form, said cobalt and rare earth metal being used in proportions substantially corresponding to those desired in a final sintered product, mixing an organic binder material with said particulate alloy, pressing said particulate alloy into a green body, subjecting said green body to a bake cycle in (a hydrogen-containing) an atmosphere containing 1 to 100% by volume hydrogen at an intermediate temperature (at which) of between 100° and 500°C for about a half-hour whereby the hydrogen reacts with the molecules forming the organic binder and the resulting molecules volatilize from the green body, and (maintaining said intermediate temperature until the bulk of the organic binder molecules have been volatilized from said body.) thereafter sintering said body.
Claim 3
Dependent Claim
17 words
The process of claim 1 wherein the intermediate temperature is within a range of 100° to 300°C.
Claim 4
Dependent Claim
12 words
The process of claim 2 in which the temperature is about 250°C.
Claim 5
Dependent Claim
12 words
The process of claim 1 in which the rare earth is samarium.
Claim 6
Dependent Claim
17 words
The process of claim 1 in which the rare earth is a mixture of samarium and cerium-mischmetal.
Claim 7
Dependent Claim
17 words
The process of claim 1 in which the rare earth is a mixture of samarium and praseodymium.
Claim 8
Dependent Claim
17 words
The process of claim 1 in which the rare earth is a mixture of samarium and gadolinium.
Claim 9
Dependent Claim
17 words
The process of claim 1 in which the rare earth is a mixture of samarium and neodymium.
References Cited (Backward Citations)
US3607462A
Cited
US3728110A
Cited
US3681151A
Cited
US3684593A
Cited
US3755007A
Cited
US3785881A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-07-20 | 1980-01-19 | 1980-07-20 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-07-20 | 1984-01-19 | 1984-07-20 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-07-20 | 1988-01-19 | 1988-07-20 | $7700.00 | Window Closed / Lapsed |