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US3963586A Expired / Lapsed US ⏱️ 0.0 years remaining

Extractive distillation of a dimethyl carbonate feed with water

Assignee: SnamProgetti SpA
•
Filing: 1974-10-25
•
Granted: 1976-06-15
•
Expires: 1994-10-25
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Abstract

Abstract Dimethyl carbonate is separated from a mixture thereof with methyl alcohol and water through an extractive distillation process wherein water is utilized as the solvent.

Inventors

  • 👤 Alessandro Ginnasi
  • 👤 Giovanni Passoni

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 22:34
CPC Classifications
C; C07; C07C; C07C68/00; C07C68/08

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 104 words
The process of separating dimethyl carbonate from a mixture thereof with methyl alcohol and water through an extractive distillation comprising the steps of feeding said mixture to an intermediate zone of an extractive distillation column, feeding solvent water in an amount equal to at least 10 times the column reflux rate to said column at a point in proximity to its top, withdrawing a stream of methyl alcohol and water from the bottom of said column, withdrawing from the top of said column a stream having an organic phase containing dimethylcarbonate and an aqueous phase, and separating said organic phase from the aqueous phase.
Claim 2
Dependent Claim 104 words
The process of separating dimethyl carbonate from a mixture thereof with methyl alcohol and water through an extractive distillation comprising the steps of feeding said mixture to an intermediate zone of an extractive distillation column, feeding solvent water in an amount equal to at least 10 times the column reflux rate to said column at a point in proximity to its top, withdrawing a stream of methyl alcohol and water from the bottom of said column, withdrawing from the top of said column a stream having an organic phase containing dimethylcarbonate and an aqueous phase, and separating said organic phase from the aqueous phase.

References Cited (Backward Citations)

US2517965A Cited
US2687425A Cited
US2787631A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-06-15 1979-12-15 1980-06-15 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-06-15 1983-12-15 1984-06-15 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-06-15 1987-12-15 1988-06-15 $7700.00 Window Closed / Lapsed

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