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US3963434A Expired / Lapsed US ⏱️ 0.0 years remaining

Carboxymethylated cotton fabric with improved conditioned and wet wrinkle recovery by reaction with propylene or ethylene carbonate

Assignee: United States Department of Agriculture
•
Filing: 1975-07-23
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Granted: 1976-06-15
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Expires: 1995-07-23
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Abstract

Abstract Partially carboxymethylated-cotton fabric prepared by a non-aqueous procedure is reacted with either ethylene carbonate or propylene carbonate in a heated, evacuated oven. The product of either reaction is a fabric with high conditioned and high wet wrinkle recovery.

Inventors

  • 👤 Truman L. Ward
  • 👤 Ruth R. Benerito
  • 👤 Dorothy M. Perrier

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 01:25
CPC Classifications
D; D06; D06M; D06M13/00; D06M13/10; D06M13/224; D06M13/232; Y; Y10; Y10S; Y10S8/00; Y10S8/11

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 139 words
A process for imparting high conditioned (dry) and high wet wrinkle recovery to partially carboxymethylated-cotton fabric, the process comprising: a. impregnating a cotton fabric which has been carboxymethylated to a degree of substitution of about from 0.1 to 0.3 by a non-aqueous procedure, with a neat heterocyclic carbonate selected from the group consisting of ethylene carbonate, propylene carbonate, and a mixture of ethylene and propylene carbonate, to a pickup of about 100%, b. placing the wet, impregnated CMC fabric in a vacuum oven preheated to a temperature of about from 160° to 180° , c. evacuating the oven to obtain a pressure of about 35 mm of mercury, d. maintaining the temperature and vacuum for about from 30 to 120 minutes to obtain reaction, and e. releasing the vacuum and washing the reacted fabric to remove all unreacted material.
Claim 2
Dependent Claim 139 words
A process for imparting high conditioned (dry) and high wet wrinkle recovery to partially carboxymethylated-cotton fabric, the process comprising: a. impregnating a cotton fabric which has been carboxymethylated to a degree of substitution of about from 0.1 to 0.3 by a non-aqueous procedure, with a neat heterocyclic carbonate selected from the group consisting of ethylene carbonate, propylene carbonate, and a mixture of ethylene and propylene carbonate, to a pickup of about 100%, b. placing the wet, impregnated CMC fabric in a vacuum oven preheated to a temperature of about from 160° to 180° , c. evacuating the oven to obtain a pressure of about 35 mm of mercury, d. maintaining the temperature and vacuum for about from 30 to 120 minutes to obtain reaction, and e. releasing the vacuum and washing the reacted fabric to remove all unreacted material.
Claim 3
Dependent Claim 12 words
The process of claim 1 wherein the heterocyclic carbonate is ethylene carbonate.
Claim 4
Dependent Claim 12 words
The process of claim 1 wherein the heterocyclic carbonate is propylene carbonate.
Claim 5
Dependent Claim 17 words
The process of claim 1 wherein the heterocyclic carbonate is a mixture of ethylene and propylene carbonate.

References Cited (Backward Citations)

US3617197A Cited
US3918899A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-06-15 1979-12-15 1980-06-15 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-06-15 1983-12-15 1984-06-15 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-06-15 1987-12-15 1988-06-15 $7700.00 Window Closed / Lapsed

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