US3960792A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Plastic foam
Assignee: Dow Chemical Co
•
Filing: 1971-09-02
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Granted: 1976-06-01
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Expires: 1991-09-02
Abstract
Abstract Dimensionally stable polystyrene foams are prepared by using a mixture of blowing agents which has a diffusion rate through the polystyrene approximating that of air.
Inventors
- 👤 Masao Nakamura
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 03:57
CPC Classifications
C; C08; C08J; C08J9/00; C08J9/04; C08J9/12; C08J9/14; C08J2325/00; C08J2325/02; C08J2325/04; C08J2325/06; Y; Y10; Y10S; Y10S264/00; Y10S264/05; Y10S521/00; Y10S521/91
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
160 words
In a process for the preparation of an expanded closed cell polystyrene resin which includes incorporated within said polystyrene resin a volatile fluid foaming agent which is a non-solvent for the polystyrene resin, subsequently expanding the polystyrene resin containing the fluid foaming agent by subjecting the expandable resin containing the fluid foaming agent to a pressure sufficiently low to permit the polystyrene resin to expand when the polystyrene resin containing the fluid foaming agent is in a heat plastified condition, and subsequently cooling the expanded polystyrene resin to form a closed cell polystyrene resin body, the improvement which comprises preparing a dimensionally stable expanded closed cell body by employing as the fluid foaming agent a volatile material which has a diffusion rate through the polystyrene resin which is about 0.75 to 6 times the diffusion rate of air through polystyrene resin, and the foaming agent consisting essentially of a mixture of at least two compounds having carbon chemically combined therein.
Claim 2
Dependent Claim
160 words
In a process for the preparation of an expanded closed cell polystyrene resin which includes incorporated within said polystyrene resin a volatile fluid foaming agent which is a non-solvent for the polystyrene resin, subsequently expanding the polystyrene resin containing the fluid foaming agent by subjecting the expandable resin containing the fluid foaming agent to a pressure sufficiently low to permit the polystyrene resin to expand when the polystyrene resin containing the fluid foaming agent is in a heat plastified condition, and subsequently cooling the expanded polystyrene resin to form a closed cell polystyrene resin body, the improvement which comprises preparing a dimensionally stable expanded closed cell body by employing as the fluid foaming agent a volatile material which has a diffusion rate through the polystyrene resin which is about 0.75 to 6 times the diffusion rate of air through polystyrene resin, and the foaming agent consisting essentially of a mixture of at least two compounds having carbon chemically combined therein.
Claim 3
Dependent Claim
22 words
The method of claim 1 wherein the expanded polystyrene resin body is cured at an elevated temperature in an atmosphere of air.
Claim 4
Dependent Claim
47 words
The method of claim 2 wherein said expanded polystyrene resin body is cured in an atmosphere of air at a temperature between about 160°F. and 180°F. until at least a major portion of the fluid foaming agent has diffused from the foam and is replaced by air.
Claim 5
Dependent Claim
132 words
In a process for the preparation of an expanded closed cell polystyrene which is a solid polymer which includes incorporating within the polystyrene a volatile fluid foaming agent, subsequently expanding the polystyrene containing the fluid foaming agent which is a non-solvent for the polystyrene by subjecting heat plastified expandable polystyrene containing the fluid foaming agent to a pressure sufficiently low to permit the polystyrene to expand and subsequently cooling the resultant expanded mass to form a closed cell polystyrene body, the improvement which comprises employing as a volatile fluid foaming agent a volatile material, the foaming agent consisting essentially of a mixture of compounds each containing chemically combined carbon, and the mixture having a transmission rate through polystyrene which is about 0.75 to 3 times the transmission rate of air through polystyrene.
Claim 6
Dependent Claim
132 words
In a process for the preparation of an expanded closed cell polystyrene which is a solid polymer which includes incorporating within the polystyrene a volatile fluid foaming agent, subsequently expanding the polystyrene containing the fluid foaming agent which is a non-solvent for the polystyrene by subjecting heat plastified expandable polystyrene containing the fluid foaming agent to a pressure sufficiently low to permit the polystyrene to expand and subsequently cooling the resultant expanded mass to form a closed cell polystyrene body, the improvement which comprises employing as a volatile fluid foaming agent a volatile material, the foaming agent consisting essentially of a mixture of compounds each containing chemically combined carbon, and the mixture having a transmission rate through polystyrene which is about 0.75 to 3 times the transmission rate of air through polystyrene.
Claim 7
Dependent Claim
172 words
In a process for the preparation of an expanded closed cell polystyrene resin which includes incorporated within said polystyrene resin a volatile fluid foaming agent which is a non-solvent for the polystyrene resin, subsequently expanding the polystyrene resin containing the fluid foaming agent by subjecting the expandable resin containing the fluid foaming agent to a pressure sufficiently low to permit the polystyrene resin to expand when the polystyrene resin containing the fluid foaming agent is in a heat plastified condition, and subsequently cooling the expanded polystyrene resin to form a closed cell polystyrene resin body, the improvement which comprises preparing a dimensionally stable expanded closed cell body by employing as the fluid foaming agent a volatile material which has a diffusion rate through the polystyrene resin which is about 0.75 to 6 times the diffusion rate of air through polystyrene resin, and the foaming agent consisting essentially of a mixture which comprises from 40 to 60 percent by weight of methyl chloride and from 60 to 40 percent by weight of dichlorodifluoromethane.
Claim 8
Dependent Claim
172 words
In a process for the preparation of an expanded closed cell polystyrene resin which includes incorporated within said polystyrene resin a volatile fluid foaming agent which is a non-solvent for the polystyrene resin, subsequently expanding the polystyrene resin containing the fluid foaming agent by subjecting the expandable resin containing the fluid foaming agent to a pressure sufficiently low to permit the polystyrene resin to expand when the polystyrene resin containing the fluid foaming agent is in a heat plastified condition, and subsequently cooling the expanded polystyrene resin to form a closed cell polystyrene resin body, the improvement which comprises preparing a dimensionally stable expanded closed cell body by employing as the fluid foaming agent a volatile material which has a diffusion rate through the polystyrene resin which is about 0.75 to 6 times the diffusion rate of air through polystyrene resin, and the foaming agent consisting essentially of a mixture which comprises from 40 to 60 percent by weight of methyl chloride and from 60 to 40 percent by weight of dichlorodifluoromethane.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-06-01 | 1979-12-01 | 1980-06-01 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-06-01 | 1983-12-01 | 1984-06-01 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-06-01 | 1987-12-01 | 1988-06-01 | $7700.00 | Window Closed / Lapsed |