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US3959014A Expired / Lapsed US ⏱️ 0.0 years remaining

Method to produce a protective oxide on the surface of positive nickel electrodes for galvanic cells

Assignee: Siemens AG
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Filing: 1972-12-14
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Granted: 1976-05-25
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Expires: 1992-12-14
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Abstract

Abstract The present invention relates to a method for the development of a protective oxide on the surface of porous, positive Mi-electrodes for galvanic cells with alkaline electrolyte.

Inventors

  • 👤 Martin Bauer
  • 👤 Henning Ewe
  • 👤 Eduard Justi

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 14:47
CPC Classifications
H; H01; H01M; H01M4/00; Y; Y10; Y10T; Y10T137/00; Y10T137/1624; Y10T137/1797; Y10T137/1819

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 117 words
The method for the production of a thin protective layer of nickel oxide on the surface of a porous nickel electrode for use in a galvanic cell comprising contacting the nickel electrode to a chemical or electro-chemical processing to form a film of 5-30 molecular layers thickness of nickel hydroxide thereon, contacting said electrode with an oxygen containing atmosphere to decompose the nickel hydroxide layer to the desired nickel oxide, contacting the nickel electrode with an oxygen containing atmosphere at a temperature in the range of 160°-400°C and for a period of time of at least half an hour and thereafter recovering a nickel electrode having a thin protective film of nickel oxide on the surface thereof.
Claim 2
Independent Claim 117 words
The method for the production of a thin protective layer of nickel oxide on the surface of a porous nickel electrode for use in a galvanic cell comprising contacting the nickel electrode to a chemical or electro-chemical processing to form a film of 5-30 molecular layers thickness of nickel hydroxide thereon, contacting said electrode with an oxygen containing atmosphere to decompose the nickel hydroxide layer to the desired nickel oxide, contacting the nickel electrode with an oxygen containing atmosphere at a temperature in the range of 160°-400°C and for a period of time of at least half an hour and thereafter recovering a nickel electrode having a thin protective film of nickel oxide on the surface thereof.
Claim 3
Dependent Claim 12 words
The method in accordance with claim 1, wherein the atmosphere is air.
Claim 4
Dependent Claim 14 words
The method in accordance with claim 1 wherein the atmosphere is substantially pure oxygen.
Claim 5
Dependent Claim 37 words
The method in accordance with claim 1, wherein the atmosphere is substantially pure oxygen and the temperature employed is in the range 160°-220°C and said contacting is carried out in the presence of a silver containing catalyst.

References Cited (Backward Citations)

SU179361A1 Cited
SU244453A1 Cited
SU169618A1 Cited
US3436267A Cited
US3582403A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-05-25 1979-11-24 1980-05-25 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-05-25 1983-11-24 1984-05-25 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-05-25 1987-11-24 1988-05-25 $7700.00 Window Closed / Lapsed

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