US3957671A
Expired / Lapsed
US
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Acid mix compositions containing benzoic acid
Assignee: Procter and Gamble Co
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Filing: 1974-11-13
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Granted: 1976-05-18
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Expires: 1994-11-13
Abstract
Abstract Low viscosity detergent acid mixes are prepared by reacting an ethoxylated alcohol, alkyl benzene, fatty alcohol or other sulfatable detergent precursor with a sulfating agent in the presence of benzoic acid. Benzoic acid does not form a sulfonate in the composition.
Inventors
- 👤 John A. Sagel
- 👤 Clarence Edward Weber
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-27 19:13
CPC Classifications
C; C11; C11D; C11D1/00; C11D1/02; C11D1/12; C11D1/29; C11D3/00; C11D3/16; C11D3/20; C11D3/2075
Claims Analysis
Total Claims: 13
Claim 1
Independent Claim
58 words
An acid mix having a low viscosity comprising: a. a member selected from the group consisting of alkyl benzene sulfonic acid, alkyl ether sulfuric acid, fatty alcohol sulfuric acids, α-olefin sulfonic acids, and α-sulfocarboxylic acids and the esters of α-sulfocarboxylic acids, and mixtures thereof; and b. an effective amount of benzoic acid to lower the acid mix viscosity.
Claim 2
Dependent Claim
58 words
An acid mix having a low viscosity comprising: a. a member selected from the group consisting of alkyl benzene sulfonic acid, alkyl ether sulfuric acid, fatty alcohol sulfuric acids, α-olefin sulfonic acids, and α-sulfocarboxylic acids and the esters of α-sulfocarboxylic acids, and mixtures thereof; and b. an effective amount of benzoic acid to lower the acid mix viscosity.
Claim 3
Dependent Claim
25 words
A composition in accordance with claim 1 wherein the weight ratio of component (a) to the benzoic acid is from about 100:1 to about 1:1.
Claim 4
Dependent Claim
11 words
A composition in accordance with claim 2 further comprising sulfuric acid.
Claim 5
Dependent Claim
25 words
A composition in accordance with claim 2 wherein the weight ratio of component (a) to the benzoic acid is from about 50:1 to about 3:2.
Claim 6
Dependent Claim
35 words
The composition of claim 4 wherein component (a) is an alkyl ether sulfuric acid having an alkyl radical with from 8 to 24 carbon atoms and the degree of ethoxylation is from 1 to 30.
Claim 7
Dependent Claim
264 words
A composition in accordance with claim 5 wherein the alkyl ether sulfuric acid has an alkyl chain length average varying between 12 and 16 and the average degree of ethoxylation of said mixture varying between 1 and 4 moles of ethylene oxide, said mixture comprising: a. from about 0 to 10 percent by weight of said alkyl ether sulfuric acid mixture of compounds containing 12 or 13 carbon atoms in the alkyl radical; b. from about 50 to 100 percent by weight of said alkyl ether sulfuric acid mixture of compounds containing 14 or 15 carbon atoms in the alkyl radical; c. from about 0 to 45 percent by weight of said alkyl ether sulfuric acid mixture of compounds containing 16 or 17 carbon atoms in the alkyl radical; d. from about 0 to 10 percent by weight of said alkyl ether sulfuric acid mixture of compounds containing 18 or 19 carbon atoms in the alkyl radical; e. from about 0 to 30 percent by weight of said alkyl ether sulfuric acid mixture of compounds having a degree of ethoxylation of zero; f. from about 45 to 95 percent by weight of said alkyl ether sulfuric acid mixture of compounds having a degree of ethoxylation of from 1 to 4; g. from about 5 to 25 percent by weight of said alkyl ether sulfuric acid mixture of compounds having a degree of ethoxylation of from 5 to 8; h. from about 0 to 15 percent by weight of said alkyl ether sulfuric acid mixture of compounds having a degree of ethoxylation greater than 8.
Claim 8
Dependent Claim
18 words
The composition of claim 4 wherein the alkyl benzene has from 9-15 carbon atoms in the alkyl radical.
Claim 9
Dependent Claim
16 words
The composition of claim 7 wherein the mean alkyl chain length is between 11 and 12.
Claim 10
Dependent Claim
20 words
The composition of claim 4 wherein the fatty alcohol contains from 8 to 24 carbon atoms in the alkyl radical.
Claim 11
Dependent Claim
20 words
The composition of claim 4 wherein the α-sulfocarboxylic acid has from 8 to 20 carbon atoms in the alkyl radical.
Claim 12
Dependent Claim
20 words
The composition of claim 4 wherein the α-olefin sulfonate has from 10 to 24 carbon atoms in the alkyl radical.
Claim 13
Dependent Claim
31 words
The composition of claim 4 wherein the α-sulfocarboxylic acid ester has from 8 to 20 carbon atoms in the acid radical and 1 to 14 carbon atoms in the alcohol radical.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-05-18 | 1979-11-17 | 1980-05-18 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-05-18 | 1983-11-17 | 1984-05-18 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-05-18 | 1987-11-17 | 1988-05-18 | $7700.00 | Window Closed / Lapsed |