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US3953260A Expired / Lapsed US ⏱️ 0.0 years remaining

Gossypol, an abundant, low-cost iron deactivator, pot-life extender, and processing aid for HTPB propellants

Assignee: United States Department of the Navy
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Filing: 1975-05-23
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Granted: 1976-04-27
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Expires: 1995-05-23
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Abstract

Abstract In a method wherein propellant ingredients including a hydroxy terminated binder, an isocyanate curative therefor and transition metal compounds or traces thereof are mixed, worked into a suitable container and allowed to cure, gossypol is used to prolong the potlife of the propellant mix. Gossypol is dissolved in a portion of the hydroxy terminated binder material and the solution is utilized as a portion of the total binder. Final formulations containing from 0.02 to 0.1 weight percent gossypol are preferred although more gossypol may be used.

Inventors

  • 👤 John D. Braun
  • 👤 M. Frank Pickett
  • 👤 Howard W. Gerrish, Jr.
  • 👤 Hans B. Jonassen

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 15:36
CPC Classifications
C; C08; C08G; C08G18/00; C08G18/06; C08G18/28; C08G18/67; C08G18/69; C06; C06B; C06B23/00; C06B23/009; C08G18/08; C08G18/089

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 50 words
In a method for mixing propellants comprising the steps of mixing solid particles with a hydroxy terminated polymeric binder, adding an isocyanate curative, working the resulting mixture into a suitable container and allowing it to cure, the improvement residing in adding gossypol to the mix to increase its pot life.
Claim 2
Dependent Claim 50 words
In a method for mixing propellants comprising the steps of mixing solid particles with a hydroxy terminated polymeric binder, adding an isocyanate curative, working the resulting mixture into a suitable container and allowing it to cure, the improvement residing in adding gossypol to the mix to increase its pot life.
Claim 3
Dependent Claim 26 words
A method according to claim 1 wherein an amount of gossypol sufficient to yield a final mix containing 0.02 to 0.1 weight percent gossypol is added.
Claim 4
Dependent Claim 19 words
A method according to claim 1 wherein the gossypol added is in the form of a gossypol-acetic acid complex.
Claim 5
Dependent Claim 20 words
A method according to claim 1 wherein at least a portion of said solid particles is a transition metal compound.
Claim 6
Dependent Claim 15 words
A method according to claim 4 wherein said transition metal compound is an iron compound.
Claim 7
Dependent Claim 14 words
A method according to claim 5 wherein said iron compound is yellow iron oxide.
Claim 8
Dependent Claim 22 words
A method according to claim 1 wherein gossypol is used as a processing aid in propellant, reducing end-of-mix viscosity in said propellant.

References Cited (Backward Citations)

US3695952A Cited
US3867354A Cited
US3801385A Cited
US3888707A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-04-27 1979-10-27 1980-04-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-04-27 1983-10-27 1984-04-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-04-27 1987-10-27 1988-04-27 $7700.00 Window Closed / Lapsed

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