US3935023A
Expired / Lapsed
US
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Alumina dispersions
Assignee: PQ Corp
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Filing: 1974-10-08
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Granted: 1976-01-27
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Expires: 1994-10-08
Abstract
Abstract Stable aqueous dispersions of alumina are formed at concentrations of above about 18% to about 26% on a weight basis by dispersing alumina in a hydrochloric acid solution where the Al 2 O 3 /HCl parts by weight ratio is maintained between 54 and 65 pbw of Al 2 O 3 /l pbw of HCl.
Inventors
- 👤 Mahlon Robert Derolf
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 08:51
CPC Classifications
D; D21; D21H; D21H27/00; C; C09; C09D; C09D17/00; D21H19/00; D21H19/36; D21H19/38; D21H19/385; D21H5/00; D21H5/0072
Claims Analysis
Total Claims: 22
Claim 1
Independent Claim
106 words
A method of preparing stable aqueous dispersions of alumina at concentrations of about 18 to 26% Al 2 O 3 onn a weight basis, consisting essentially of: 1. preparing an aqueous solution of hydrochloric acid, 2. controlling the temperature below the boiling point of the dispersion, 3. maintaining the pressure between 0.5 to 5 atmospheres, 4. adding alumina to said aqueous solution such that the weight ratio of alumina to HCl is 53 to 66 parts alumina to 1 part HCl and the Al 2 O 3 is 18 to 26% of the total mixture, and 5. simultaneously agitating said mixture to obtain the desired dispersion.
Claim 2
Independent Claim
106 words
A method of preparing stable aqueous dispersions of alumina at concentrations of about 18 to 26% Al 2 O 3 onn a weight basis, consisting essentially of: 1. preparing an aqueous solution of hydrochloric acid, 2. controlling the temperature below the boiling point of the dispersion, 3. maintaining the pressure between 0.5 to 5 atmospheres, 4. adding alumina to said aqueous solution such that the weight ratio of alumina to HCl is 53 to 66 parts alumina to 1 part HCl and the Al 2 O 3 is 18 to 26% of the total mixture, and 5. simultaneously agitating said mixture to obtain the desired dispersion.
Claim 3
Dependent Claim
24 words
The method of claim 1 in which the concentration of Al 2 O 3 is 54 to 65 pbw per 1 pbw of HCl.
Claim 4
Dependent Claim
39 words
The method of claim 1 in which the concentration of Al 2 O 3 is 18% and the ratio of Al 2 O 3 is 54 to 61 pbw of Al 2 O 3 per 1 pbw of HCl.
Claim 5
Dependent Claim
41 words
The method of claim 1 in which the concentration of Al 2 O 3 is 26% and the ratio of Al 2 O 3 to HCl is 58 to 65 pbw of Al 2 O 3 per 1 pbw of HCl.
Claim 6
Dependent Claim
15 words
The method of claim 1 in which the temperature is maintained between 20° and 80°C.
Claim 7
Dependent Claim
11 words
The method of claim 1 in which the pressure is atmospheric.
Claim 8
Dependent Claim
11 words
The method of claim 5 in which the pressure is atmospheric.
Claim 9
Dependent Claim
19 words
The method of claim 2 wherein the alumina introduced into said mixture is in the form of alumina monohydrate.
Claim 10
Dependent Claim
28 words
The dispersion of alumina produced by the method of claim 1 in which the pH is between 3.5 and 4.2 and the stability is greater than 6 months.
Claim 11
Dependent Claim
47 words
A dispersion of alumina with a concentration of Al 2 O 3 between 18 and 26%, a ratio of Al 2 O 3 to HCl of 53 to 66 pbw of Al 2 O 3 per 1 pbw of HCl and a pH of 3.5 to 4.2.
Claim 12
Dependent Claim
47 words
A dispersion of alumina with a concentration of Al 2 O 3 between 18 and 26%, a ratio of Al 2 O 3 to HCl of 53 to 66 pbw of Al 2 O 3 per 1 pbw of HCl and a pH of 3.5 to 4.2.
Claim 13
Dependent Claim
38 words
A dried powder having therein 53 to 66 pbw Al 2 O 3 per 1 pbw HCl prepared by drying the dispersion of claim 10 under conditions that do not alter the Al 2 O 3 --HCl ratio.
Claim 14
Dependent Claim
48 words
The dispersion of claim 10 with an Al 2 O 3 concentration of 18% and a ratio of Al 2 O 3 to HCl of 54 to 61 pbw of Al 2 O 3 per 1 pbw of HCl with a shelf life of 6 to 12 months.
Claim 15
Dependent Claim
50 words
The dispersion of claim 10 with an Al 2 O 3 concentration of 26% Al 2 O 3 and a ratio of Al 2 O 3 to HCl of 58 to 65 pbw of Al 2 O 3 per 1 pbw of HCl with a shelf life of 6 months.
Claim 16
Dependent Claim
12 words
The dispersion of claim 10 with a pH of 3.8 to 4.1.
Claim 17
Dependent Claim
83 words
in the known process of forming an aqueous alumina dispersion comprising forming an aqueous solution of HCl and then adding alumina, the improvement being that concentrations of 18 to 26% Al 2 O 3 on a weight basis having stability for at least 6 months are obtained by maintaining the ratio of Al 2 O 3 to HCl in the dispersion at 53 to 66 pbw of Al 2 O 3 per 1 pbw of HCl and the pH at 3.5 to 4.2.
Claim 18
Dependent Claim
83 words
in the known process of forming an aqueous alumina dispersion comprising forming an aqueous solution of HCl and then adding alumina, the improvement being that concentrations of 18 to 26% Al 2 O 3 on a weight basis having stability for at least 6 months are obtained by maintaining the ratio of Al 2 O 3 to HCl in the dispersion at 53 to 66 pbw of Al 2 O 3 per 1 pbw of HCl and the pH at 3.5 to 4.2.
Claim 19
Dependent Claim
13 words
The process of claim 15 in which the pH is 3.8 to 4.1.
Claim 20
Dependent Claim
44 words
The process of claim 15 in which the weight concentration of Al 2 O 3 in the dispersion is 18% and the Al 2 O 3 to HCl ratio is 54 to 61 pbw of Al 2 O 3 per 1 pbw of HCl.
Claim 21
Dependent Claim
44 words
The process of claim 15 in which the weight concentration of Al 2 O 3 in the dispersion is 26% and the Al 2 O 3 to HCl ratio is 58 to 65 pbw of Al 2 O 3 per 1 pbw of HCl.
Claim 22
Dependent Claim
33 words
The process of claim 15 in which the Al 2 O 3 to HCl ratio of the dispersion is 54 to 65 pbw of Al 2 O 3 per 1 pbw of HCl.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-01-26 | 1979-07-28 | 1980-01-27 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-01-26 | 1983-07-28 | 1984-01-27 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-01-26 | 1987-07-28 | 1988-01-27 | $7700.00 | Window Closed / Lapsed |