US3933981A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Tin-lead purification of silicon
Assignee: Texas Instruments Inc
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Filing: 1973-11-30
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Granted: 1976-01-20
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Expires: 1993-11-30
Abstract
Abstract Disclosed is a method of purifying silicon by introducing the silicon into liquid tin-lead alloy at a certain temperature. The silicon goes into solution with the tin-lead alloy, after which the temperature of the liquid metal solution is reduced to a temperature low enough to cause the solution to become super-saturated with respect to silicon which then solidifies as pure material. The solid pure silicon is withdrawn from the tin-lead solution leaving substantially all of the impurities behind.
Inventors
- 👤 Gene Felix Wakefield
- 👤 H. S. Nagaraja Setty
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 09:04
CPC Classifications
C; C01; C01B; C01B33/00; C01B33/02; C01B33/037
Claims Analysis
Total Claims: 3
Claim 1
Independent Claim
161 words
The method of purifying silicon in a refiner containing liquid tin-lead alloy at varying temperatures, comprising the steps of: a. introducing impure solid silicon into a molten tin-lead alloy, said alloy having a composition ranging between 80% tin - 20% lead and 50% tin-50% lead, and said impure silicon being introduced into a first compartment of said refiner, the temperature of said first compartment being sufficiently high to cause the silicon to go into solution with said alloy; b. circulating said solution of liquid alloy and silicon from said high temperature zone into a second compartment of said refiner maintained at a low temperature zone, the temperature range of said low temperature zone being sufficiently lower than the high temperature zone of said first compartment to cause said silicon to become supersaturated and to begin to crystallize; and c. removing purified solid silicon from said low-temperature zone as said silicon crystallizes, leaving impurities of said silicon behind in said liquid alloy.
Claim 2
Independent Claim
161 words
The method of purifying silicon in a refiner containing liquid tin-lead alloy at varying temperatures, comprising the steps of: a. introducing impure solid silicon into a molten tin-lead alloy, said alloy having a composition ranging between 80% tin - 20% lead and 50% tin-50% lead, and said impure silicon being introduced into a first compartment of said refiner, the temperature of said first compartment being sufficiently high to cause the silicon to go into solution with said alloy; b. circulating said solution of liquid alloy and silicon from said high temperature zone into a second compartment of said refiner maintained at a low temperature zone, the temperature range of said low temperature zone being sufficiently lower than the high temperature zone of said first compartment to cause said silicon to become supersaturated and to begin to crystallize; and c. removing purified solid silicon from said low-temperature zone as said silicon crystallizes, leaving impurities of said silicon behind in said liquid alloy.
Claim 3
Dependent Claim
43 words
The method of purifying silicon in a tin-lead alloy of varying temperature, as defined in claim 1, including the step of continuously introducing said impure solid silicon to be purified into said alloy, and continuously removing said purified solid silicon from said alloy.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-01-19 | 1979-07-21 | 1980-01-20 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-01-19 | 1983-07-21 | 1984-01-20 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-01-19 | 1987-07-21 | 1988-01-20 | $7700.00 | Window Closed / Lapsed |