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US3928108A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of making a poly(methyl methacrylate) pre-holographic element

Assignee: United States Department of the Navy
•
Filing: 1974-08-12
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Granted: 1975-12-23
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Expires: 1994-08-12
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Abstract

Abstract Methods for manufacturing pre-holographic elements are disclosed. The methods comprise the steps of providing a poly(methyl methacrylate) base, coating the base with a nitrocellulose-containing coating composition, denitrating the coating composition, covering the coated base with water, placing a pre-hardened gelatin film under the water near the coating on the base and removing the water from between the coating and the pre-hardened gelatin film.

Inventors

  • 👤 Arnold Adicoff
  • 👤 Warren J Murbach

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 22:25
CPC Classifications
B; B32; B32B; B32B27/00; B32B27/06; B32B27/30; B32B27/308; G; G03; G03C; G03C1/00; G03C1/66; G03C1/76; G03C1/91; G03C1/93; G03H; G03H1/00; G03H1/02; B32B2255/00; B32B2255/10; B32B2255/24; G03H1/04; G03H1/0402; G03H2001/043; G03H2250/00; G03H2250/39; G03H2260/00; G03H2260/10; G03H2270/00; G03H2270/10; G03H2270/14; Y; Y10; Y10S; Y10S428/00; Y10S428/913; Y10T; Y10T428/00; Y10T428/31504; Y10T428/31725; Y10T428/31779; Y10T428/31783

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 119 words
A METHOD FOR MANUFACTURING A PRE-HOLOGRAPHIC ELEMENT COMPRISING THE STEPS OF: A. PROVIDING A POLY (METHYL METHACRYLATE) BASE; B. COATING THE BASE WITH A COATING COMPOSITION MADE UP OF 2 WEIGHT PERCENT NITROCELLULOSE AND 98 WEIGHT PERCENT 2-METHOXYETHANOL; C. DRYING THE COATING D. DENITRATING THE COATING BY IMMERSING IT IN A STIRRED BATH OF A DENITRATING COMPOSITION MADE UP OF 50 VOLUME PERCENT AMMONIUM SULFIDE AND 50 VOLUME PERCENT ETHANOL FOR 1 HOUR TO FORM REGENERATED CELLULOSE; E. COVERING THE COATED BASE WITH WATER; F. PLACING A PRE-HARDENED GELATIN FILM UNDER THE WATER NEAR THE COATED BASE; AND G. REMOVING THE WATER FROM BETWEEN THE COATED BASE AND THE GELATIN FILM ALLOWING THE GELATIN FILM TO CONTACT THE COATING.
Claim 2
Independent Claim 119 words
A METHOD FOR MANUFACTURING A PRE-HOLOGRAPHIC ELEMENT COMPRISING THE STEPS OF: A. PROVIDING A POLY (METHYL METHACRYLATE) BASE; B. COATING THE BASE WITH A COATING COMPOSITION MADE UP OF 2 WEIGHT PERCENT NITROCELLULOSE AND 98 WEIGHT PERCENT 2-METHOXYETHANOL; C. DRYING THE COATING D. DENITRATING THE COATING BY IMMERSING IT IN A STIRRED BATH OF A DENITRATING COMPOSITION MADE UP OF 50 VOLUME PERCENT AMMONIUM SULFIDE AND 50 VOLUME PERCENT ETHANOL FOR 1 HOUR TO FORM REGENERATED CELLULOSE; E. COVERING THE COATED BASE WITH WATER; F. PLACING A PRE-HARDENED GELATIN FILM UNDER THE WATER NEAR THE COATED BASE; AND G. REMOVING THE WATER FROM BETWEEN THE COATED BASE AND THE GELATIN FILM ALLOWING THE GELATIN FILM TO CONTACT THE COATING.
Claim 3
Dependent Claim 22 words
The method according to claim 1 wherein the coating is dried for at least 4 hours before the denitrating step is performed.
Claim 4
Dependent Claim 18 words
the method according to claim 2 wherein the denitrating step is carried out for at least 1 hour.
Claim 5
Dependent Claim 30 words
the method according to claim 3 wherein the base is selected from the group consisting of poly(methyl methacrylate) objects having spheroidal surfaces and poly (methyl methacrylate) objects having toroidal surfaces.
Claim 6
Dependent Claim 22 words
The method according to claim 3 wherein the base is selected from the group consisting of polymethyl methacrylate) objects having flat surfaces.

References Cited (Backward Citations)

US2276151A Cited
US2471583A Cited
US2606130A Cited
US3178287A Cited
US3402087A Cited
US3833383A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-12-22 1979-06-23 1979-12-23 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-12-22 1983-06-23 1983-12-23 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-12-22 1987-06-23 1987-12-23 $7700.00 Window Closed / Lapsed

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