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US3926748A Expired / Lapsed US ⏱️ 0.0 years remaining

Electrodeposition of gold-antimony alloys and compositions therefor

Assignee: TE Connectivity Corp
•
Filing: 1974-06-28
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Granted: 1975-12-16
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Expires: 1994-06-28
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Abstract

Abstract A neutral and stable gold and antimony metal plating bath and gold and antimony metal alloys of outstanding properties; an electrolytic bath operated at a pH between 6.8 and 7.3 which is stable under the plating conditions for a period up to a year and longer capable of depositing from the electrolyzed solution a gold and antimony metal alloy at weight percentages heretofore producing poor deposits; codeposition as an alloy of gold and antimony metal which is suitable as a doped chip-attach surface.

Inventors

  • 👤 Lewis Brian Lerner

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 21:52
CPC Classifications
C; C25; C25D; C25D3/00; C25D3/02; C25D3/56; C25D3/62

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 86 words
AN ELECTROLYTE FOR ELECTRODEPOSITION OF A GOLD ANTIMONY ALLOY FROM AN AQUEOUS SOLUTION AT A PH OF 6.8 TO 7.3 CONSISTING ESSENTIALLY OF (A) DIBASIC POTASSIUM PHOSPHATE FROM 100 TO 200 GRAMS LITER, (B) MONOBASIC POTASSIUM PHOSPHATE, FROM 30 TO 60 GRAMS/LITER, POTASSIUM TARTRATE, FROM 5 TO 50 GRAMS/LITER, GOLD AS KAU2, FROM 8 TO 17 GRAMS LITER, AND ANTIMONY POTASSIUM TARTRATE, FROM 1 TO 1 GRAMS LITER AND WHEREIN A TO B IS 70 TO 75% ON HYDROUS BASIS TO ANHYDROUS BASIS, BY WEIGHT, RESPECTIVELY.
Claim 2
Dependent Claim 86 words
AN ELECTROLYTE FOR ELECTRODEPOSITION OF A GOLD ANTIMONY ALLOY FROM AN AQUEOUS SOLUTION AT A PH OF 6.8 TO 7.3 CONSISTING ESSENTIALLY OF (A) DIBASIC POTASSIUM PHOSPHATE FROM 100 TO 200 GRAMS LITER, (B) MONOBASIC POTASSIUM PHOSPHATE, FROM 30 TO 60 GRAMS/LITER, POTASSIUM TARTRATE, FROM 5 TO 50 GRAMS/LITER, GOLD AS KAU2, FROM 8 TO 17 GRAMS LITER, AND ANTIMONY POTASSIUM TARTRATE, FROM 1 TO 1 GRAMS LITER AND WHEREIN A TO B IS 70 TO 75% ON HYDROUS BASIS TO ANHYDROUS BASIS, BY WEIGHT, RESPECTIVELY.
Claim 3
Independent Claim 101 words
A method for electrodepositing an antimony gold alloy which comprises electrolyzing an aqueous solution by impressing a current between anode and a workpiece as a cathode, said solution consisting essentially of potassium phosphate (dibasic), from 100 to 200 grams/liter, potassium phosphate (monobasic), from 30 to 60 grams/liter, potassium tartrate, from 5 to 50 grams/litEr, gold as KAu2, from 8 to 17 grams/liter, antimony potassium tartrate, from 1. to 1 grams/liter, wherein the specific gravity of said solution at 25*C is 18*Be and the pH at 25*C as determined electrometrically is from 6.8 to 7.3 and depositing said alloy on said workpiece.
Claim 4
Independent Claim 101 words
A method for electrodepositing an antimony gold alloy which comprises electrolyzing an aqueous solution by impressing a current between anode and a workpiece as a cathode, said solution consisting essentially of potassium phosphate (dibasic), from 100 to 200 grams/liter, potassium phosphate (monobasic), from 30 to 60 grams/liter, potassium tartrate, from 5 to 50 grams/litEr, gold as KAu2, from 8 to 17 grams/liter, antimony potassium tartrate, from 1. to 1 grams/liter, wherein the specific gravity of said solution at 25*C is 18*Be and the pH at 25*C as determined electrometrically is from 6.8 to 7.3 and depositing said alloy on said workpiece.
Claim 5
Dependent Claim 22 words
The method as defined in claim 2, wherein the anode is platinum anode and wherein during the deposition, the solution is agitated.
Claim 6
Dependent Claim 56 words
A composition for use to make an electrolyte for the electrodeposition of a gold-antimony alloy consisting essentially of potassium phosphate (dibasic), potassium phosphate (monobasic), potassium gold cyanide, antimony potassium tartrate, and potassium tartrate, wherein the potassium phosphate (dibasic) to potassium phosphate (monobasic) is 70 to 75 percent on hydrous basis to anhydrous basis, by weight, respectively.
Claim 7
Dependent Claim 56 words
A composition for use to make an electrolyte for the electrodeposition of a gold-antimony alloy consisting essentially of potassium phosphate (dibasic), potassium phosphate (monobasic), potassium gold cyanide, antimony potassium tartrate, and potassium tartrate, wherein the potassium phosphate (dibasic) to potassium phosphate (monobasic) is 70 to 75 percent on hydrous basis to anhydrous basis, by weight, respectively.

References Cited (Backward Citations)

US3020217A Cited
US2905601A Cited
US3380814A Cited
US3666640A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-12-15 1979-06-16 1979-12-16 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-12-15 1983-06-16 1983-12-16 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-12-15 1987-06-16 1987-12-16 $7700.00 Window Closed / Lapsed

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