US3925041A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Thermal swing gas adsorber
Assignee: Union Carbide Industrial Gases Technology Corp
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Filing: 1974-12-06
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Granted: 1975-12-09
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Expires: 1994-12-06
Abstract
Abstract This invention relates to a gas adsorbent vessel with an internal compressible fibrous layer of thermal insulation positioned against the casing inner surface with rigid preformed sheets of thermal insulation covering the compressible layer in an end to end and side to side abutting relationship with means for outwardly compressing the assembly against the casing inner wall. The vessel is of a type having particular utility for prepurifying air of atmospheric contaminants by thermal swing adsorption prior to cryogenic air separation.
Inventors
- 👤 Michael Frederick Patterson
- 👤 Kenneth Calvin Kather
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-06 01:40
CPC Classifications
B; B01; B01D; B01D53/00; B01D53/02; B01D53/04; B01D53/0407; B01D53/0446; B01D53/0423; B01D53/26; B01D53/261; F; F16; F16L; F16L59/00; F16L59/02; B01D2253/00; B01D2253/10; B01D2253/106; B01D2253/108; B01D2253/30; B01D2253/302; B01D2253/304; B01D2256/00; B01D2256/10; B01D2256/12; B01D2257/00; B01D2257/30; B01D2257/302; B01D2257/40; B01D2257/404; B01D2257/50; B01D2257/504; B01D2257/70; B01D2257/702; B01D2257/80; B01D2259/00; B01D2259/40; B01D2259/40083; B01D2259/40088; B01D2259/4009; B01D2259/402; B01J; B01J2219/00; B01J2219/18; B01J2219/182; Y; Y02; Y02C; Y02C20/00; Y02C20/40
Claims Analysis
Total Claims: 19
Claim 1
Independent Claim
186 words
A GAS ADSORBENT VESSEL COMPRISING: A RIGID OUTER CASING, AN ADSORBENT BED WITHIN SAID CASING; SUPPORT MEANS FOR SAID ADSORBENT BED BEARING AGAINST THE CASING INNER SURFACE AND THE ADSORBENT BED OUTER SURFACE; GAS FLOW PASSAGE MEANS EXTENDING THROUGH THE BOTTOM WALL AND THE TOP WALL OF SAID CASING; A COMPRESSIBLE FIBROUS LAYER OF THERMAL INSULATION MATERIAL HAVING FIBER DIAMETER OF LESS THAN 20 MICRONS AND AN UNCOMPRESSED POROSITY OF GREATER THAN 0.95 POSITIONED AGAINST THE CASING INNER SURFACE; A MULTIPLICITY OF RIGID PREFORMED SHEETS OF THERMAL INSULATION MATERIAL HAVING PERMEABILITY OF LESS THAN 150 FT2/HR-ATM BASED ON AIR AT 70*F. BEING SUBSTANTIALLY PLANAR AND POSITIONED INWARDLY OF AND COVERING SAID COMPRESSIBLE FIBROUS LAYER IN AN END-TO-END AND SIDE-TO-SIDE ABUTTING RELATIONSHIP WITH TRANSVERSE GAPS BETWEEN THE CASING INNER SURFACE AND OUTER SURFACE OF SAID PREFORMED SHEETS NOT EXCEEDING 1/2 INCH; AND MEANS FOR POSITIONING AND OUTWARDLY COMPRESSING THE COMPRESIBLE FIBROUS LAYER-RIGID PREFORMED SHEET ASSEMBLY AGAINST SAID CASING INNER SURFACE SUCH THAT THE RATIO OF THE DENSITY OF THE COMPRESSIBLE FIRBOUS LAYER IN THE COMPRESSED STATE TO ITS DENSITY IN THE UNCOMPRESSED STATE IS AT LEAST 1.5.
Claim 2
Dependent Claim
186 words
A GAS ADSORBENT VESSEL COMPRISING: A RIGID OUTER CASING, AN ADSORBENT BED WITHIN SAID CASING; SUPPORT MEANS FOR SAID ADSORBENT BED BEARING AGAINST THE CASING INNER SURFACE AND THE ADSORBENT BED OUTER SURFACE; GAS FLOW PASSAGE MEANS EXTENDING THROUGH THE BOTTOM WALL AND THE TOP WALL OF SAID CASING; A COMPRESSIBLE FIBROUS LAYER OF THERMAL INSULATION MATERIAL HAVING FIBER DIAMETER OF LESS THAN 20 MICRONS AND AN UNCOMPRESSED POROSITY OF GREATER THAN 0.95 POSITIONED AGAINST THE CASING INNER SURFACE; A MULTIPLICITY OF RIGID PREFORMED SHEETS OF THERMAL INSULATION MATERIAL HAVING PERMEABILITY OF LESS THAN 150 FT2/HR-ATM BASED ON AIR AT 70*F. BEING SUBSTANTIALLY PLANAR AND POSITIONED INWARDLY OF AND COVERING SAID COMPRESSIBLE FIBROUS LAYER IN AN END-TO-END AND SIDE-TO-SIDE ABUTTING RELATIONSHIP WITH TRANSVERSE GAPS BETWEEN THE CASING INNER SURFACE AND OUTER SURFACE OF SAID PREFORMED SHEETS NOT EXCEEDING 1/2 INCH; AND MEANS FOR POSITIONING AND OUTWARDLY COMPRESSING THE COMPRESIBLE FIBROUS LAYER-RIGID PREFORMED SHEET ASSEMBLY AGAINST SAID CASING INNER SURFACE SUCH THAT THE RATIO OF THE DENSITY OF THE COMPRESSIBLE FIRBOUS LAYER IN THE COMPRESSED STATE TO ITS DENSITY IN THE UNCOMPRESSED STATE IS AT LEAST 1.5.
Claim 3
Dependent Claim
57 words
A gas adsorbent vessel according to claim 1 wherein the preformed sheets are aligned in a multiplicity of rows extending perpendicular to the direction of gas flow through the adsorbent bed, said abutting ends are substantially parallel to said direction of gas flow, and said abutting ends in transversely adjacent rows are transversely displaced from each other.
Claim 4
Dependent Claim
22 words
A gas adsorbent vessel according to claim 1 wherein the fiber diameter of said compressible fibrous layer is less than 10 microns.
Claim 5
Dependent Claim
21 words
A gas adsorbent vessel according to claim 1 wherein the uncompressed porosity of said compressible fibrous layer is greater than 0.98.
Claim 6
Dependent Claim
34 words
A gas adsorbent vessel according to claim 1 wherein the ratio of the density of the compressible fibrous layer in the compressed state to its density in the uncompressed state is at least 4.0.
Claim 7
Dependent Claim
34 words
A gas adsorbent vessel according to claim 1 wherein the outer surface of said preformed sheet is at least partially contoured so as to mate with the inner surface of said rigid outer casing.
Claim 8
Dependent Claim
32 words
A gas adsorbent vessel according to claim 1 wherein said compressible fibrous layer is formed of glass fibers having fiber diameter of about 1.0 microns and an uncompressed porosity of about 0.996.
Claim 9
Dependent Claim
33 words
A gas adsorbent vessel according to claim 1 wherein said rigid preformed sheets are formed of calcium silicate reinforced with glass fiber having permeability of about 1 ft2/hr-atm, based on air at 70*F.
Claim 10
Dependent Claim
27 words
A gas adsorbent vessel according to claim 1 wherein the gas permeability of the preformed sheets is no more than 1/100 that oF the compressible fibrous layer.
Claim 11
Dependent Claim
59 words
A gas adsorbent vessel according to claim 1 wherein the preformed sheets are aligned in a multiplicity of rows extending perpendicular to the direction of gas flow through the adsorbent bed, and gas flow-diverting barrier means are disposed between said abutting aides of the preformed sheets in said transversely adjacent rows to direct bypassing gas into said adsorbent bed.
Claim 12
Dependent Claim
49 words
A gas adsorbent vessel according to claim 10 wherein said gas flow-diverting barrier means comprise metal foil sheets gas-tightly secured to said casing inner surface at one end and extending inwardly between said abutting sides of the preformed sheets with the opposite end substantially adjacent to said adsorbent bed.
Claim 13
Dependent Claim
23 words
A gas adsorbent vessel according to claim 2 including compressible fibrous thermal insulation between at least said abutting ends of adjacent preformed sheets.
Claim 14
Dependent Claim
239 words
A gas adsorbent vessel comprising: a rigid cylindrical outer casing with its longitudinal axis aligned substantially in the horizontal direction, an adsorbent bed within said casing in the central part thereof and extending from end-to-end; support means for said adsorbent bed bearing against the casing inner surface and the adsorbent bed outer surface; gas flow passage means extending through the bottom wall and the top wall of said casing; gas distributor means between said gas flow passage means and the end-to-end length of the adsorbent bed bottom and top for gas flow through said adsorbent bed substantially normal to said longitudinal axis; a compressible fibrous layer of thermal insulation material having fiber diameter of less than 20 microns and an uncompressed porosity of greater than 0.95 positioned against the casing inner surface; a multiplicity of rigid preformed sheets of thermal insulation material having permeability of less than 150 ft2/hr-atm based on air at 70*F, being substantially planar and positioned inwardly of and covering said compressible fibrous layer in an end-to-end and side-to-side abutting relationship with transverse gaps between the casing inner surface and outer surface of said preformed sheets not exceeding 1/2 inch; and means for positioning and outwardly compressing the compressible fibrous layer-rigid preformed sheet assembly against said casing inner surface such that the ratio of the density of the compressible fibrous layer in the compressed state to its density in the uncompressed state is at least 1.5.
Claim 15
Dependent Claim
239 words
A gas adsorbent vessel comprising: a rigid cylindrical outer casing with its longitudinal axis aligned substantially in the horizontal direction, an adsorbent bed within said casing in the central part thereof and extending from end-to-end; support means for said adsorbent bed bearing against the casing inner surface and the adsorbent bed outer surface; gas flow passage means extending through the bottom wall and the top wall of said casing; gas distributor means between said gas flow passage means and the end-to-end length of the adsorbent bed bottom and top for gas flow through said adsorbent bed substantially normal to said longitudinal axis; a compressible fibrous layer of thermal insulation material having fiber diameter of less than 20 microns and an uncompressed porosity of greater than 0.95 positioned against the casing inner surface; a multiplicity of rigid preformed sheets of thermal insulation material having permeability of less than 150 ft2/hr-atm based on air at 70*F, being substantially planar and positioned inwardly of and covering said compressible fibrous layer in an end-to-end and side-to-side abutting relationship with transverse gaps between the casing inner surface and outer surface of said preformed sheets not exceeding 1/2 inch; and means for positioning and outwardly compressing the compressible fibrous layer-rigid preformed sheet assembly against said casing inner surface such that the ratio of the density of the compressible fibrous layer in the compressed state to its density in the uncompressed state is at least 1.5.
Claim 16
Dependent Claim
199 words
A gas adsorbent vessel comprising: a rigid cylindrical outer casing with its longitudinal axis aligned substantially in the vertical direction, an adsorbent bed within said casing; support means for said adsorbent bed bearing against the casing inner surface and the adsorbent bed outer surface; gas flow passage means extending through the bottom end wall and the top end wall of said casing; a compressible fibrous layer of thermal insulation material having fiber diameter of less than 20 microns and an uncompressed porosity of greater than 0.95 positioned against the casing inner surface; a multiplicity of rigid preformed sheets of thermal insulation material having permeability of less than 150 ft2/hr-atm based on air at 70*F, being substantially planar and positioned inwardly of and covering said compressible fibrous layer in an end-to-end and side-to-side abutting relationship with transverse gaps between the basing inner surface and outer surface of said preformed sheets not exceeding 1/2 inch; and means for positioning and outwardly compressing the compressible fibrous layer-rigid preformed sheet assembly against said casing inner surface such that the ratio of the density of the compressible fibrous layer in the compressed state to its density in the uncompressed state is at least 1.5.
Claim 17
Dependent Claim
199 words
A gas adsorbent vessel comprising: a rigid cylindrical outer casing with its longitudinal axis aligned substantially in the vertical direction, an adsorbent bed within said casing; support means for said adsorbent bed bearing against the casing inner surface and the adsorbent bed outer surface; gas flow passage means extending through the bottom end wall and the top end wall of said casing; a compressible fibrous layer of thermal insulation material having fiber diameter of less than 20 microns and an uncompressed porosity of greater than 0.95 positioned against the casing inner surface; a multiplicity of rigid preformed sheets of thermal insulation material having permeability of less than 150 ft2/hr-atm based on air at 70*F, being substantially planar and positioned inwardly of and covering said compressible fibrous layer in an end-to-end and side-to-side abutting relationship with transverse gaps between the basing inner surface and outer surface of said preformed sheets not exceeding 1/2 inch; and means for positioning and outwardly compressing the compressible fibrous layer-rigid preformed sheet assembly against said casing inner surface such that the ratio of the density of the compressible fibrous layer in the compressed state to its density in the uncompressed state is at least 1.5.
Claim 18
Dependent Claim
320 words
An air prepurifier adsorbent vessel comprising: a rigid cylindrical outer casing with its longitudinal axis aligned substantially in the horizontal direCtion, a sodium zeolite X adsorbent bed within said casing inner the central parts thereof and extending from end-to-end; support means for said adsorbent bed bearing against the casing inner surface and the adsorbent bed outer surface; air flow passage means extending through the bottom wall and the top wall of said casing; air distributor means between said air flow passage means and the end-to-end length of the absorbent bed bottom and top; a compressible glass fibrous layer of thermal insulation material having fiber diameter of about 1.0 microns and an uncompressed porosity of about 0.996 positioned against the casing inner surface; a multiplicity of rigid preformed sheets of calcium silicate reinforced with glass fiber thermal insulation material having permeability of about 1 ft2/hr-atm, based on air at 70*F, being substantially planar and positioned inwardly of and covering said compressible glass fibrous layer in an end-to-end and side-to-side abutting relationship with outer surfaces at least partially contoured so as to mate with the inner surface of said cylindrical outer casing and transverse gaps between the casing inner surface and the outer surface of said rigid preformed sheets not exceeding about 1/16 inch, said preformed sheets being aligned in a multiplicity of longitudinal rows with abutting ends in transversely adjacent rows being transversely displaced from each other; compressible glass fibrous thermal insulation between at least the abutting ends of adjacent preformed sheets which abutting ends are substantially parallel to the direction of glass flow through said adsorbent bed; and means for positioning and outwardly compressing the compressible glass fibrous layer-rigid preformed calcium silicate and glass fiber sheet assembly against said casing inner surface such that the ratio of the density of the compressible glass fibrous layer in the compressed state to its density in the uncompressed state it at least 4.
Claim 19
Dependent Claim
320 words
An air prepurifier adsorbent vessel comprising: a rigid cylindrical outer casing with its longitudinal axis aligned substantially in the horizontal direCtion, a sodium zeolite X adsorbent bed within said casing inner the central parts thereof and extending from end-to-end; support means for said adsorbent bed bearing against the casing inner surface and the adsorbent bed outer surface; air flow passage means extending through the bottom wall and the top wall of said casing; air distributor means between said air flow passage means and the end-to-end length of the absorbent bed bottom and top; a compressible glass fibrous layer of thermal insulation material having fiber diameter of about 1.0 microns and an uncompressed porosity of about 0.996 positioned against the casing inner surface; a multiplicity of rigid preformed sheets of calcium silicate reinforced with glass fiber thermal insulation material having permeability of about 1 ft2/hr-atm, based on air at 70*F, being substantially planar and positioned inwardly of and covering said compressible glass fibrous layer in an end-to-end and side-to-side abutting relationship with outer surfaces at least partially contoured so as to mate with the inner surface of said cylindrical outer casing and transverse gaps between the casing inner surface and the outer surface of said rigid preformed sheets not exceeding about 1/16 inch, said preformed sheets being aligned in a multiplicity of longitudinal rows with abutting ends in transversely adjacent rows being transversely displaced from each other; compressible glass fibrous thermal insulation between at least the abutting ends of adjacent preformed sheets which abutting ends are substantially parallel to the direction of glass flow through said adsorbent bed; and means for positioning and outwardly compressing the compressible glass fibrous layer-rigid preformed calcium silicate and glass fiber sheet assembly against said casing inner surface such that the ratio of the density of the compressible glass fibrous layer in the compressed state to its density in the uncompressed state it at least 4.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1978-12-08 | 1979-06-09 | 1979-12-09 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1982-12-08 | 1983-06-09 | 1983-12-09 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1986-12-08 | 1987-06-09 | 1987-12-09 | $7700.00 | Window Closed / Lapsed |