US3918919A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Reactor for the preparation of halogenated compounds from hydrocarbons
Assignee: Hoechst AG
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Filing: 1973-06-21
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Granted: 1975-11-11
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Expires: 1993-06-21
Abstract
Abstract Halogenated compounds from hydrocarbons are prepared at temperatures of from 400* to 800*C and under pressures of from 50 to 700 kp/cm2. The required reactor contains several independently heated reactor units mounted in adjacent or superjacent position between which sealing elements are placed. The reactor units are provided with a nickel lining flanged at the ends, and the sealing elements consist of a nickel core with orifice and two circumferential flanged rings. The reactor units are compressed by spring-mounted expansion bolts.
Inventors
- 👤 Richard Walburg
- 👤 Helmut Gerstenberg
- 👤 Hans Osterbrink
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 10:34
CPC Classifications
B; B01; B01J; B01J19/00; B01J19/0053; B01J19/0073; B01J19/02; B01J3/00; B01J3/04; B01J3/042; C; C07; C07C; C07C17/00; C07C17/361; F; F16; F16L; F16L21/00; F16L21/02; F16L21/04; F16L23/00; F16L23/006; B01J2219/00; B01J2219/02; B01J2219/0204; B01J2219/0236; F16B; F16B2200/00; F16B2200/50; F16B2200/506; Y; Y02; Y02P; Y02P20/00; Y02P20/141
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
214 words
A REACTOR FOR THE PREPARATION OF HALOGENATED COMPOUNDS FROM HYDROCARBONS, AT TEMPERATURES OF FROM 400* TO 800*C. AND UNDER PRESSURES OF FROM 50 TO 700 KP/CM2 COMPRISING A PLURALITY OF CYLINDRICAL REACTOR UNITS, SAID REACTOR UNITS HAVING INTERNAL BORES AND BEING ALIGNED ON A COMMON LONGITUDUNAL AXIS WITH SAID INTERNAL BORES IN AXIAL ALIGNMENT WITH EACH OTHER, A SEALING ELEMENT POSITIONED BETWEEN AND CONNECTING THE ADJACENT ENDS OF EACH OF SAID ALIGNED REACTOR UNITS, SAID SEALING ELEMENT COMPRISING A NICKEL CORE HAVING AN INTERNAL BORE LOCATED GENERALLY IN ALIGNMENT WITH THE BORES OF ITS ADJACENT REACTOR UNITS, EACH OF SAID REACTOR UNITS HAVING A NICKEL LINING ON THEIR RESPECTIVE INTERNAL BORES, SAID LINING EXTENDING BEYOND THE END PORTIONS OF THE REACTOR UNITS AND BEING FLANGED OVER AT LEAST A PORTION OF THEIR ASSOCIATED REACTOR UNIT END PORTIONS, TWO CIRCUMFERENTIAL FLANGED RINGS BOLTED TOGETHER SURROUNDING SAID SEALING ELEMENT IN A PLANE PERPENDICULAR TO THE AXIS OF ITS BORE TO REINFORCE SAID SEALING ELEMENT, SAID REACTOR UNITS BEING INDEPENDENTLY HEATED AND HAVING RADIALLY EXTENDING CIRCUMFERENTIAL FLANGES SECURED THERETO ADJACENT THEIR RESPECTIVE END PORTIONS, A PLURALITY OF EXPANSION BOLTS EXTENDING THROUGH ALL OF SAID FLANGES, AND SPRING MEANS COOPERATING BETWEEN SAID FLANGES AND SAID BOLTS FOR COMPRISING SAID SEALING ELEMENT BETWEEN THE FLANGES OF SAID NICKEL LINING.
Claim 2
Dependent Claim
214 words
A REACTOR FOR THE PREPARATION OF HALOGENATED COMPOUNDS FROM HYDROCARBONS, AT TEMPERATURES OF FROM 400* TO 800*C. AND UNDER PRESSURES OF FROM 50 TO 700 KP/CM2 COMPRISING A PLURALITY OF CYLINDRICAL REACTOR UNITS, SAID REACTOR UNITS HAVING INTERNAL BORES AND BEING ALIGNED ON A COMMON LONGITUDUNAL AXIS WITH SAID INTERNAL BORES IN AXIAL ALIGNMENT WITH EACH OTHER, A SEALING ELEMENT POSITIONED BETWEEN AND CONNECTING THE ADJACENT ENDS OF EACH OF SAID ALIGNED REACTOR UNITS, SAID SEALING ELEMENT COMPRISING A NICKEL CORE HAVING AN INTERNAL BORE LOCATED GENERALLY IN ALIGNMENT WITH THE BORES OF ITS ADJACENT REACTOR UNITS, EACH OF SAID REACTOR UNITS HAVING A NICKEL LINING ON THEIR RESPECTIVE INTERNAL BORES, SAID LINING EXTENDING BEYOND THE END PORTIONS OF THE REACTOR UNITS AND BEING FLANGED OVER AT LEAST A PORTION OF THEIR ASSOCIATED REACTOR UNIT END PORTIONS, TWO CIRCUMFERENTIAL FLANGED RINGS BOLTED TOGETHER SURROUNDING SAID SEALING ELEMENT IN A PLANE PERPENDICULAR TO THE AXIS OF ITS BORE TO REINFORCE SAID SEALING ELEMENT, SAID REACTOR UNITS BEING INDEPENDENTLY HEATED AND HAVING RADIALLY EXTENDING CIRCUMFERENTIAL FLANGES SECURED THERETO ADJACENT THEIR RESPECTIVE END PORTIONS, A PLURALITY OF EXPANSION BOLTS EXTENDING THROUGH ALL OF SAID FLANGES, AND SPRING MEANS COOPERATING BETWEEN SAID FLANGES AND SAID BOLTS FOR COMPRISING SAID SEALING ELEMENT BETWEEN THE FLANGES OF SAID NICKEL LINING.
Claim 3
Dependent Claim
79 words
A reactor as claimed in claim 1, wherein said reactor units are formed as steel jackets and each flanged end of the nickel lining of a reactor unit is inserted in a relief of the surrounding steel jacket in such a manner that the sealing surface of the flanged end protrudes over the steel jacket to an extent of less than 20% of the total thickness of the flanged end, which percentage corresponds to a maximum of 3 mm.
Claim 4
Dependent Claim
57 words
A reactor as claimed in claim 1, wherein the length of the flanged rings bolted together is less than that of the nickel core of the sealing element, measured at the exterior diameter of the nickel core, and the protrusion of the nickel core over the flanged ring is no more than 5 mm on each face.
Claim 5
Dependent Claim
24 words
A reactor as claimed in claim 1, wherein the nickel core and the orifice of the sealing elements are manufactured from one single piece.
Claim 6
Dependent Claim
15 words
A reactor as claimed in claim 1, wherein the springs are centered in a bush.
Claim 7
Dependent Claim
27 words
A reactor as claimed in claim 1 wherein said sealing element has a generally radially extending orifice formed therein to provide access to the internal bore thereof.
References Cited (Backward Citations)
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Cited
US1188530A
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US2290333A
Cited
US2633414A
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US3472632A
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US3488070A
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1978-11-10 | 1979-05-12 | 1979-11-11 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1982-11-10 | 1983-05-12 | 1983-11-11 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1986-11-10 | 1987-05-12 | 1987-11-11 | $7700.00 | Window Closed / Lapsed |