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US3918168A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for drying adherent particulate matter such as a polyvinyl chloride resin

Assignee: Olin Corp
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Filing: 1974-10-04
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Granted: 1975-11-11
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Expires: 1994-10-04
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Abstract

Abstract A novel method and apparatus for drying cohesive particulate polyvinyl chloride resin is provided. Adherent solids are mixed with recycle solids until free flowing and are fed to a turbulent primary drying zone provided with lifting flights and then transferred to a flight-free quiescent diffusion drying zone of the dryer.

Inventors

  • 👤 Walter C Saeman

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 13:00
CPC Classifications
F; F26; F26B; F26B11/00; F26B11/02; F26B11/04; F26B11/0404

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 144 words
A METHOD FOR DRYING COHESIVE PARTICULATE MATERIALS IN AN ELONGATED SUBSTANTIALLY CYLINDRICAL DRUM WHICH IS ROTATABLE ABOUT A SUBSTANTIALLY HORIZONTAL AXIS, WHICH HAS A FEED END AND A DISCHARGE END THROUGH WHICH HEATED DRYING GASES ARE FED COCURRENTLY WITH SAID PARTICULATE FROM SAID FEED END TO SAID DISCHARGE END, WHEREIN THE METHOD COMPRISES: A. FEEDING WET COHESIVE PARTICULATE AND SUFFICIENT AT LEAST PATIALLY DRIED RECYCLE PARTICULATE TO A FEED AND MIXING ZONE AT THE FEED END OF SAID DRUM AND MIXING TO PROVIDE A SUBSANIALLY NON-ADHEREN AND RELATIVELY FREE-FLOWING FEED. B. ADVANCING SAID FEED TO THE BED OF A PRIMARY DRYING ZONE PROVIDED WITH A PLURIY OF CIRCUMFERENTIALLY SPACED FLIGHTS. C. LIFTING A PORTION OF SAID BED ON SAID FLIGHTS TO AN UPPER PORTION OF SAID PRIMARY DRYING ZONE AND RELEASING SAID PORTION TO FREEFALL INTO SAID BED THROUGH A STREAM OF HEATED GASES,
Claim 2
Independent Claim 144 words
A METHOD FOR DRYING COHESIVE PARTICULATE MATERIALS IN AN ELONGATED SUBSTANTIALLY CYLINDRICAL DRUM WHICH IS ROTATABLE ABOUT A SUBSTANTIALLY HORIZONTAL AXIS, WHICH HAS A FEED END AND A DISCHARGE END THROUGH WHICH HEATED DRYING GASES ARE FED COCURRENTLY WITH SAID PARTICULATE FROM SAID FEED END TO SAID DISCHARGE END, WHEREIN THE METHOD COMPRISES: A. FEEDING WET COHESIVE PARTICULATE AND SUFFICIENT AT LEAST PATIALLY DRIED RECYCLE PARTICULATE TO A FEED AND MIXING ZONE AT THE FEED END OF SAID DRUM AND MIXING TO PROVIDE A SUBSANIALLY NON-ADHEREN AND RELATIVELY FREE-FLOWING FEED. B. ADVANCING SAID FEED TO THE BED OF A PRIMARY DRYING ZONE PROVIDED WITH A PLURIY OF CIRCUMFERENTIALLY SPACED FLIGHTS. C. LIFTING A PORTION OF SAID BED ON SAID FLIGHTS TO AN UPPER PORTION OF SAID PRIMARY DRYING ZONE AND RELEASING SAID PORTION TO FREEFALL INTO SAID BED THROUGH A STREAM OF HEATED GASES,
Claim 3
Dependent Claim 12 words
The method of claim 1 wherein said particulate is polyvinyl chloride resin.
Claim 4
Dependent Claim 26 words
The method of claim 2 wherein the wet feed to said primary drying zone has a moisture content in the range of 20-30 percent by weight.
Claim 5
Dependent Claim 23 words
The method of claim 2 wherein said recycle particulate has a moisture content in the range of 1.0 to 5 percent by weight.
Claim 6
Dependent Claim 23 words
The process of claim 2 wherein the feed to said primary drying zone has a moisture content in the range of 5-20 percent.
Claim 7
Dependent Claim 23 words
The process of claim 2 wherein the bed of said secondary drying zone has a moisture content below about 5 percent by weight.
Claim 8
Dependent Claim 35 words
The process of claim 2 wherein said heated gases are fed at a temperature in the range of 250*-400*F and wherein said dried particulate has a moisture content of 0.5 percent by weight or less.
Claim 9
Independent Claim 304 words
A method for drying polyvinyl chloride resin drum dryer rotatable about a substantially horizontal axis which has a feed end and a discharge end through which heated drying gases are fed cocurrently with said particulate from said feed end to said discharge end, comprising: a. feeding wet polyvinyl chloride resin having a moisture content in the range of 20-30 percent by weight and sufficient recycle polyvinyl chloride resin having a moisture content of 1.0 to 5 percent by weight of a feed and mixing zone at the feed end of said dryer and mixing to provide a non-adherent relatively free-flowing feed to a primary drying zone, said feed having a moisture content in the range of 5-20 percent by weight, b. advancing said feed to a primary drying zone provided with a plurality of circumferentially spaced flights and depositing the same in a bed of partially dried polyvinyl chloride resin, c. lifting a portion of said bed on said flights to an upper portion of said primary drying zone and releasing said portion to free-fall through a stream of heated gases fed at temperature in the range of 200* to 350*F, d. entraining a portion of said free-falling portion having a moisture content below about 5 percent by weight in said stream of heated gases and advancing the entrained portion of the bed of a flight-free secondary drying zone of said drum, e. maintaining the bed of said secondary drying zone in rolling motion in contact with said strEam of heated gases permitting diffusion drying to occur while said resin is retained in said secondary drying zone, f. recycling a portion of said resin from said secondary drying zone to step (a), and g. removing dried resin having a moisture content below about 0.5 percent by weight from the discharge end of said dryer.
Claim 10
Independent Claim 304 words
A method for drying polyvinyl chloride resin drum dryer rotatable about a substantially horizontal axis which has a feed end and a discharge end through which heated drying gases are fed cocurrently with said particulate from said feed end to said discharge end, comprising: a. feeding wet polyvinyl chloride resin having a moisture content in the range of 20-30 percent by weight and sufficient recycle polyvinyl chloride resin having a moisture content of 1.0 to 5 percent by weight of a feed and mixing zone at the feed end of said dryer and mixing to provide a non-adherent relatively free-flowing feed to a primary drying zone, said feed having a moisture content in the range of 5-20 percent by weight, b. advancing said feed to a primary drying zone provided with a plurality of circumferentially spaced flights and depositing the same in a bed of partially dried polyvinyl chloride resin, c. lifting a portion of said bed on said flights to an upper portion of said primary drying zone and releasing said portion to free-fall through a stream of heated gases fed at temperature in the range of 200* to 350*F, d. entraining a portion of said free-falling portion having a moisture content below about 5 percent by weight in said stream of heated gases and advancing the entrained portion of the bed of a flight-free secondary drying zone of said drum, e. maintaining the bed of said secondary drying zone in rolling motion in contact with said strEam of heated gases permitting diffusion drying to occur while said resin is retained in said secondary drying zone, f. recycling a portion of said resin from said secondary drying zone to step (a), and g. removing dried resin having a moisture content below about 0.5 percent by weight from the discharge end of said dryer.
Claim 11
Dependent Claim 22 words
The process of claim 8 wherein said heated gases are discharged from said dryer at a temperature in the range of 130*-180*F.

References Cited (Backward Citations)

US2754105A Cited
US2283858A Cited
US2351870A Cited
US3765102A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-11-10 1979-05-12 1979-11-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-11-10 1983-05-12 1983-11-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-11-10 1987-05-12 1987-11-11 $7700.00 Window Closed / Lapsed

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