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US3915770A Expired / Lapsed US ⏱️ 0.0 years remaining

Method and apparatus for thermo-chemically slicing crystal boules

Assignee: International Business Machines Corp
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Filing: 1974-12-16
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Granted: 1975-10-28
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Expires: 1994-12-16
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Abstract

Abstract Disclosed is a method and apparatus for thermochemically slicing wafers from a crystal boule by propelling a continuous flow of an acid etching solution against a heated wire which is adjacent the intended line of etch while providing for relative movement between the boule and the chemical etching solution to thereby effect a slicing action of the boule.

Inventors

  • 👤 Jr George R Santillo

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 09:04
CPC Classifications
C; C04; C04B; C04B41/00; C04B41/53; C04B41/5338; C04B41/5353; B; B28; B28D; B28D5/00; C23; C23F; C23F1/00; C23F1/02

Claims Analysis

Total Claims: 20
Claim 1
Independent Claim 74 words
A METHOD OF SLICING A CRYSTAL BOUBLE TO FORM A WAFER, SAID METHOD COMPRISING THE STEPS OF: CLAMPING A BOULE, PROPELLING A CHEMICAL ETCHING SOLUTION ALONG A LINE OF INTENDED ETCH AND ALONG A PREDETERMINED PLANE WITH RESPECT TO THE LONGITUDINAL AXIS OF SAID BOULE, APPLYING HEAT ADJACENT THE ARE OF SAID LINE OF INTENDED ETCH TO THEREBY HEAT AT LEAST ONE OF SAID BOULE AND SAID SOLUTION, AND PROVIDING RELATIVE MOVEMENT BETWEEN SAID
Claim 2
Independent Claim 74 words
A METHOD OF SLICING A CRYSTAL BOUBLE TO FORM A WAFER, SAID METHOD COMPRISING THE STEPS OF: CLAMPING A BOULE, PROPELLING A CHEMICAL ETCHING SOLUTION ALONG A LINE OF INTENDED ETCH AND ALONG A PREDETERMINED PLANE WITH RESPECT TO THE LONGITUDINAL AXIS OF SAID BOULE, APPLYING HEAT ADJACENT THE ARE OF SAID LINE OF INTENDED ETCH TO THEREBY HEAT AT LEAST ONE OF SAID BOULE AND SAID SOLUTION, AND PROVIDING RELATIVE MOVEMENT BETWEEN SAID
Claim 3
Dependent Claim 35 words
A method of slicing a crystal boule in accordance with claim 1, wherein said propelling step occurs due to the rotation of a wheel which to the periphery thereof has been applied said etching solution.
Claim 4
Dependent Claim 55 words
A method of slicing a crystal boule in accordance with claim 1, wherein said heating step occurs by the steps of; providing a wire resistant to said chemical etching solution; positioning said wire adjacent said boule, intermediate said boule and said chemical solution, and passing an electric current through said wire to heat said wire.
Claim 5
Dependent Claim 21 words
A method in accordance with claim 3, wherein sufficient current is passed through said wire to heat said solution between 50*-100*C.
Claim 6
Dependent Claim 66 words
A method of slicing a crystal boule in accordance with claim 1, including the steps of; rotating an etchant applicator wheel in said predetermined plane to propel said chemical etching solution; providing a heating element between said applicator wheel and said boule, and passing a current through said element to heat said element and to thereby heat at least one of said boule and said solution.
Claim 7
Dependent Claim 37 words
A method of slicing a crystal boule in accordance with claim 5, including the step of applying said etchant to said etchant applicator wheel tangentially to said wheel whereby said etchant is propelled radially from said wheel.
Claim 8
Independent Claim 82 words
A method of slicing a crystal boule to form a wafer, said method comprising the steps of: clamping the boule at one end thereof; propelling a chemical etching solution along a line of intended etch and along a predetermined plane with respect to the longitudinal axis of said boule; heating said solution at a point adjacent the line of intended etch and providing relative movement between said boule and said chemical etching solution to thereby effect a slicing action of said boule.
Claim 9
Independent Claim 82 words
A method of slicing a crystal boule to form a wafer, said method comprising the steps of: clamping the boule at one end thereof; propelling a chemical etching solution along a line of intended etch and along a predetermined plane with respect to the longitudinal axis of said boule; heating said solution at a point adjacent the line of intended etch and providing relative movement between said boule and said chemical etching solution to thereby effect a slicing action of said boule.
Claim 10
Dependent Claim 66 words
a method of slicing a crystal boule in accordance with claim 7, including the steps of; rotating an etchant applicator wheel in said predetermined plane to propel said chemical etching solution; providing a heating element between said applicator wheel and said boule, and passing a current through said element to heat said element and to thereby heat at least one of said boule and said solution.
Claim 11
Dependent Claim 36 words
A method slicing a crystal boule in accordance with claim 8, including the step of applying said etchant to said etchant applicator wheel tangentially to said wheel whereby said etchant is propelled radially from said wheel.
Claim 12
Dependent Claim 75 words
Apparatus for slicing crystal boules, said apparatus comprising: means to clamp a boule in a predetermined position; means for propelling an etchant onto said boule along an intended line and plane of etch, means for applying heat to at least one of said boule and said solution along said intended line of etch, and means for providing relative movement between said boule and said chemical etchant to thereby effect a slicing action of said boule.
Claim 13
Dependent Claim 75 words
Apparatus for slicing crystal boules, said apparatus comprising: means to clamp a boule in a predetermined position; means for propelling an etchant onto said boule along an intended line and plane of etch, means for applying heat to at least one of said boule and said solution along said intended line of etch, and means for providing relative movement between said boule and said chemical etchant to thereby effect a slicing action of said boule.
Claim 14
Dependent Claim 51 words
Apparatus in accordance with claim 10, wherein said means for applying heat to at least one of said boule and said solution comprises a heating element resistant to said etching solution, in the plane of etch and adjacent said boule, and means to permit the passage of current through said element.
Claim 15
Dependent Claim 13 words
Apparatus in accordance with claim 11, wherein said heating element comprises a wire.
Claim 16
Dependent Claim 13 words
Apparatus in accordance with claim 10, wherein said etchant comprises an acid sOlution.
Claim 17
Dependent Claim 24 words
Apparatus in accordance with claim 12, wherein said means for propelling said etchant comprises a rotating etchant applicator wheel in said plane of etch.
Claim 18
Dependent Claim 21 words
Apparatus in accordance with claim 13, wherein said acid solution comprises a mixture of nitric acid, hydrofluoric acid and acetic acid.
Claim 19
Dependent Claim 94 words
Apparatus for slicing a boule of semi-conductor crystal into discrete wafers, said apparatus comprising; means to clamp a boule in a predetermined position; a rotatable etchant applicator wheel and a nozzle positioned to apply chemical etchant material onto the periphery of said wheel, said wheel being positioned in a plane along the intended line of etch of said boule; a heating element intermediate said boule and said wheel and in said plane; and means for providing relative movement between said boule and said chemical etchant to thereby effect a slicing action of said boule.
Claim 20
Dependent Claim 94 words
Apparatus for slicing a boule of semi-conductor crystal into discrete wafers, said apparatus comprising; means to clamp a boule in a predetermined position; a rotatable etchant applicator wheel and a nozzle positioned to apply chemical etchant material onto the periphery of said wheel, said wheel being positioned in a plane along the intended line of etch of said boule; a heating element intermediate said boule and said wheel and in said plane; and means for providing relative movement between said boule and said chemical etchant to thereby effect a slicing action of said boule.

References Cited (Backward Citations)

US2144370A Cited
US2933437A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-10-27 1979-04-28 1979-10-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-10-27 1983-04-28 1983-10-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-10-27 1987-04-28 1987-10-28 $7700.00 Window Closed / Lapsed

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