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US3903337A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for processing cellulose containing material to impart flame resistance

Assignee: Mitsui Toatsu Chemicals Inc
•
Filing: 1974-04-04
•
Granted: 1975-09-02
•
Expires: 1994-04-04
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Abstract

Abstract This invention relates to a new method for imparting flame resistance coupled with excellent resistance to washing to cellulose containing fibrous materials by treatment with a methylene ether bond bearing phosphorus compound.

Inventors

  • 👤 Kosuke Yamamoto
  • 👤 Masahiro Kono

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 12:13
CPC Classifications
D; D06; D06M; D06M13/00; D06M13/244; D06M13/282; D06M13/288; C; C07; C07F; C07F9/00; C07F9/02; C07F9/28; C07F9/38; C07F9/40; C07F9/4003; C07F9/4006

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 51 words
A METHOD FOR FLAMEPROOFING CELLULOSE CONTAINING MATERIAL COMPRISING: PROVIDING A SOLUTION CONTAINING A PHOSPHORUS COMPOUND REPRESENTED BY THE FOLLOWING GENERAL FORMULA: R1-O-P(=O)(-O-R2)-CH2-CH2-CO-NH-CH2-O-CH2-NH-COCH2-CH2-P(=O)(-O-R3)-O-R4 WHEREIN R1 TO R4 ARE THE SAME OR DIFFERENT ALKYL, ALEKNYL, HALOGENALKYL OR ALKOXYALKYL GROUPS, APPLYING SAID SOLUTION TO THE CELLULOSIC CONTAINING MATERIAL, AND DRYING THE CELLULOSIC CONTAINING MATERIAL.
Claim 2
Independent Claim 51 words
A METHOD FOR FLAMEPROOFING CELLULOSE CONTAINING MATERIAL COMPRISING: PROVIDING A SOLUTION CONTAINING A PHOSPHORUS COMPOUND REPRESENTED BY THE FOLLOWING GENERAL FORMULA: R1-O-P(=O)(-O-R2)-CH2-CH2-CO-NH-CH2-O-CH2-NH-COCH2-CH2-P(=O)(-O-R3)-O-R4 WHEREIN R1 TO R4 ARE THE SAME OR DIFFERENT ALKYL, ALEKNYL, HALOGENALKYL OR ALKOXYALKYL GROUPS, APPLYING SAID SOLUTION TO THE CELLULOSIC CONTAINING MATERIAL, AND DRYING THE CELLULOSIC CONTAINING MATERIAL.
Claim 3
Dependent Claim 23 words
The method of claim 1 wherein R1, R2, R3 and R4 are alkyl or halogenalkyl groups having not more than 4 carbon atoms.
Claim 4
Dependent Claim 24 words
The method of claim 1 wherein the phosphorus compound is prepared by condensing a phosphonopropionamide with paraformaldehyde in the presence of an acid catalyst.
Claim 5
Dependent Claim 15 words
The method of claim 2 wherein R1, R2, R3 and R4 are all methyl groups.
Claim 6
Dependent Claim 15 words
The method of claim 2 wherein R1, R2, R3 and R4 are all isopropyl groups.
Claim 7
Dependent Claim 15 words
The method of claim 2 wherein R1, R2, R3 and R4 are all chloroethyl groups.
Claim 8
Dependent Claim 48 words
The method of claim 1 wherein the material is applied in the form of an aqueous solution containing 5-80 percent by weight of said compounds to wet the material and wherein the wetted material is dried and cured at a temperature within the range of 120* to 200*C.

References Cited (Backward Citations)

US3374292A Cited
US3381063A Cited
US3381062A Cited
US3577270A Cited
US3700403A Cited
US3679778A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-09-01 1979-03-03 1979-09-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-09-01 1983-03-03 1983-09-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-09-01 1987-03-03 1987-09-02 $7700.00 Window Closed / Lapsed

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