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US3903075A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the preparation of water-insoluble hydroxybutyl cellulose

Assignee: Hoechst AG
•
Filing: 1971-06-07
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Granted: 1975-09-02
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Expires: 1991-06-07
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Abstract

Abstract This invention relates to a process for the preparation of hydroxybutyl cellulose which comprises etherifying alkali cellulose with butylene oxide in a quantity corresponding to at least four times the weight of cellulose present in the form of alkali cellulose, at a temperature of at least 60*C., continuing the reaction until at least 0.7 mole of butylene oxide per glucose unit has been used for substitution on the cellulose and washing the reaction product with water.

Inventors

  • 👤 Wolfgang Schminke
  • 👤 Hans Macholdt

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 14:38
CPC Classifications
C; C08; C08B; C08B11/00; C08B11/02; C08B11/04; C08B11/08

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 77 words
A PROCESS FOR THE PREPARATION OF HYDROXY BUTLY CELLULOSE WHICH COMPRISES ETHERIFYING ALKALI CELLULOSE IN A SINGLE STAGE WITH BUTYLENE OXIDE IN A QUANTITY CORRESPONDING TO AT LEAST FOUR TIMES THE WEIGHT OF CELLULOSE PRESENT IN THE FORM OF ALKALI CELLULOSE, AT A TEMPERATURE OF AT LEAST 60*C, CONTINUING THE REACTION UNTIL 1.8 TO 3.0 MOLES OF BUTYLENE OXIDE PER GLUCOSE UNIT HAVE BEEN USED FOR SUBSTITUTION ON THE CELLULOSE, AND WASHING THE REACTION PRODUCT WITH WATER.
Claim 2
Dependent Claim 77 words
A PROCESS FOR THE PREPARATION OF HYDROXY BUTLY CELLULOSE WHICH COMPRISES ETHERIFYING ALKALI CELLULOSE IN A SINGLE STAGE WITH BUTYLENE OXIDE IN A QUANTITY CORRESPONDING TO AT LEAST FOUR TIMES THE WEIGHT OF CELLULOSE PRESENT IN THE FORM OF ALKALI CELLULOSE, AT A TEMPERATURE OF AT LEAST 60*C, CONTINUING THE REACTION UNTIL 1.8 TO 3.0 MOLES OF BUTYLENE OXIDE PER GLUCOSE UNIT HAVE BEEN USED FOR SUBSTITUTION ON THE CELLULOSE, AND WASHING THE REACTION PRODUCT WITH WATER.

References Cited (Backward Citations)

US2053768A Cited
US3131176A Cited
US3131177A Cited
US3251825A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-09-01 1979-03-03 1979-09-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-09-01 1983-03-03 1983-09-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-09-01 1987-03-03 1987-09-02 $7700.00 Window Closed / Lapsed

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