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US3901772A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of sealing by brazing of a metal part on a ceramic part

Assignee: QUARTEX POUR L APPLIC Ste
•
Filing: 1973-11-26
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Granted: 1975-08-26
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Expires: 1993-11-26
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Abstract

Abstract The present invention relates to a method of brazing a fluidtight sealing joint between a metal part and a part of ceramic material, of the kind in which, before the actual brazing is carried out, the said ceramic part is first metallized by the application of a metallization product containing at least one metallic derivative, and sintering the said product, followed by nickelling of the ceramic part thus metallized, the operations of metallization being repeated twice, said method comprising the further steps of effecting the metallization of said ceramic part by applying said metallization product and effecting two successive nickelling operations on the ceramic part thus metallized, a first nickelling operation being effected chemically by the application of a nickelling product and reduction of said product under heat, while a second nickelling operation is carried out by an electrolytic process. The invention finds a particular application in the brazing of joints sealing a metallic conductor into a bore passing through a ceramic part.

Inventors

  • 👤 Fernand Guillotin
  • 👤 Rene Cerutti

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 18:50
CPC Classifications
C; C04; C04B; C04B37/00; C04B37/02; C04B37/023; C04B37/026; C04B2237/00; C04B2237/02; C04B2237/12; C04B2237/123; C04B2237/124; C04B2237/125; C04B2237/30; C04B2237/32; C04B2237/34; C04B2237/343; C04B2237/40; C04B2237/403; C04B2237/405; C04B2237/50; C04B2237/76; C04B2237/84

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 78 words
A METHOD FOR SEALING A METAL PART TO A CERAMIC PART COMPRISING THE CONSECUTIVE STEPS OF METALIZING THE CERAMIC PART WITH METALIZING MATERIAL CONTAINING AT LEAST ONE METALLIC DERIVATIVE, SINTERING THE METALIZED CERAMIC PART, THEN NICKELING THE CERAMIC PART FIRST CHEMICALLY IN A REDUCING ATMOSPHERE AT AN ELEVATED TEMPERATURE AND THEN ELECTROLYTICALLY, THE METALIZING STEP COMPRISING SPREADING THE METALIZING MATERIAL ON THE CERAMIC PART BY RECIPROCATING A SUBSTANTIALLY RIGID APPLICATOR MEMBER IN SLIDING CONTACT WITH THE CERAMIC PART.
Claim 2
Independent Claim 78 words
A METHOD FOR SEALING A METAL PART TO A CERAMIC PART COMPRISING THE CONSECUTIVE STEPS OF METALIZING THE CERAMIC PART WITH METALIZING MATERIAL CONTAINING AT LEAST ONE METALLIC DERIVATIVE, SINTERING THE METALIZED CERAMIC PART, THEN NICKELING THE CERAMIC PART FIRST CHEMICALLY IN A REDUCING ATMOSPHERE AT AN ELEVATED TEMPERATURE AND THEN ELECTROLYTICALLY, THE METALIZING STEP COMPRISING SPREADING THE METALIZING MATERIAL ON THE CERAMIC PART BY RECIPROCATING A SUBSTANTIALLY RIGID APPLICATOR MEMBER IN SLIDING CONTACT WITH THE CERAMIC PART.
Claim 3
Dependent Claim 34 words
A method as claimed in claim 1, wherein the substantially rigid applicator member is a rod, and the metalizing Material is applied by reciprocating sliding movement of the rod relative to the ceramic part.
Claim 4
Dependent Claim 36 words
A method as claimed in claim 1, wherein the ceramic part has a bore therein, and wherein the metalizing material is applied in the bore by axial reciprocating sliding movement of a rod in the bore.
Claim 5
Dependent Claim 36 words
A method as claimed in claim 3, wherein the electrolytic nickeling comprises inserting a U-shaped metal loop into the bore in the ceramic part and connecting said loop to the negative pole of an electric source.
Claim 6
Dependent Claim 18 words
A method as claimed in claim 3, wherein a countersink is provided at an end of the bore.
Claim 7
Dependent Claim 15 words
A method as claimed in claim 5, where in the countersink is frustoconical in shape.
Claim 8
Dependent Claim 34 words
A method as claimed in claim 1 in which a peripheral clearance of 0.03 to 0.05 mm is provided between said metal part and said bore, and brazing said metal part in said core.

References Cited (Backward Citations)

US2722496A Cited
US2821013A Cited
US3006069A Cited
US3023492A Cited
US3290171A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-08-25 1979-02-24 1979-08-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-08-25 1983-02-24 1983-08-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-08-25 1987-02-24 1987-08-26 $7700.00 Window Closed / Lapsed

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