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US3899554A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for forming a ceramic substrate

Assignee: International Business Machines Corp
•
Filing: 1973-12-14
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Granted: 1975-08-12
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Expires: 1993-12-14
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Abstract

Abstract Production of a sintered ceramic dielectric formed from a green sheet having a uniform microporous structure providing uniform dielectric properties and compressibility for lamination of stacked green sheets into a unitary laminate which may be provided with an internal pattern of electrical conductors extending therein. The structure is obtained by blending the ceramic particulate with a binder resin soluble in an azeotropic mixture which is formed from a solvent for the binder resin and a non-solvent in which the resin is at most only slightly soluble, which on evaporation of said azeotropic mixture forms said structure.

Inventors

  • 👤 Harold D Kaiser
  • 👤 Robert W Nufer

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 14:55
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/622; C04B35/626; C04B35/63; C04B35/632; C04B35/634; C04B35/63404; C04B35/6342; B; B32; B32B; B32B3/00; B32B3/26; B32B3/266; B32B43/00; B32B43/006; B32B7/00; B32B7/04; B32B7/12; B32B38/00; B32B38/04; B32B2038/042; B32B2264/00; B32B2264/10; B32B2264/107; B32B2315/00; B32B2315/02

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 97 words
IN A PROCESS FOR FORMING CERAMIC SUBSTRATES, THE STEPS COMPRISING: A. FORMULATING A CERAMIC SLIP COMPOSITION BY BLENDING A CERAMIC PARTICULATE WITH A SOLVENT SOLUBLE THERMOPLATIC BINDER RESIN DISSLOVED IN A VOLATILE ORGANIC SOLVENT MIXTURE FORMING A COMPLETE SOLVENT FOR SAID RESIN AND COMPRISING A VOLATILE FIRST SOLVENT FRACTION AND A VOLATILE SECOND NON-SOLVENT FRACTION WITH SAID FIRST SOLVENT FRACTION CONSTITUTING A COMPLETE SOLVENT FOR SAID RESIN AND SAID SECOND FRACTION BEING SUBSTANTIALLY A NON-SOLVENT FOR SAID RESIN, SAID FIRST AD SECOND SOLVENT FRACTIONS COMBINING TO FORM AN AZEOTROPIC MIXTURE, WITH AN EXCESS OF SAID NONSOLVENT FRACTION:
Claim 2
Dependent Claim 97 words
IN A PROCESS FOR FORMING CERAMIC SUBSTRATES, THE STEPS COMPRISING: A. FORMULATING A CERAMIC SLIP COMPOSITION BY BLENDING A CERAMIC PARTICULATE WITH A SOLVENT SOLUBLE THERMOPLATIC BINDER RESIN DISSLOVED IN A VOLATILE ORGANIC SOLVENT MIXTURE FORMING A COMPLETE SOLVENT FOR SAID RESIN AND COMPRISING A VOLATILE FIRST SOLVENT FRACTION AND A VOLATILE SECOND NON-SOLVENT FRACTION WITH SAID FIRST SOLVENT FRACTION CONSTITUTING A COMPLETE SOLVENT FOR SAID RESIN AND SAID SECOND FRACTION BEING SUBSTANTIALLY A NON-SOLVENT FOR SAID RESIN, SAID FIRST AD SECOND SOLVENT FRACTIONS COMBINING TO FORM AN AZEOTROPIC MIXTURE, WITH AN EXCESS OF SAID NONSOLVENT FRACTION:
Claim 3
Dependent Claim 36 words
In a process for forming ceramic substrates as in claim 1 further including the step of varying the amount of the second non-solvent fraction with respect to the first solvent for adjusting the quantity of micropores.
Claim 4
Dependent Claim 46 words
In a process for forming ceramic substrates as in claim 1 wherein said azeotropic mixture is a ternary mixture, at least one member of which is a complete solvent for and at least one member of which is substantially a non-solvent for said thermoplastic binder resin.
Claim 5
Dependent Claim 23 words
In a process for forming ceramic substrates as in claim 1 wherein said first solvent is methanol and said second non-solvent is toluene.
Claim 6
Dependent Claim 27 words
In a process for forming ceramic substrates as claimed in claim 1 wherein the boiling point of said non-solvent is above the boiling point of the azeotrope.
Claim 7
Dependent Claim 35 words
In a process for forming ceramic substrates as claimed in claim 1 wherein the ratio in parts by weight of the binder resin system to solvent system is within the range of 1:2 to 1:12.
Claim 8
Dependent Claim 35 words
In a process for forming ceramic substrates as claimed in claim 1 wherein the ratio in parts by weight of the binder resin system to solvent system is within the range of 1:5 to 1:7.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-08-11 1979-02-10 1979-08-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-08-11 1983-02-10 1983-08-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-08-11 1987-02-10 1987-08-12 $7700.00 Window Closed / Lapsed

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